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Development of High-Pressure Precise Magnetization Measurement System and Studies of Magnetic Phase Transitions under High Pressure

Research Project

Project/Area Number 09640434
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 固体物性Ⅱ(磁性・金属・低温)
Research InstitutionOsaka University

Principal Investigator

ISHIZUKA Mamoru  Osaka Univ., Reseach Center for materials Science at Extreme Condictions, Reserch associate, 極限科学研究センター, 助手 (30184542)

Co-Investigator(Kenkyū-buntansha) ENDO Shoichi  Osaka Univ.Research Center for Materials Aciences at Extreme Conditions Professo, 極限科学研究センター, 教授 (10001843)
Project Period (FY) 1997 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥3,100,000 (Direct Cost: ¥3,100,000)
Fiscal Year 1998: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1997: ¥2,600,000 (Direct Cost: ¥2,600,000)
Keywordshigh pressure / SQUIDmagnetometer / magnetization measurement / diamond-anvil cell / vanadium / superconducting transition temperature / 磁気測定
Research Abstract

We have improved the performance of the high-pressure magnetization measurement system consisting of a diamond-anvil cell (DAC) and a SQUID vibrating coil magnetometer in order to increase the pressure range of a high-pressure research in magnetism and superconductivity to more than 100 GPa. Results are as follows. (1) The sensitivity of the system has been increased by a factor of 10 by compensating the magnetic-field signal which previously prevented us from applying larger magnetic field than 3 Oe. (2) Thermal insulation of the actuators for vibration of the SQUID detection coil from the DAC has been improved, resulting in an increase in the temperature of the measurements by a factor of more than two. (3) Using this system we have investigated a pressure-induced magnetic phase transition in CrTe (T_c=330-350 K) and pressure effect on superconducting transition of vanadium at megabar. A magnetic phase transition in CrTe at around 3.5 GPa was first reported by Grazhdankina et al., but their results are controversial because the sample they used was not single phase and the experimental accuracy seems not to be enough for establishing the magnetic state. We have observed a disappearance of the ferromagnetism of CrTe at 6-7 GPa for samples with good quality. The superconducting transition temperature T_c of vanadium increases linearly with pressure up to 50 GPa. Pressure dependence of T_c has been measured up to 112 GPa so as to investigate to what extent such a monotonic increase in T_c would hold. T_c at 112 GPa was found to be more than three times as large as that at ambient pressure and to still increase with pressure. This value of T_c is the largest one observed in single elements.

Report

(3 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • Research Products

    (17 results)

All Other

All Publications (17 results)

  • [Publications] Mamoru Ishizuka: "Pressure-Induced Structural Phase Transition in the Two-Dimensional Heisenberg Ferromagnet KzCuF_4" Phys.Rev.B. 57. 64-67 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 石塚 守: "超高圧下精密磁化測定装置の最近の進展" 大阪大学極限科学研究センター報告書. 2. 48-51 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru Ishizuka: "Magnetization Measurements under High Pressure in a Diamond-Anvil Cell Using a SQUID Vibrating Coil Magnetometer" Rev.High Pressure Sci.Technol.7. 484-486 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru Ishizuka: "Pressure-Induced Magnetic Phase Transition in the Two-Dimensional Heisenberg Ferromagnet KzCuF_4" J.Magn.Magn.Mater.177-181. 725-726 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 石塚 守: "CrTeの高圧下での磁性" 大阪大学極限科学研究センター報告書. 3. (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru Ishizuka: "Measurements of Superconducting Transitions at Pressures up to 83GPa" to be published in Physica B. (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Recent Development of High-Pressure Precise Magnetization Measurement System"" Annual Report of Research Center for Materials Science at Extreme Conditions, Osaka University. No.2. 48-51 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Pressure-Induced Structural Phase Transition in the Two-Dimensional Heisenberg Ferromagnet K_2CuF_4"" Phys.Rev.B57. 64-67 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Magnetization Measurements under High Pressure in a Diamond-Anvil Cell Using a SQUID Vibrating Coil Magnetometer"" Rev.High Pressure Sci.Technol.7. 484-486 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Pressure-Induced Magnetic phase Transition in the Two-Dimensional Heisenberg Ferromagnet K2CuF4"" J.Magn.Magn.Mater. 177-181. 725-726 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Magnetic Behavior of CrTe under High Pressure"" to be published in Annual Report of Research Center for Materials Science at Extreme Conditions, Osaka University. (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru ISHIZUKA: ""Measurements of Supercondcting Transitions at Pressures up to 83 GPa"" to be published in Physica B. (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Mamoru Ishizuka: "Measurements of Superconducting Transitions at Pressures" Physica B. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 石塚 守: "CrTeの高圧下での磁性" 大阪大学極限科学研究センター報告書. Vol3. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Mamoru Ishizuka: "Magnetization Measurements under High Pressure in a Diamond-Anvil Cell Using a SQUID Vibrating Coil Magnetometer" Rev. High Pressure Sci. Technol.Vol.7. 484-486 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Mamoru Ishizuka: "Pressure-induced structural phase transition in the two-dimensional Heisenberg ferromagnet K_2CuF_4" Physical Review B. Vol57,No1. 64-67 (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 石塚守: "超高圧下精密磁化測定装置の最近の進展" 大阪大学極限科学研究センター報告書. Vol.2. (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2020-05-15  

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