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FABRICATION OF HIGH STRAIN RATE SUPERPLASTIC ALLOYS USING INTENSE PLASTIC STRAINING

Research Project

Project/Area Number 09555212
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Structural/Functional materials
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

NEMOTO Minoru  Kyushu Univ., Dpt.Mater.Sci.& Eng., prof., 工学部, 教授 (90005265)

Co-Investigator(Kenkyū-buntansha) TOINO Harumichi  Nippon Light Metal Co.Ltd., R&D Center, Manager, 技術開発本部・製品化技術室, 主任研究員
OH-ISHI Keiichiro  Kyushu Univ., Dpt.Mater.Sci.& Eng., Ass., 工学部, 助手 (70294890)
HORITA Zenji  Kyushu Univ., Dpt.Mater.Sci.& Eng., Ass.Prof., 工学部, 助教授 (20173643)
Project Period (FY) 1997 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥10,400,000 (Direct Cost: ¥10,400,000)
Fiscal Year 1998: ¥1,200,000 (Direct Cost: ¥1,200,000)
Fiscal Year 1997: ¥9,200,000 (Direct Cost: ¥9,200,000)
Keywordssuperplasticity / equal-channel angular pressing / microstructural evolution / ultrafine grain sizes / aluminum alloys / intense straining / grain growth / TEM / 高速超塑性 / ECAE / Al合金 / 再結晶 / 組織設計
Research Abstract

The equal-channel angular (ECA) pressing is capable of introducing an ultrafine grain size into bulk materials and the precise nature of the microstructure is dependent upon the total strain introduced by the pressing, temperature and speed of pressing. When the strain is sufficiently high, it is possible to achieve very high tensile ductilities at high strain rates. It is noted that the use of different processing routes provides an opportunity to alter the shearing planes and shear directions within the sample and therefore to modify, in a favorable manner, the microstructures induced by ECA pressing. It is known that the combination of shear in three dimensional way is effective to increase the amount of misorientation formed during each pressing. The attained grain size is as small as 1.2 micrometers even in high purity aluminum. When the alloying elements are added, the attained grain size reduced appreciably. To increase the elevated temperature stability of fine grain size, whic … More h is a prerequisite for attaining high strain rate superplasticity, a fine dispersion of particles is required. The present results provide a very clear demonstration of refinement of grain size and resultant advantageous high strain rate superplasticity which may be achieved by ECA pressing and microstructural control in a typical commercial Al-Mg-Li-Zr alloy where precipitates are present to retain the ultrafine grain sizes even at high temperatures where diffusion is rapid. Similar grain refinement and high strain rate superplasticity are achieved also in a commercial Al-2004 alloy known as Supral 100 with a chemical composition of Al-6% Cu-0.4% Zr. Furthermore, the exceptionally high strain rate superplasticity of the Al-3%Mg-0.2%Sc alloy was achieved by ECA pressing at room temperature without the use of any intermediate heating. In the Al-Mg-Sc alloy, the migration of grain boundaries are suppressed by the fine dispersion Al_3 Sc phase and then enhancing the grain boundary sliding and the matrix is solution strengthened by Mg suppressing the dislocation glide in the grains. The present work also provides the potential for substantially increasing the viability of superplastic forming in the metal forming industry. Less

Report

(3 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • Research Products

    (52 results)

All Other

All Publications (52 results)

  • [Publications] S.Komura: "High Strain Rate Supenpiasticity in a Al-Mg Alloy Containing Scandium" Scripta Mater.38・12. 1851-1856 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi: "Microstructural Characteristics of Ultrafine-Graiued Aluminum Produced Using Equal-Channel Augular Pressing" Metall. Mater. Trans.29A・9. 2245-2252 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa: "Factors Influencing the Flow and Hardnoss of Materials with Ultrafine Grain Sizes" Phil. Mag. A. 78・1. 203-215 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi: "Factors Influencing the Equilibrium Grain Size in Equal-Channel Angular Pressing : Role of Additions of Aluminum" Metall. Mater. Trans.29A・10. 2503-2510 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa: "The Shearing Characteristics Associated with Equal-Channel Angular Pressing" Mater. Sci. Eng.257A. 328-332 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 堀田 善治: "新しい組織制御法としての Equal-Channel Angular Pressing(ECAP)" まてりあ(日本金属学会会報). 37・9. 9-16 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, P.Berbpm, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Production of Ultrafine-Grained Metallic Materials Using an Intense Plastic Straining Technique" Materials Science Forum. Vols.233-234. 177-184 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Z.Horita, M.Furukawa, M.Nemoto, N.K.Tsenev, R.Z.Valiev, P.Berbon and T.G.Langdon: "Proceeding of an Al-Mg-Li-Zr Alloy with Ultra-Fine Grain Size" Materials Science Forum. 243-245. 239-244 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Y.Iwahashi, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Structural Evolution and Hall-Petch Relationship in an Al=Mg-Li-Zr Alloy with Ultra-Fine Grain Size" Acta Mater. 45. 4751-4757 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto, R.Z.Valies and T.G.Langdon: "Recrystallization in Ultrafine-Grained Materials with Non-Equilibrium Grain Boundaries" Proc.of Rex'96, the Third Inter.Conf.on Recrystallization and Related Phenomena, ed.by T.R.McNelly. 149-160 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "An Investigation of Microstructural Evolution during Equal-Channel Angular Pressing" Acta Mater.45. 4733-4741 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Y.Ma, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Microstructural Characteristics and Superplastic Ductility in a Zn-22%Al Alloys with Submicrometer Grain Size" Mater.Sci.Eng.A241. 122-128 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Y.Ma, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Fabrication and Properties of a Submicrometer-Grained Zn-22%Al Alloy" Inter.Conf.on Thermomechanical Processing of Steel & Other Materials, THERMEC'97, (T.Chandra and T.Sakai, eds.), The Minerals, Metals & Materials Society. 1875-1881 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Z.Horita, D.J.Smith, M.Furukawa, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Characterization of Ultra-Fine Grained Materials Produced by Torsion Straining" Inter.Conf.on Thermomechanical Proceesing of Steel & Other Materials, THERMEC'97, (T.Chandra and T.Sakai, eds.), The Minerals, Metals & Materials Society. 1937-1943 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "Equal-Channel Angular Pressing for the Processing of Superplastic Materials" Inter.Conf.on Thermomechanical Processing of Steel & Other Materials, THERMEC'97, (T.Chandra and T.Sakai, eds.), The Minerals, Metals & Materials Society. 1945-1951 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, P.B.Berbon, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Age Hardening and the Potential for Superplasticity in a Fine-Grained Al-Mg-Li-Zi Alloy" Metall.Mater.Trans.A. 29 (1). 169-177 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "The Process of Grain Refinement in Equal-Channel Angular Pressing" Acta Mater.46 (9). 3317-3331 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Nakashima, Z.Horita, M.Nemoto and T.G.Langdon: "Influence of Channel Angle on the Development of Ultrafine Grains in Equal-Channel Angular Pressing" Acta Mater.46 (5). 1589-1599 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Z.Horita, D.J.Smith , M.Nemoto, R.Z.Valiev and T.G.Langdon: "Obervations of Grain Boundary Structure in Submicro-meter-Grained Cu and Ni Using High-Resolution Electron Microscopy" J.Mat.Res.13 (2). 446-450 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.B.Berbon, N.K.Tsenev, R.Z,Valiev, M.Furukawa, Horita, M.Nemoto and T.G.Langdon: "Superplasticity in Alloys Processed by Equal-Channel Angular Pressing" Superplasticity and Superplastic Z.Forming 1998, (edited by A.K.Ghosh and T.R.Bieler), The Minerals, Metals & Materials Society. 127-134 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Microstructural Evolution in Pure Aluminum during Equal-Channel Angular Pressing" Modeling the Mechanical Response of Structural Materials, (edited by E.M.Teleff and R.K.Mahidhara), The Minerals, Metals & Materials Society. 165-172 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z,Valiev and T.G.Langdon: "Application of Equal-Channel Angular Pressing for Producing Superplastic Aluminum Alloys" Modeling the Mechanical Response of Structural Materials, (edited by E.M.Teleff and R.K.Mahidhara), The Minerals, Metals & Materials Society. 165-172 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Komura, P.B.Bercon, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "High Strain Rate Superplasticity in an Al-Mg Alloy Containing Scandium" Scripta Mater.38 (12). 1851-1856 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Microstructural Characteristics of Ultrafine-Grained Aluminum Produced Using Equal-Channel Angular Pressing" Metall.Mater.Trans.29A (9). 2245-2252 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.G.Langdon, M.Furukawa, Z.Horita and M.Nemoto: "Using Intense Plastic Straining for High-Strain-Rate Superplasticity" J.Metals. 50 (6). 41-45 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Factors Influencing the Flow and Hardness of Materials with Ultrafine Grain Sizes" Phill.Mag.A. 78 (1). 203-215 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] H.Hasegawa, S.Komura, Z.Horita, M.Furukawa, M.Nemoto and T.G.Langdon: "Grain Refinement and Potential for Superplasticity in Al Alloys Containing Small Particles" Proc.The Third Pacific Rim Inter.Conf.on Advanced Materials and Processing (PRICM3), ed.by M.A.Imam et al., The Minerals, Metals and Materials Society. 1873-1878 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Oh-ishi, Z.Horita, M.Furukawa, M.Nemoto and T.G.Langdon: "Optimizing the Rotation Conditions in Equal-Channel Angular Pressing" Metall.Mater.Trans.29A (7). 2011-2015 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Z.Horita, T.Fujinami, M.Nemoto and T.G.Langdon: "Microstructures and Mechanical Properties of Submicro-meter-Grained Al Alloys Produced by Equal-Channel Angular Pressing" Aluminum Alloys, Vol.1, Proc.ICAA-6. 449-454 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, M.K.Tsenev, E.Z.Valiev and T.G.Langdon: "Processing of Aluminum Alloys for High Strain Rate Superplasticity" Hot Deformation of Aluminum Alloys II,ed.T.R.Bieler et al., The Mineral, Metals and Materials Society. 111-124 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Komura, P.B.Bercon, A.Utsunomiya, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Superplasticity in an Ultrafine-Grained Al-Mg-Sc Alloy Produced by Equal-Channel Angular Pressing" Hot Deformation of Aluminum Alloys II,ed.T.R.Bieler et al., The Mineral, Metals and Materials Society. 125-138 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, H.Kawahara, Z.Horita, M.Nemoto and T.G.Langdon: "Effect of Mg on Grain Size Refinement of Aluminum by Equal-Channel Angular Pressing" Proc.of Inter.Seminar on Microstructure, Micromechanics and Processing of Superplastic Materials, IMSP'97, ed.T.Aizawa et al.45-52 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Optimizing the Processings of a Commercial Al-Based Alloy for High Strain Rate Superplasticity" Proc.of Inter.Seminar on Microstructure, Micromechanics and Processing of Superplastic Materials, IMSP'97, ed.T.Aizawa et al.81-88 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.Berbon, N.K.Tsenev, R.Z.Valiev, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Fabrication of Bulk Ultrafine-Grained Materials through Intense Plastic Straning" Metall.Mater.Trans.29A (9). 2237-2243 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "Factors Influencing the Equilibrium Grain Size in Equal-Channel Angular Pressing : Role of Mg Additions to Aluminum" Metall.Mater.Trans.29A (10). 2503-2510 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] P.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev, and T.G.Langdon: "Requirements for Achieving High-Strain-Rate Superplasticity in Cast Aluminum Alloys" Phil.Mag.Letters.74 (4). 313-318 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Furukawa, Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "The Shearing Characteristics Associated with Equal-Channel Angular Pressing" Mater.Sci.Eng.257A. 328-332 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Komura, A.Utsunomiya, Z.Horita, M.Furukawa, P.B.Berbon, T.G.Langdon, M.Nemoto: "Ultrafine-Grained Structure Produced by Intense Plastic Straining (in Japanese)" The Japan Institute of Metals. 37 (5). 376 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Equal-Channel Angular Pressing (ECAP): "A Novel Method for Microstructural Control (in Japanese)" The Japane Institute of Metals. 37 (9). 9-16 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Iwahashi, Z.Horita, M.Nemoto and T.G.Langdon: "The Procesing of Ultrafine-Grained Materials Using Equal-Channel Angular Pressing" Processig and Fabrication of Advanced Materials VI,ed.K.A.Khor et al., The Institute of Metals. 3-14 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.Komura: "High Strain Rate Supevplastici ty in a Al-Mg Alloy Containing Scandiuni" Scripta Mater.38・12. 1851-1856 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Iwahashi: "Microstructural Characteristics of Ultrafine-Graived Aluminum Produced Using Egual Chanuel Augular Pressing" Metall Mater.Tvans.29A・9. 2245-2252 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Furukawa.: "Factors Influencing the Flow and Havdness of Materials with Ultrafine Grain Sizes" Phil.Mog A. 78・1. 203-215 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Iwahashi: "Factors Influenciug the Eguilibriuni Grain Size in Egual Cliannel Angulae Pressing:Role of Mg Additiens to Aluminum" MeTall.Mater.Trans. 29A・10. 2503-2510 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Furukawa.: "The Shearing Characteristics Associated with Egual-Channel Angular Pressing" Mater.Sci.Eug.257A. 328-332 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 堀田 善治: "新しい組織制御法としてのEgual-Chauuel Angular Pressing(ECAP)" まてりあ(日本金属学会会報). 37・9. 9-16 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Furukawa: "Structural Evolution and the Hall-Petch Relationship in an Al-Mg-Li-Zr Alloy with Ultra-Fine Grain size" Acta Materialia. 45・11. 4751-4757 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Iwahashi: "Anlnvestigation of Microstructural Evolution during Equal-Channel Angular Pressing" Acta Materialia. 45・11. 4733-4741 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Furukawa: "Production of Ultrafine-Grained Metallic Materials Using an Intense Plastic Straining Technique" Materials Science Forum. 233-234. 177-184 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Z.Horita: "Processing of an Al-Mg-Li-Zr Alloy with Ultra-Fine Grain Size" Materials Science Forum. 243・245. 239-244 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Furukawa: "Microstructural Characteristics and Superplastic Ductility in a Zn-22% Al Alloys with Submicrometer Grain Size" Materials Science and Engineering. A241. 122-128 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Nakashima: "Influence of Channel Angle on the Development of Ultratine Grainsin Equal-Channel Angular Pressing" Acta Materialia. (印刷中). (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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