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Development of curved crystal spectrometer for soft X-ray emission spectroscopy

Research Project

Project/Area Number 10554012
Research Category

Grant-in-Aid for Scientific Research (B).

Allocation TypeSingle-year Grants
Section展開研究
Research Field 固体物性Ⅰ(光物性・半導体・誘電体)
Research InstitutionUtsunomiya University

Principal Investigator

NAKAI Shun-ichi  Faculty of Engineering, Utsunomiya University Professor, 工学部, 教授 (70081429)

Co-Investigator(Kenkyū-buntansha) SAITOH Keiichi  Toshiba Co.Ltd.Division of electronic devices, researcher, 電子デバイス事業部, 主務(研究職)
KASHIWAKURA Takayuki  Faculty of Engineering, Utsunomiya University Assistant, 工学部, 助手 (90261817)
斎藤 啓一  株式会社 東芝, 電子デバイス事業部, 主務
Project Period (FY) 1998 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥15,400,000 (Direct Cost: ¥15,400,000)
Fiscal Year 2000: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1999: ¥2,500,000 (Direct Cost: ¥2,500,000)
Fiscal Year 1998: ¥12,000,000 (Direct Cost: ¥12,000,000)
KeywordsSoft X-ray Spectrometer / X-ray Crystal Spectrometer / Position Sensitive Detector / Soft X-ray Monochrometor / Soft X-ray Spectroscopy / 軟X線分光法
Research Abstract

Soft X-ray resonant emission spectroscopy is one of powerful methods to study the information about the electronic structure of solids. The synchrotron radiation is selected by the double crystal monochrometor. The secondary X-ray emission spectra(fluorescence spectra)from sample are analyzed by the secondary monochrometor. However, the intensity of the secondary radiation is generally weak, then we developed the new high resolution, high efficiency spectrometer. In order to achieve high efficiency, we developed the bent crystal spectrometer equipped with the position sensitive detector.
We designed the new soft X-ray spectrometer. The spectrometer is the bent crystal vacuum spectrometer of Johann type, in which a bent crystal of radius of curvature 100cm is mounted. The analyzing crystal with its atomic planes parallel to the face is placed tangent to a circle corresponding to the Rowland circle. The position sensitive detector is placed tangent to this circle.
The test measurement of this spectrometer was performed by using Si K_α emission spectra from Silicon target. In this case, the electron beam(3KV, 80μA)from electron gun was used for excitation source. The resolution of the spectrometer was estimated about 0.5 eV for Si K_α region. Three type detectors, microchannel plate, resistive anode gas proportional counter and backgammon type position sensitive detector have been tested.

Report

(4 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • Research Products

    (10 results)

All Other

All Publications (10 results)

  • [Publications] S.Nakai, et al.: "Resonant emission spectra of YF_3, YCL_3, Y_2O_2 and Y-metal in the YL_<III> absorption region"Phys.Rev.B. B61・11. 7433-7439 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Kashiwakura, et al: "Electronic Structures of CeNi_2Al_5 and CeNiAl_4 Studied by Photoelectron Spectroscopy"J.Phys.Soc.Jpn.. 69・9. 3095-3099 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Nakai, et al: "Comparison between resonant L_α emission spectra and resonant LMM Auger spectra of Yttrium compounds"J.Synchrotron Rad.. 8・2. 401-403 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Nakai, et al.: "Resonant emission spectra of YF_3, YCl_3, Y_2O_2 and Y-metal in the Yl_<III> absorption region"Phys.Rev.B. B61・11. 7433-7439 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Kasiwakura, et al.: "Electronic Structures of CeNi_2Al_5 and CeNiAl_4 Studied by Photoelectron Spectroscopy"J.Phys.Soc.Jpn.. 69・9. 3095-3099 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Nakai, et al.: "Comparison between resonant L_α emission spectra and resonant LMM Auger spectra of Yttrium compounds"J.Synchrotron Rad.. 8・2. 401-403 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Nakai, et al.: "Resonant emission spectra of YF_3, YCl_3, Y_2O_2 and Y-metal in the Yl_<III> absorption region"Phys.Rev.B. B61・11. 7433-7439 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Kashiwakura, et al: "Electronic Structures of CeNi_2Al_5 and CeNiAl_4 Studied by Photoelectron Spectroscopy"J.Phys.Soc.Jpn.. 69・9. 3095-3099 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Nakai, et al: "Comparison between resonant L_α emission spectra and resonant LMM Auger spectra of Yttrium compounds"J.Synchrotron Rad.. 8・2. 401-403 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Nakai, Y.Megawa, F.Terasaki, Chen Gang, T. Ohuchi, K. Obara, T.Kojima, H.Arai T.Kashiwakura and Y.Kitajima: "Resonant emission spectra of YF_3,Ycl_3,Y_2O_3 and Y-metal in Y Lm absorption region"Phys. Rev. B. 2000年3月15日号. (2000)

    • Related Report
      1999 Annual Research Report

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Published: 1998-04-01   Modified: 2020-05-15  

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