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Creation of Low defect and Super High Strength Ceramics by High-Speed Centrifugal Compaction Process

Research Project

Project/Area Number 10355030
Research Category

Grant-in-Aid for Scientific Research (A).

Allocation TypeSingle-year Grants
Section展開研究
Research Field Material processing/treatments
Research InstitutionHiroshima University

Principal Investigator

KUROKI Hidenori  Faculty of Engineering, Hiroshima University, Professor, 工学部, 教授 (80037853)

Co-Investigator(Kenkyū-buntansha) SUZUKI Hiroyuki  Faculty of Engineering, Hiroshima University, Research Associate, 工学部, 助手 (90284158)
SASAKI Gen  Faculty of Engineering, Hiroshima University, Associate Professor, 工学部, 助教授 (30192595)
SHINOZAKI Kenji  Faculty of Engineering, Hiroshima University, Associate Professor, 工学部, 助教授 (70154218)
FUKAYA Yasuhiro  Kinki University Faculty of Engineering, Professor, 工学部, 教授 (40268454)
TASHIMA Shunzo  Faculty of Education, Hiroshima University, Associate Professor, 教育学部, 助教授 (40136130)
Project Period (FY) 1998 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥30,200,000 (Direct Cost: ¥30,200,000)
Fiscal Year 2000: ¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 1999: ¥4,800,000 (Direct Cost: ¥4,800,000)
Fiscal Year 1998: ¥23,700,000 (Direct Cost: ¥23,700,000)
Keywordsalumina / WC / low-defect / defect removing function / compactability / compacting velocity / highstrength / 着肉速度 / 沈降 / 高遠心力
Research Abstract

The contents of the present research is divided into three sections. Firstly, the compacting mechanism of High-Speed Centrifugal Compaction Process (HCP) is investigated. Then, the HCP alumina are made under a variety of compacting condition, and the effect of the condition on the properties of sintered alumina is clarified. And finally, the WC sintered material is made by HCP.
The results are as follows :
(1) Since the compacting mechanism of HCP is entirely different from that of pressure casting, HCP possesses much higher compacting velocity than pressure casting. The compacting velocity of HCP increases in proportion to the square of rotational speed, but it does not affected by the initial concentration of slip. Therefore, the efficiency of the production can be improved using a easy-to-prepare dilute slip and higher rotational speed. The compacting velocity of HCP can be estimated quantitatively applying Kynch's theory.
(2) The packing density of HCP green compact increases as rolational speed increases. In addition, the defects within the slip are removed more effectively at higher rotational speed. Thus, a dense and low defect green compact can be obtained with higher rotational speed.
(3) The high strength of HCP alumina is due to the fine and low-defect sintered microstructure. The HCP alumina possesses one of the most low-defect microstructure among ever fabricated or commercially available aluminas.
(4) The above mentioned characteristics are also effective for the compaction of WC fine powder. By dispersing the WC powder in heptane, a dense green compact is obtained within a short time. This green compact can be sintered to almost 100% in relative density without adding cobalt, and it shows high hardness of Hv 2300.

Report

(4 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • Research Products

    (23 results)

All Other

All Publications (23 results)

  • [Publications] 鈴木裕之: "高速遠心成形法の成形機構(第一報)-成形途中における泥漿の観察-"日本セラミックス協会学術論文誌. 109巻. 137-142 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 鈴木裕之: "高速遠心成形法の成形機構(第二報)-粒子の沈降速度および着肉速度の定量的な検討-"日本セラミックス協会学術論文誌. 109巻. 248-253 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki: "Effect of Slip Condition on Compacting Kinetics of High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. 625-628 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki: "Effect of High Centrifugal Force on the Properties of Green Compacts Made by High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. 582-585 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 鈴木裕之: "高速遠心成形アルミナの焼結挙動と機械的性質におよぼす粒末特性の影響"粉体および粉末冶金. 47巻. 866-873 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 鈴木裕之: "高速遠心成形法と加圧鋳込み法によるアルミナ成形体の浸液透光法観察"粉体および粉末冶金. 47巻. 874-881 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Compacting Mechanism in High-Speed Centrifugal Compaction Process (Part 1)-Observation of Slips during Compaction-"J.Ceram.Soc.Japan. vol.109 [2]. 137-142 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Compacting Mechanism in High-Speed Centrifugal Compaction Process (Part 2)-Quantitative Analysis of Falling Velocity of Particles and Compacting Velocity-"J.Ceram.Soc.Japan. vol.109 [3]. 248-253 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Effect of Slip Condition on Compacting Kinetics of High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. 625-628 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Effect of High Centrifugal Force on the Properties of Green Compacts Made by High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. 582-585 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Effect of Powder Characteristics on Sintering Behavior and Mechanical Properties of Alumina Compacted by High-Speed Centrifugal Compaction process"J.Japan Soc.Powder and Powder Metal.. vol.47 [8]. 866-873 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Y.Suzuki, et al.: "Observation of Alumina Green Compacts Made by High-Speed Centrifugal Compaction Process and Pressure Casting Using Liquid Immersion Technique"J.Japan Soc.Powder and Powder Metal.. vol.47 [8]. 874-881 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 鈴木裕之: "高速遠心成形法の成形機構(第一報)-成形途中における泥漿の観察-"日本セラミックス協会学術論文誌. 109巻. 137-142 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形法の成形機構(第二報)-粒子の沈降速度および着肉速度の定量的な検討-"日本セラミックス協会学術論文誌. 109巻. (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Y.Suzuki: "Effect of Slip Condition on Compacting Kinetics of High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Y.Suzuki: "Effect of High Centrifugal Force on the Properties of Green Compacts Made by High-Speed Centrifugal Compaction Process"Proceeding of 2000 Powder Metallurgy World Congress. (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形アルミナの焼結挙動と機械的性質におよぼす粉末特性の影響"粉体および粉末冶金. 47巻. 866-873 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形法と加圧鋳込み法によるアルミナ成形体の浸液透光法観察"粉体および粉末冶金. 47巻. 874-881 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形法による高純度アルミナの焼結中における気孔組織の変化"粉体および粉末冶金. 45巻. 473-479 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形法による高純度アルミナの焼結中における気孔組織の変化の定量的解析"粉体および粉末冶金. 45巻. 1122-1129 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] 鈴木裕之: "高速遠心成形法による高純度アルミナの焼結中の機械的特性の組織依存性"粉体および粉末冶金. 46巻. 331-338 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] H,Y.Suzuki: "Sintered Microstructure and Mechanical Properties of High Purity Alunina Ceramics Made by High-Speed Centrifugal Compaction Process"Key Engineering Materials. 159-160. 187-192 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] H,Y.Suzuki: "Green Compact Defect Removal by High-Speed Centrifugal Compacting"Sintering Technologies 1999,edited by R.M.German,G.L.Messing,and R.G.Cornwall,Plenum Press,New York. (in press).

    • Related Report
      1999 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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