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Development of Scanning Nonlinear Dielectric Microscope with high resolution and its Application to Ferroelectric Recording

Research Project

Project/Area Number 09555022
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Applied physics, general
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

CHO Yasuo  Research Institute of Electrical Communication, Tohoku University, Associate Professor, 電気通信研究所, 助教授 (40179966)

Project Period (FY) 1997 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥12,700,000 (Direct Cost: ¥12,700,000)
Fiscal Year 1999: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1998: ¥5,700,000 (Direct Cost: ¥5,700,000)
Fiscal Year 1997: ¥6,100,000 (Direct Cost: ¥6,100,000)
KeywordsScanning Nonlinear dielectric microscopy / nano-meter resolution / ferroelectric domain / ferroelectric recording / 局所異方性 / 分極ドメイン / 強誘電体 / ドメイン / 高分解能
Research Abstract

Recently, we have proposed and developed a new, purely electrical method for imaging the state of remanent polarization of ferroelectric materials, which involves the measurement of point-to-point variation of the nonlinear dielectric constant of a specimen, and is termed "scanning nonlinear dielectric microscopy (SNDM)". However, greater demand for the observation of very small domains (or dipoles) of nanometer size has arisen amongst researchers of ferroelectric materials to, for example, investigate domain wall structures or clarify minimum domain sizes.
To achieve higher resolution of the nanometer order, a probe contact sensing mechanism for detecting the exact contact point of the probe needle with the surface of specimen were developed. By combining the contact sensing mechanism and a new lumped constant resonator probe with a very tin pointed end needle, we have succeeded in developing a SNDM system with nanometer resolution.
Next, a theory for scanning nonlinear dielectric microscopy (SNDM) and its application to the quantitative evaluation of the linear and nonlinear dielectric constants of dielectric materials were also developed. A general theorem for the capacitance variation under an applied electric field is derived and then, it was proved that the sensitivity of the SNDM probe does not change, even if a tip with a smaller radius is selected to obtain a finer resolution. Using the theoretical results and the data taken by SNDM, the quantitative linear and nonlinear dielectric properties of several dielectric materials were successfully determined. From the calculation of a one-dimensional image of a 180°c-c domain boundary, it is demonstrated that the SNDM has an atomic scale resolution. The polarities of piezoelectric thin films on piezoelectric substrates were also determined.
Finally, we succeeded in the basic experiment on ferroelectric recording system with a micron-meter order ferroelectric bits.

Report

(4 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (27 results)

All Other

All Publications (27 results)

  • [Publications] 長康雄: "走査型非線形誘電率顕微鏡"応用物理. Vol.67,No.3. 327-331 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Cho.,K.Matsuura and J.Kushibiki: "Scanning nonlinear dielectric microscope with submicron resolution"Jpn. J. Appl. Phys.. Vol.37,No.5B. 3132-3133 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Cho,K.Matsuura,S.Kazuta,H.Odagawa and KYamanouchi: "Observation of Ultra thin Single-domain Layers Formed on LiTaO_3 and LiNbO_3 Surface Using Scanning Nonlinear Dielectric Microscope with Submicron Resolution"Jpn. J. Appl. Phys.. Vol.38,No.5B. 3279-3282 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Cho,S.Kazuta and K.Matsuura: "Scanning Nonlinear Dielectric Microscopy with Contact Sensing Mechanisum for Observation of Nano-Meter Sized Ferroelectric Domains"Jpn. J. Appl. Phys.. Vol.38,No.9B. 5689-5694 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Cho,S.Kazuta and K.Matsuura: "Scanning Nonlinear Dielectric Microscopy with Nano-Meter Resolution"Appl. Phys. Lett.. Vol.72,No.18. 2833-2835 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Cho,S.Kazuta,K.Ohara and H.Odagawa: "Quantitative Measurement of Linear and Nonlinear Dielectric Characteristics Using Scanning Nonlinear Dielectric Microscopy"Jpn. J. Appl. Phys.. Vol.39No.5B(印刷中). (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yasuo Cho: "Scanning nonlinear dielectric microscope"OYO BUTSURI. Vol.67, No.3. 327-331 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Cho, K. Matsuura and J. Kushibiki: "Scanning nonlinear dielectric microscope with submicron resolution"Jpn. J. Appl. Phys.. Vol.37, No.5B. 3132-3133 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Cho, K. Matsuura, S. Kazuta, H. Odagawa and K. Yamanouchi: "Observation of ultra thin single-domain layers formed on LiTaOィイD23ィエD2 and LiNbOィイD23ィエD2 surface using scanning nonlinear dielectric microscope with submicron resolution"Jpn. J. Appl. Phys.. Vol.38, No.5B. 3279-3282 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Cho, S. Kazuta and K. Matsuura: "Scanning Nonlinear Dielectric Microscopy with Contact Sensing Mechanism for Observation of Nano-Meter Sized Ferroelectric Domains"Jpn. J. Appl. Phys.. Vol.38, No.9B. 5689-5694 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Cho, S. Kazuta and K. Matsuura: "Scanning Nonlinear Dielectric Microscopy with Nano-Meter Resolution"Appl. Phys. Lett.. Vol.72, No.18. 2833-2835 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Cho, S. Kazuta, K. Ohara and H. Odagawa: "Quantitative Measurement of Linear and Nonlinear Dielectric Characteristics Using Scanning Nonlinear Dielectric Microscopy"Jpn. J. Appl. Phys.. Vol.39 (in print). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 長 康雄: "走査型非線形誘電率顕微鏡"応用物理. Vol.67・No.3. 327-331 (1988)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Cho,K.Matsuura and J.Kushibiki: "Scanning nonlinear dielectric microscope with submicron resolution"Jpn. J. Appl. Phys.. Vol.37・No.5B. 3132-3133 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Cho,K.Matsuura,S.Kazuta,H.Odagawa and K.Yamanouchi: "Observation of Ultra thin Single-domain Layers Formed on LitaO_3 and LiNbO_3 Surface Using Scanning nonlinear dielectric microscope with submicron resolution"Jpn. J. Appl. Phys.. Vol.38・No.5B. 3279-3282 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Cho,S.Kazuta and K.Matsuura: "Scanning Nonlinear Dielectric Microscopy with Contact Sensing Mechanism for Observation of Nano-Meter Sized Ferroelectric Domains"Jpn. J. Appl. Phys.. Vol.38・No.9B. 5689-5694 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Cho,S.Kazuta and K.Matsuura: "Scanning Nonlinear Dielectric Microscopy with Nano-Meter Resolution"Appl. Phys. Lett.. Vol.72・No18. 2833-2835 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Cho,S.Kazuta,K.Ohara and H.Odagawa: "Quantitative Measurement of Linear and Nonlinear Dielectric Characteristics Using Scanning Nonlinear dielectric Microscopy"Jpn. J. Appl. Phys.. Vol.73・No.5B. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 長 康雄: "走査型非線形誘電率顕微鏡" 応用物理. 67. 327-331 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Cho,K.Matsuura,J.Kushibiki: "Scanning Nonlinear Dielectric Microscope with Submicron Resolution" Jpn.J.Appl.Phys.37. 3132-3133 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Cho,K.Matsuura,S.Kazuta,K.Yamanouchi: "Observation of Ultra Thin Single Domain Layers Formed on LiTaO,and LiNbo, Surfaces Using Scanning Nonlinear Dielectric Microscope with Submicron Resolution" Jpn.J.Appl.Phys.38. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Cho.: "Observation of Photothermal Dielectric Signal for Powder" Jpn.J.Appl.Phys.Vol.36・No.5B. 3303-3304 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Cho.: "Scanning Nonlinear Dielectric Microscope Using a Lumped Constant Resonator Probe and Its Application to Investigation of Ferroelectric Polarization Distribution" Jpn.J.Appl.Phys.Vol.36.No.5B. 3152-3156 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Cho,: "Microscopic Observation of the Temperature Coefficient Distribution of Dielectric Material for Microwave Application Using Scanning Phototharmal Dielectric Microscope" 1997 IEEE MTT-S International Microwave Synposium. 1647-1650 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Cho: "Temperature Coefficient Image of Dielectric Material" Jpn.J.Appl.Phys.Vol.36,No.90. 6001-6003 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 長 康雄: "走査型非線形誘電率顕微鏡" 応用物理. 67巻3号. (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Cho,: "Scanning Nonlinear Dielectric Microscope" Jpn.J.Appl.Phys.Vol.37,No.5B. (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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