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Observation of Surface Deformation of Ferroelectric and Ferroelastic Crystals by Atomic Force Microscopy

Research Project

Project/Area Number 09640406
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 固体物性Ⅰ(光物性・半導体・誘電体)
Research InstitutionIWAKI MEISEI UNIVERSITY

Principal Investigator

TAKASHIGE Masaaki  IWAKI MEISEI UNIVERSITY,FACULTY OF SCIENCE AND ENGINEERING,DEPARTMENT OF ELECTRONIC ENGINEERING,PROFESSOR, 理工学部, 教授 (70114527)

Co-Investigator(Kenkyū-buntansha) SHIMIZU Fuminao  IWAKI MEISEI UNIVERSITY,FACULTY OF SCIENCE AND ENGINEERING,DEPARTMENT OF ELECTRO, 理工学部, 講師 (20206212)
Project Period (FY) 1997 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,900,000)
Fiscal Year 1998: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1997: ¥3,400,000 (Direct Cost: ¥3,400,000)
Keywordsdomain / ferroelectric / ferroelastic / atomic force microscopy / AFM / barium titanate / lead titanate / tungsten oxide / 相転移
Research Abstract

AFM(Atomic Force Microscopy) is one of the useful methods for visualizing the surface morphology due to the ferroelectric and ferroelastic domain configurations, since the measurement is possible without any modification or damage of the sample surface in contrast to other methods such as surface etching, scanning electron microscopy, etc.
In this project, we made AFM observations about surface structure of the following five crystals, BaTiO_3(BT), PbTiO_3(LT), Gd_2(MoO_4)_3(GMO), NdP_<5p>O_<14>(NDPP) and W0_3, all of which show phase transitions with alteration of the crystal system. Namely, 90 degree domain structure due to the cubic to tetragonal phase transition in BT and LT, the tetragonal to orthorhoinbic domain structure in GMO, and the orthorhombic to monoclinic domain structure in NDPP and W0_3, were visualized at room temperature, respectively. In particular, further experiments such as observation of the 90 degree domain image under application of electric field in BT, temperature-dependent triclinic-domain images in W0_3 were also made.

Report

(3 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] M.Takashige et al.: "Surface morphology of tetragonal PbTiO_3 and BaTiO_3 observed by atomic force microscopy" J.Phys.Soc.Jpn.66. 1848-1849 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al.: "AFM observation of 90°domains of BaTiO_3 under application of electric field" J.Phys.Soc.Jpn.66. 2272-2275 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al.: "Surface merphology of Gd_2(M_0O_4)_3 observed by atomic force microscopy." Ferroelectrics. 203. 221-225 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al.: "AFM observation of 90°domain structure in the crystallized grains from amorphous PbTiO_3" Jpn.J.Appl.Phys.37. 5397-5399 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al.: "Three types of domains in WO_3 observed by atomic force microscopy." J.Phys.Soc.Jpn.67. 2144-2145 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al.: "The surface images of monoclinic domains in NdP_5O_<14> and WO_3 by atomic force microscopy." Ferroclectrics. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al: "Surface Morphology of Tetragonal PbTiO_3 and BaTiO_3 Observed by Atomic Force Micrcroscopy" J.Phys.Soc.Jpn.66. 1848-1849 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al: "AFM Observation of 90゚Domains of BaTiO_3 under Application of Electric Field" J.Phys.Soc.Jpn.66. 2272-2275 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al: "Surface Morphology of Ferroelectric Gd_2 (MoO_4)_3) Observed by Atomic Force Micrcroscopy" Ferroelectrics. 203. 221-225 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al: "Atomic Force Microscope Observation of 90゚Domain Structure in the Crystallized Grains from Amorphous PbTiO_3" Jpn.J.Appl.Phys.37. 5397-5399 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al: "Three types of domains in WO_3 observation by Atomic Force Microscope" J.Phys.Soc.Jpn.67. 2144-2145 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al: "The surface Images of Monoclinic Domains in NdP_5O_<14> and WO_3 by Atomic Force Microscopy" Ferroelctrics. (to be published).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Takashige et al.: "Surface morphology of tetragonal PbTiO_3 and BaTiO_3 obserwed by Atomic foru Microscopy" J.Phys.Soc.Jpn.66. 1848-1849 (1997)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Takashige et al.: "AFM observation of 90° domains of BaTiO_3 under application of elctric bield." J.Phys.Soc.Jpn.66. 2272-2275 (1997)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Takashige et al.: "Surbace morphology of Gd_2(MoO_4)_3 observed by Atomic farce microscopy." Ferroelectrics. 203. 221-225 (1997)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Takashige et al.: "AFM observation of 90° domain structure in the crystalliged grains from amorphous PbTiO_3" Jpn.J.Appl.Phys.37. 5397-5399 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] S.I.Hamagaki et al.: "Three types of domains in WO_3 observed by atomic force microscopy" J.Phys.Soc.Jpn.67. 2144-2145 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] S.I.Hamagaki et al.: "The surface images of monoclinic domains in NdP_5O_<14> and WO_3 by atomic force microscopy" Ferroelectrics. (印刷中).

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Takashige et al.: "Surface Morphology of Tetragonal PbTiO_3 and BaTiO_3 Obserued by Atomic Force Microscopy" J.Phys.Soc.Jpan.66. 1848-1849 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Takashige et al.: "AFM Observation of 90° Domains of BaTiO_3 under Application of Electric Field" J.Phys.Soc.Jpan.66. 2272-2275 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Takashige et al.: "Observation of the Crystallization Process from Amorphous PbTiO_3 and Pb_5Ge_3 O_<11> by Atomic Force Microscopy" Japan.J Appl.Phys.36. 6150-6154 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Takashige et al.: "AFM Obseruation of the Ferroclectric and Farroelastic Crystals." J.Kor.Phys.Soc.(in press).

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2020-05-15  

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