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Investigation of Solid State Reaction by Means of Direct Observation of Atomistic Structural Changes

Research Project

Project/Area Number 10305046
Research Category

Grant-in-Aid for Scientific Research (A).

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionHiroshima Institute of Technology

Principal Investigator

KIRITANI Michio  Hiroshima Institute of Technology, School of Engineering, Professor, 工学部, 教授 (70033826)

Co-Investigator(Kenkyū-buntansha) KOMATSU Masao  Hiroshima Inst.of Tech., School of Engineering, Associate Professor, 工学部, 助教授 (80309616)
Project Period (FY) 1998 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥41,800,000 (Direct Cost: ¥41,800,000)
Fiscal Year 2000: ¥4,200,000 (Direct Cost: ¥4,200,000)
Fiscal Year 1999: ¥16,100,000 (Direct Cost: ¥16,100,000)
Fiscal Year 1998: ¥21,500,000 (Direct Cost: ¥21,500,000)
KeywordsLattice Defect / Point Defect / Dislocation / Radiation Damage / Plastic Deformation / High-Speed Deformation / Ductile Fracture / Electron Microscopy / 転位構造 / 無秩序反応
Research Abstract

The most superior method of direct observation of defect reactions is to utilize high energy electron irradiation in a high-voltage electron microscope : (a) A systematic investigation has been performed on the effect of solute addition to defect structure evolution, (b) A method of the identification of the nature of small point defect clusters in neutron irradiated materials was established by superimposing electron irradiation and applied to representative materials, (c) Effect of strain field around dislocation on cascade defects was elucidated, (d) Detection of stochastic fluctuation of point defect reaction processes was successfully made during the growth of electron irradiation-induced dislocation loops, (e) Measurement of short relaxation phenomena was made by newly designed intermittent irradiation technique. As for the defect microstructures induced by high energy neutron irradiation : (f) The role of electron microscopically invisible small defect clusters in iron was eluci … More dated, (g) Relation between the destination of cascade collision induced point defects and the microstructure evolution was studied, (h) Effect of solute elements to the defect microstructure evolution was systematically investigated, (i) The mechanism of defect reaction during neutron irradiation with temperature variation was also studied. Plastic deformation of crystalline metals without dislocation was the most important and new subject in this research project : (j) Absence of the operation of dislocations was confirmed by direct observation of the progress of deformation in an electron microscope, (k) From the dynamic observation of the appearance and disappearance of point defect clusters, point defects are concluded to be introduced as dispersed point defects, but not as point defect clusters, (l) Local strain was successfully measured by the deformation of plastically deformable precipitates, (m) Deformation mode was examined by using samples containing various kinds of secondary defects, (n) all of these experimental results lead to the proposal of a new mechanism of deformation with glide elements which replace dislocations, under the condition of extremely high internal stress. Investigation of high-speed deformation achieved the strain rate of 10^7/s, and (o) Defect structures were found to change drastically by the deformation with strain rate over 10^5/s. Less

Report

(4 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • Research Products

    (67 results)

All Other

All Publications (67 results)

  • [Publications] Y.Kizuka,Y.Satoh,S.Arai,and M.Kiritani: "Identification of the nature of neutron-irradiaton-induced defects in copper by means of electron irradiation"Radiation Effects and Defects in Solids. 145. 143-146 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Kizuka and M.Kiritani: "Defect structure near edge dislocation in neutron-irradiated Cu-0.3at.%Ge"Radiation Effects and Defects in Solids. 143. 333-342 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Defect reaction processes through electron microscopy"Proc.Ixth Chinese-Japanese Electron Microscopy Seminor, Dailian. 35-38 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 荒井重勇,桐谷道雄: "間歇電子照射法の開発とその応用"日本電子顕微鏡学会誌. 34. 144-146 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] R.Oshima,M.Fukuzumi,M.Komatsu and M.Kiritani: "Phase transformation of Fe-Rh alloys induced by high speed deformation"Proc.Int.Conf.On Solid-Solid Phase Transformation, The Japan Institute of Metals. 981-984 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki,S.Arai,Y.Satoh,and M.Kiritani: "Identification of the nature of small point defect clusters in neutron Irradiated Fe-16Ni-15Cr by means of electron irradiation"Journal of Nuclear Materials. 255. 165-173 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani and N.M.Ghoniem: "Damage production and accumulation"Journal of Nuclear Materials. 271&272. 540-552 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki,T.Yoshiie,M.Iseki,and M.Kiritani: "Invisible and visible point defect clusters in neutron irradiated iron"Journal of Nuclear Materials. 271&272. 256-260 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Yoshiie and M.Kiritani: "Destination of point defects and microstructural evolution under collision cascade damage"Journal of Nuclear Materials. 271&272. 296-300 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani et.al: "Anomalous production of vacancy clusters and the possibility of plastic deformation of crystalline metals without dislocations"Philosophical Magazine Letters. 79. 797-807 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Design of experiments on production and reaction of point defects"Radiation Effects and Defects in Solids. 148. 233-269 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh,T.Yoshiie,S.Arai,and M.Kiritani: "Defect structure development in electron irradiated Cu-Pd and Cu-Pt alloys with HVEM"J.Electron Microscopy. 48. 393-398 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Similarity and difference between fcc, bcc and hcp metals from the viewpoint of point defect cluster formation"Journal of Nuclear Materials. 276. 41-49 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] K.Arakawa,Y.Satoh,S.Arai and M.Kiritani: "Fluctuation of point defect reaction observed during the growth of dislocation loops under electron irradiaton"Philosophical Magazine. A80. 2041-2055 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh,T.Yoshiie,I.Ishida and M.Kiritani: "Defect structure development in electron-irradiated Cu-based Si, Ge and Sn binary alloys"Philosophical Magazine. A80. 2567-2590 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Yoshiie,Q.Xu,Y.Satoh,H.Ohkubo and M.Kiritani: "The effect of alloying elements on the defect structural evolution in neutron irradiated Ni alloys"Journal of Nuclear Materials. 283-287. 229-233 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki,T.Yoshiie,Q.Xu,M.Iseki and M.Kiritani: "Defect structure introduced in iron under varying temperature neutron irradiation"Journal of Nuclear Materials. 283-287. 282-285 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani,K.Yasunaga,Y.Matsukawa and M.Komatsu: "Plastic deformation of metal thin films without dislocation and anomalous production of point defects"Radiation Effects and Defects in Solids. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh,T.Yoshiie,H.Mori and M.kiritani: "Local strain in thin-foil deformation using deformation of Pb precipitates in Al matrix"Radiation Effects and Defects in Solids. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] K.Arakawa,K.Ono,M.Iseki and M.Kiritani: "Elongation fracture of metals containing pre-introduced secondary defects"Radiation Effects and Defects in Solids. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Kizuka, Y.Satoh, S.Arai, and M.Kiritani: "Identification of the nature of neutron-irradiaton-induced defects in copper by means of electron irradiation"Radiation Effects and Defects in Solids. 145. 143-146 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Kizuka and M.Kiritani: "Defect structure near edge dislocation in neutron-irradiated Cu-0.3at.%GE"Radiation Effects and Defects in Solids. 143. 333-342 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Defect reaction processes through electron microscopy"Proc.IXth Chinese-Jap.Electron Microscopy Seminor, Dailian. 35-38 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] R.Oshima, M.Fukuzumi, M.Komatsu and M.Kiritani: "Phase transformation of Fe-Rh alloys induced by high speed deformation"Proc.Int.Conf.on Solid-Solid Phase Transformation, The Japan Institute of Metals. 981-984 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki, S.Arai, Y.Satoh, and M.Kiritani: "Identification of the nature of small point defect clusters in neutron Irradiated Fe-16Ni-15Cr by means of electron irradiation"Journal of Nuclear Materials. 255. 165-173 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani and N.M.Ghoniem: "Damage production and accumulation"Journal of Nuclear Materials. 271&272. 540-552 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki, T.Yoshiie, M.Iseki, and M.Kiritani: "Invisible and visible point defect clusters in neutron irradiated iron"Journal of Nuclear Materials. 271&272. 256-260 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Yoshiie and M.Kiritani: "Destination of point defects and microstructural evolution under collision cascade damage"Journal of Nuclear Materials. 271&272. 296-300 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani et.al.: "Anomalous production of vacancy clusters and the possibility of plastic deformation of crystalline metals without dislocations"Philosophical Magazine Letters. 79. 797-807 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Design of experiments on production and reaction of point defects"Radiation Effect and Defects in Solids. 148. 233-269 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh, T.Yoshiie, S.Arai, and M.Kiritani: "Defect structure development in electron irradiated Cu-Pd and Cu-Pt alloys with HVEM"J.Electron Microscopy. 48. 393-398 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Similarity and difference between fcc, bcc and hcp metals from the viewpoint of point defect cluster formation"Journal of Nuclear Materials. 276. 41-49 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] K.Arakawa, Y.Satoh, S.Arai and M.Kiritani: "Fluctuation of point defect reaction observed during the growth of dislocation loops under electron irradiaton"Philosophical Magazine. A80. 2041-2055 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh, T.Yoshiie, I.shida and M.Kiritani: "Defect structure development in electron-irradiated Cu-based Si, Ge and Sn binary alloys"Philosophical Magazine. A80. 2567-2590 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Yoshiie, Q.Xu, Y.Satoh, H.Ohkubo and M.Kiritani: "The effect of alloying elements on the defect structural evolution in neutron irradiated Ni alloys"Journal of Nuclear Materials. 283-287. 229-233 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Horiki, T.Yoshiie, Q.Xu, M.Iseki and M.Kiritani: "Defect structures introduced in iron under varying temperature neutron irradiation"Journal of Nuclear Materials. 283-287. 282-285 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani, K.Yasunaga, Y.Matsukawa and M.Komatsu: "Plastic deformation of metal thin films without dislocation and anomalous production of point defects"Radiation Effects and Defects in Solids. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Y.Satoh, T.Yoshiie, H.Mori and M.Kiritani: "Local strain in thin-foil deformation using deformation of Pb precipitates in Al matrix"Radiation Effects and Defects in Solids. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] K.Arakawa, K.Ono, M.Iseki and M.Kiritani: "Elongation fracture of metals containing pre-introduced secondary defects"Radiation Effects and Defects in Solids. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Kiritani: "Similarity and difference between fcc, bcc and hcp metals from the viewpoint of point defect cluster formation"Journal of Nuclear Materials. Vol.276. 41-49 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Arakawa,Y.Satoh,S.Arai and M.Kiritani: "Fluctuation of point defect reactions observed during the growth of dislocation loops under electron irradiation"Philosophical Magazine. Vol.A80. 2041-2055 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Y.Satoh,T.Yoshiie,I.Ishida and M.Kiritani: "Defect structure development in elecltron-irradiated Cu-based Si,Ge and Sn binary alloys"Philosophical Magazine. Vol.A80. 2567-2590 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Yoshiie,Q.Xu,Y.Satoh,H.Ohkubo and M.Kiritani: "The effect of alloying elements on the defect structural evolution in neutron irradiated Ni alloys"Journal of Nuclear Materials. Vol.283-287. 229-233 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Horiki,T.Yoshiie,Q.Xu,M.Iseki and M.Kiritani: "Defect structures introduced in iron under varying temperature neutron irradiation"Journal of Nuclear Materials. Vol.283-287. 282-285 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Kiritani,K.Yasunaga,Y.Matsukawa and M.Komatsu: "Plastic deformation of metal thin films without dislocation and anomalous production of point defects"Radiation Effects and defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Kiritani,T.Tawara,H.Arimura,and M.Komatsu: "Defect structures introduced in nickel and copper by impact compression"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Arakawa,K.Ono,M.Iseki and M.Kiritani: "Elongation fracture of metals containing pre-introduced secondary defects"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] N.Yoneyama,S.Kumai,A.Sato,M.Komatsu and M.Kiritani: "Microstructures in Fe based shape memory alloy and Al based dual phase crystals after high speed deformation"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] A.Okada,Y.Asao and M.Kiritani: "Application of a rail gun to the ultra-high speed plastic deformation experiment"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Komatsu and M.Kiritani: "Design of high-speed impact deformation experiments and evaluation of stress and strain rate"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Sota,K.Yasunaga,M.Komatsu and M.Kiritani: "High-speed impact compression induced defect structures in aluminum"Radiation Effects and Defects in Solids. (発表予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Kiritani and N.M.Ghoniem: "Damage production and accumulation"Journal of Nuclear Materials. Vol.271&272. 540-552 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M.Horiki,T.Yoshiie,M.Iseki and M.Kiritani: "Invisible and visible point defect clusters in neutron irradiated iron"Journal of Nuclear Materials. Vol.271&272. 256-260 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] T.Yoshiie and M.Kiritani: "Destination of point defects and microstructural evolution under collision cascade damage"Journal of Nuclear Materials. Vol.271&272. 296-300 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M.Kiritani,Y.Satoh,Y.Kizuka,K.Arakawa,Y.Ogasawara,et.al.: "Anomalous production of vacancy clusters and the possibility of plastic deformation of crystalline metals without dislocations"Philosophical Magazine Letters. Vol.79. 797-804 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M.Kiritani: "Design of experiments on production and reaction of point defects"Radiation Effects and Defects in Solids. Vol.148. 233-267 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Satoh,T.Yoshiie,S.Arai and M.Kiritani: "Defect structure development in electron irradiated Cu-Pd and Cu-Pt alloys with HVEM"Journal of Electronmicroscopy. Vol.48. 393-398 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 荒井重雄 桐谷道雄: "間歇電子照射法の開発とその応用"電子顕微鏡. Vol.34. 144-146 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M.Kiritani: "Similarity and difference between fcc,bcc and hcp metals from the viewpoint of point defect cluster formation"Journal of Nuclear Materials. Vol.276. 41-49 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Kizuka and M.Kiritani: "Defect structure near edge dislocation in neutron-irradiated Cu-0.3at.%Ge" Radiation Effects and Defects in Solids. Vol.143. 333-343 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Horiki.S.Arai and M.Kiritani: "Identification of the nature of small point defect clusters in neutron irradiated Fe-16Ni-15Cr by means of electron irradiation" Journal of Nuclear Materials. Vol.255. 165-173 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Kizuka,Y.Satoh,S.Arai and M.Kiritani: "Identification of the nature of neutron-irradiation-induced defects in copper by means of electron irradiation" Radiation Effects and Defects in Solids. Vol.145. 237-251 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Kiritani and N.M.Ghoniem: "Damage production and accumulation" Journal of Nuclear Materials. (in press). 13 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Kiritani: "Design and experiments on production and reaction of point defects" Radiation Effects and Defects in Solids. (in press). 35 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 小松正雄、森博太郎: "超高圧電子顕微鏡用高温雰囲気試料筒の開発とその応用" 電子顕微鏡. Vol.33. 5-6 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] M.Komatsu,T.Adachi,K.Yoshida and H.Mori: "In situ observation of growth process of CuO whiskers by environmental HVEM" Proc.International Conference on Electron Microscopy,Mexico. Vol.1. 281-282 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] H.Mori,M.Komatsu,H.Okabayashi and D.E.Grosjean: "Study of electromigration in Al interconnects for LSI by electron microscopy" Proc.Internatinal Conference on Electron Microscopy,Mexico. Vol.1. 283-284 (1998)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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