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Development of Noncontact Mode Scanning Force/Tunneling Microscopy

Research Project

Project/Area Number 09555005
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field 表面界面物性
Research InstitutionOsaka University

Principal Investigator

MORITA Seizo  Department of Electronic Engineering, Graduate School of Engineering, Osaka University Professor, 大学院・工学研究科, 教授 (50091757)

Project Period (FY) 1997 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥12,800,000 (Direct Cost: ¥12,800,000)
Fiscal Year 1998: ¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 1997: ¥11,100,000 (Direct Cost: ¥11,100,000)
Keywordsatomic force microscope / atomic force / scanning tunneling microscope / tunneling current / well-defined surface / atomic resolution / semiconductor surface / AFM / STM
Research Abstract

Simultaneous measurement of atomic force and tunneling current will offer new opportunity to investigate the mechanical and electronic properties on the surface on an atomic scale. However, so far, simultaneous measurement of atomic force and tunneling current has not been achieved on atomic scale. This is due to the following three main reasons : (i) It is much difficult to measure weak attractive atomic force with a good signal-to-noise (SIN) ratio. (ii) It is much difficult to develop the clean and sharp conducting tip with atomic scale. (iii) It is much difficult to reduce the cross-talk between the atomic force and tunneling current.
In this project, we constructed noncontact mode scanning atomic force/tunneling microscope (noncontact AFM/STM) to detect atomic force and tunneling current simultaneously on atomic scale. Atomic force measurement is based on frequency modulation (FM) detection method. The high sensitive atomic force measurement was realized by improving the displacement sensor and FM demodulator. Novel technique to fabricate the clean and sharp conducting Si cantilevers was developed, in which the argon ion sputtering method was used. Also, new technique to measure the atomic force and tunneling current without the cross-talk was developed, which is based on the frequency and time domain method. Measurement conditions for simultaneous measurement of atomic force and tunneling current were investigated theoretically and experimentally.

Report

(3 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • Research Products

    (65 results)

All Other

All Publications (65 results)

  • [Publications] Y.Sugawara et al.: ""True atomic resolution imaging with noncontact atomic force microscopy"" Appl.Sur.Sci.113/114. 364-370 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe et al.: "Measurement of the Evanescent Field Using Noncontact Mode Atomic Force Microscope"" Opt.Rev.4・1B. 232-235 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi et al.: ""Charge Dissipation on Chemically Treated Thin Silicon Oxide in Air"" Jpn.J.Appl.Phys.36・6A. 3755-3758 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi et al.: ""Development of ultrahigh vacuum atomic force microscopy with frequency modulation detection and its application to electrostatic force measurement"" J.Vac.Sci.Technol.B. 15・4. 1543-1546 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe et al.: ""Detection mechanism of optical evanescent field using a noncontact mode Atomic force microscope with a frequency modulation detection method"" J.Vac.Sci.Technol.B. 15・4. 1512-1515 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] N.Sasaki et al.: ""Analysis of frictional-force image patterns of a graphite surface"" J.Vac.Sci.Technol.B. 15・4. 1479-1482 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] J.Ohgami et al.: ""Growth of Two-Dimensional Nucleus on a Cleaved (010) Surface of (NH_2CH_2COOH)_3・H_2SO_4"" J.Phys.Soc.Jpn.66・9. 2747-2750 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi et al.: ""Role of a covalent bonding interaction in noncontact-mode atomic-force microscopy"" Phys.Rev.B. 56・16. 9834-9840 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Nishi et al.: ""Simulated Computed Tomography for Reconstruction of Vacancies from Atomic Force Microscope Image"" Jpn.J.Appl.Phys.36・10B. L1410-L1412 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe et al.: ""Force Imaging of Optical Near-Field Using Noncontact Mode Atomic Force Microscopy"" Jpn.J.Appl.Phys.37・2A. L167-L169 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] H.Ueyama et al.: ""Stable operation mode for dynamic noncontact atomic force microscopy"" Appl.Phys.A. 66. S295-S297 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Nishi et.al.: ""New computed tomography algorithm of electrostatic force microscopy based on the singular value decomposition combined with the discrete Fourier transform"" Jpn.J.Appl.Phys.37・4A. L417-L419 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] N.Sasaki et al.: "Theoretical analysis of atomic-scale friction in frictional-force microscopy" Tribology Lett.4. 125-128 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Fujisawa et.al.: "Analysis of experimental load dependence of two-dimensional atomic-scale friction" Phys.Rev.B. 58・8. 4909-4916 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe et al.: "Optical near-field imaging using Kelvin probe technique" Jpn.J.App.Phys.37・9A/B. L1074-L1077 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Orisaka et.al.: ""The Atomic Resolution Imaging of Metallic Ag(111)Surface by Noncontact Atomic Force Microscope"" Appl.Sur.Sci.140・3-4. 243-246 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Minobe et.al.: ""Distance Dependence of Noncontact AFM Image Contrast on Si(111)√<3>×√<3>-Ag Structure"" Appl.Sur.Sci.140・3-4. 298-303 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi et.al.: ""Imaging of Chemical Reactivity and Buckled Dimers on Si(100)2×1 Reconstructed Surface with Noncontact AFM"" Appl.Sur.Sci.140・3-4. 304-308 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Sugawara et.al.: "True atomic resolution imaging of surface structure and surface charge on the GaAs(110)" Appl.Sur.Sci.140・3-4. 371-375 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe et.al.: ""Near-field Optical Imaging Using Force Detection with New Tip-Electrode Geometry"" Appl.Sur.Sci.140・3-4. 383-387 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Morita and Y.Sugawara: ""Guidelines for the Achievement of True Atomic Resolution with Noncontact Atomic Force Microscopy"" Appl.Sur.Sci.140・3-4. 406-410 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Sugawara et.al.: "Non-contact AFM Images Measured on Si(111)√<3>×√<3>-Ag and Ag(111)" Surface and Interface Analysis. 27・5-6(In press). (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Sugawara, H.Ueyama, T.Uchihashi, M.Ohta, S.Morita, M.Suzuki and S.Mishima: ""True atomic resolution imaging with noncontact atomic force microscopy"" Appl.Sur.Sci.Vol.113/114. 364-370 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe, T.Uchihashi, M.Ohta, H.Ueyama, Y.Sugawara, and S.Morita :""Measurement of the Evanescent Field Using Noncontact Mode Atomic Force Microscope"" Opt.Rev.Vol.4, No.1B. 232-235 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi, A.Nakano, T.Ida, Y.Ando, R.Kaneko Y.Sugawara and S.Morita ;: ""Charge Dissipation on Chemically Treated Thin Silicon Oxide in Air"" Jpn.J.Appl.Phys.Vol.36, Part I No.6A. 3755-3758 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi, M.Ohta, Y.Sugawara, Y.Yanase, T.Shigematsu, M.Suzuki and S.Morita :""Development of ultrahigh vacuum atomic force microscopy with frequency modulation detection and its application to electrostatic force measurement"" J.Vac.Sci.Technol.B. Vol.15, No.4. 1543-1546 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe, T.Uchihashi, M.Ohta, M.Ohta, H.Ueyama, Y.Sugawara and S.Morita :""Detection mechanism of optical evanescent field using a noncontact mode Atomic force microscope with a frequency modulation detection method"" J.Vac.Sci.Technol.B. Vol.15, No.4. 1512-1515 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] N.Sasaki, M.Tsukada, S.Fujisawa, Y.Sugawara, S.Morita and K.Kobayashi :""Analysis of frictional-force image patterns of a graphite surface"" J.Vac.Sci.Technol.B. Vol.15, No.4. 1479-1482 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] J.Ohgami, Y.Sugawara, S.Morita and T.Ozaki :""Growth of Two-Dimensional Nucleus on a Cleaved (010) Surface of (NH_2CH_2COOH)_3・H_2SO_4"" J.Phys.Soc.Jpn.Vol.66, No.9. 2747-2750 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi, Y.Sugawara, T.Tsukamoto, M.Ohta and S.Morita :""Role of a covalent bonding Interaction in noncontact-mode atomic-force mictoscopy"" Phys.Rev.B. Vol.56, No.16. 9834-9840 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Nishi, T.Ohta, Y.Sugawara, S.Morita and T.Okada :""Simulated Computed Tomography for Reconstruction of Vacancies from Atomic Force Microscope Image"" Jpn.J.Appl.Phys.Vol.36, No.10B. L1410-L1412 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe, Y.Sugawara, Y.Hara, K.Sawada and S.Morita :""Force Imaging of Optical Near-Field Using Noncontact Mode Atomic force Misroscopy"" Jpn.J.Appl.Phys.Vol.37, No.2A. L167-L169 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] N.Sasaki, M.Tsukada, S.Fujisawa, Y.Sugawara, S.Morita and K.Kobayashi: ""Load dependence of the frictional-force microscopy image pattern of the graphite surface"" Phys.Rev.B. Vol.57, No.7. 3785-3786 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] H.Ueyama, Y.Sugawara and S.Morita: ""Stable operation mode for dynamic noncontact atomic force microscopy"" Appl.Phys.A. Vol.66. S292-S297 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Nishi, Y.Nakao, T.Ohta, Y.Sugawara, S.Morita and T.Okada: ""New computed tomography algorithm of electrostatic force microscopy based on the singular value decomposition combined with the discrete Fourier transform"" Jpn.J.Appl.Phys.Vol.37, No.4A. L417-L419 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] N.Sasaki, M.Tsukada, S.Fujisawa, Y.Sugawara and S.Morita: ""Theoretical analysis of atomic-scale friction in frictional-force microscopy"" Tribology Lett.Vol.4. 125-128 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Fujisawa, K.Yokoyama, Y.Sugawara and S.Morita: ""Analysis of experimental load dependence of two-dimensional atomic-scale friction"" Phys.Rev.B. Vol.58, No.8. 4909-4916 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe, Y.Sugawara, Y.Hara, K.Sawada and S.Morita: ""Force Imaging of Optical Near-Field Using Noncontact Mode Atomic Force Microscopy"" Jpn.J.Appl.Phys.Vol.37, No.9A/B. L1074-L1077 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Orisaka, T.Minobe, Y.Sugawara and S.Morita: ""The Atomic Resolution Imaging of Metallic Ag(111)Surface by Noncontact Atomic Force Microscope"" Appl.Sur.Sci.Vol.140, No.3-4. 243-246 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Minobe, T.Uchihashi, T.Tsukamoto, S.Orisaka, Y.Sugawara and S.Morita: ""Distance Dependence of Noncontact AFM Image Contrast on Si(111)ROO<3>3*ROO<3>3-Ag Structure"" Appl.Sur.Sci.Vol.140, No.3-4. 298-303 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Uchihashi, Y.Sugawara, T.Tsukamoto, T.Minobe, S.Orisaka T.Okada and S.Morita: ""Imaging of Chemical Reactivity and Buckled Dimers on Si(100)2*1 Reconstructed Surface with Noncontact AFM"" Appl.Sur.Sci.Vol.140, No.3-4. 304-308 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Sugawara, T.Uchihashi, M.Abe and S.Morita: ""True Atomic Resolution Imaging of Surface Structure and Surface Charge on the GaAs(110)"" Appl.Sur.Sci.Vol.140, No.3-4. 371-375 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Abe, Y.Sugawara, K.Sawada, Y.Andoh and S.Morita :""Near-field Optical Imaging Using Force Detection with New Tip-Electrode Geometry"" Appl.Sur.Sci.Vol.140, No.3-4. 383-387 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Morita and Y.Sugawara ;: ""Guidelines for the Achievement of True Atomic Resolution with Noncontact Atomic Force Microscopy"" Appl.Sur.Sci.Vol.140, No.3-4. 406-410 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Sugawara, T.Minobe, S.Orisaka, T.Uchihashi, T.Tsukamoto and S.Morita: ""Non-contact AFM Images Measured on Si(111)ROO<3>3*ROO<3>3-Ag and Ag(111)Surfaces"" Surface and Interface Analysis. Vol.27, No.5-6(In press). (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] H.Ueyama et al.: "“Stable operation mode for dynamic noncontact atomic force microscopy"" Appl.Phys.A. Vol.66. S295-S297 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] R.Nishi et.al.: ""New computed tomography algorithm of electrostatic force microscopy based on the singular value decomposition combined with discrete Fourier transform"" Jpn.J.Appl.Phys.37・4A. L417-L419 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M・Abe et.al.: "Optical near-field imaging using Kelvin probe technique" Jpn.J.App.Phys.37・9A/B. L1074-L1077 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Sugawara et.al.: "True atomic resolution imaging of surface structure and surface charge on the GaAs(110)" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] S.Orisaka et.al.: "“The Atomic Resolution Imaging of Metallic Ag(111)Surface by Noncontact Atomic Force Microscope"" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] S.Morita and Y.Sugawara: "“Guidelines for the Achievement of True Atomic Resolution with Noncontact Atomic Force Microscopy"" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] T.Minobe et.al.: "“Distance Dependence of Noncontact AFM Image Contrast on Si(111)【square root】3×【square root】3-Ag Structure"" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Abe et.al.: "“Near-field Optical Imaging Using Force Detection with New Tip-Electrode Geometry"" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] T.Uchihashi et.al.: "“Imaging of Chemical Reactivity and Buckled Dimers on Si(100)2×1 Reconstructed Surface with Noncontact AFM"" Appl.Sur.Sci.137・3-4. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Sugawara et al.: "“True atomic resolution imaging with noncontact atomic force microscopy"" Appl.Sur.Sci.Vol.113/114. 364-370 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Abe et al.,: "Measurement of the Evanescent Field Using Noncontact Mode Atomic Force Microscope″" Opt.Rev.Vol.4,No.1B. 232-235 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] T.Uchihashi et al.: "“Charge Dissipation on Chemically Treated Thin Silicon Oxide in Air″" Jpn.J.Appl.Phys.Vol.36,No.6A. 3755-3758 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] T.Uchihashi et al.: "“Development of ultrahigt vacuum atomic force microscopy with frequency modulation detection and its aplication to electrostatic force measurement″" J.Vac.Sci.Technol.B.Vol.15,No.4. 1543-1546 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Abe et al.: "“Detection mechanism of optical evanescent field using a noncontact mode Atomic force microscope with a frequency modulation detectionmethod"" J.Vac.Sci.Technol.B.Vol.15,No.4. 1512-1515 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] N.Sasaki et al.: "“Analysis of frictional-force image patterns of a graphite surface"" J.Vac.Sci.Technol.B.Vol.15,No.4. 1479-1482 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] J.Ohgami et al.: "“Growth of Two-Dimensional Nucleus on a Cleaved(010)Surface of (NH_2CH_2COOH)_3・H_2SO_4″" J.Phys.Soc.Jpn.Vol.66,No.9. 2747-2750 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] T.Uchihashi et al.: "“Role of a covalent bonding interaction in noncontact-mode atomic-force microscopy"" Phys.Rev.B. Vol.56,No.16. 9834-9840 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] R.Nishi et al.: "“Simulated Computed Tomography for Reconstruction of Vacancies from Atomic Force Microscope Image"" Jpn.J.Appl.Phys.Vol.36,No.10B. L1410-L1412 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Abe et al.: "“Force Imaging of Optical Near-Field Using Noncontact Mode Atomic Force Microscopy"" Jpn.J.Appl.Phys.Vol.37,No.2A. L167-L169 (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] H.Ueyama et al.: "“Stable operation mode for dynamic noncontact atomic force microscopy"" Appl.Phys.A.Vol.66(in press). (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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