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STUDY OF TWO-DEMENSIONAL HYDROGEN ANALYSISUSING NANOFOCUSED ELECTRON BEAM

Research Project

Project/Area Number 10555010
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field 表面界面物性
Research InstitutionTOYOTA TECHNOLOGICAL INSTITUTE

Principal Investigator

UEDA Kazuyuki  TOYOTA TECHNOLOGICAL INSTITUTE, GRADUATE COURSE, PROFESSOR, 大学院・工学研究科, 教授 (60029212)

Co-Investigator(Kenkyū-buntansha) OGAI(KIMURA)  TOYOTA TECHNOLOGICAL INSTITUTE, POST DOCTORAL FELLOW, 大学院・工学研究科, PD研究員 (60262862)
YOSHIMURA Masamichi  TOYOTA TECHNOLOGICAL INSTITUTE, ASSOCIATE , PROFESSOR, 大学院・工学研究科, 助教授 (40220743)
小野 泉  豊田工業大学, 大学院・工学研究科, PD (70288562)
石川 憲一  豊田工業大学, 大学院・工学研究科, PD (90288556)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥11,100,000 (Direct Cost: ¥11,100,000)
Fiscal Year 1999: ¥5,600,000 (Direct Cost: ¥5,600,000)
Fiscal Year 1998: ¥5,500,000 (Direct Cost: ¥5,500,000)
KeywordsHYDROGEN / TOF-FSD / ELECTRON-STIMULATED DESORPTION / TWO-DIMENSIONAL DISTRIBUTION / IMAGING / PROTIUM / 電子励起脱離 / TOF / ESD / 水素検知 / 電子励起 / イオン脱離 / 飛行時間 / 走査型 / シリコン / 水素終端
Research Abstract

This project has been started in order to improve the spatial resolution of a scanning electron-stimulated desorption ion microscope (SESDIM) and to accomplish a quantitative analysis of surface hydrogen, We have achieved the spatial resolution with smaller than 0.7 μm using PbO pipes of 12μm in diameter. The SESDIM is also useful to detect oxygen and imageing of oxygen ion is better resolution than proton image. A practical application to the hydrogen storage alloys (V,Ti,Ni system) shows that hydrogen exist on the matrix surface of V and oxygen localizes at the grain boundary of Ti- and Ni-oxides, A quantitative analysis has not yet been established because delay of an experiment of the low-energy ion scattering apparatus.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (49 results)

All Other

All Publications (49 results)

  • [Publications] K. Ojima and K. Ueda: "Oxygen adsorption induced hydrogen segragation on zirconium surface"Appl. Surface Sci.. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K. Ogai, K. Ishikawa and M. Yoshimura: "Two-dimensional Hydrogen Analysis of Hydrogen Storage Alloy Surface by Electron-Stimulated Desorption Microscopy"Jpn. J. Appl. Phys.. 39. L315-L317 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K. Ueda, K.Ogai, K.Ishikawa and M.Yoshimura: "Two-dimensional hydrogen analysis on solid surface by TOF-EDS"Jpn. J. Appl. Phys.. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K. Ueda, K.Ishikawa K.Ogai and M.Yoshimura: "Two-dimensional analysis of hydrogen on solid surface by electron stimulated desorption microscopy"Applied Surface Science.. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kazuyuki Ueda: "Imaging of hydrogen on solid surfaces by desorption spectroscopy (Invited)"J. of Cristal Growth.. 210. 416-420 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K. Ishikawa and M.Yoshimura: "Two-dimensional hydrogen distribution on solid surface studied by electron stimulated desorption microscopy,(Invited)"Applied Surface Science,. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Yoshimura, T.An, I..Ono and K.Ueda: "Ni-induced surface reconstructions on Si(110) studied by scanning tunneling microscopy"Surface Science,. 433-435. 470-474 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 上田一之: "電子励起脱離法による表面上の水素と酸素の挙動"触媒. 41・7. 537-541 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 上田一之: "電子励起イオン脱離法による水素分析"真空. 42・10. 892-896 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K.Ishikawa and M.Yoshimura: "A New System of Two-Dimensional Hydrogen Analysis and Application to Metal Surfaces"J. Alloys and Comp. 293-295. 361-363 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ishikawa, K.Ueda and M.Yoshimura: "New development of scanning-type microscope for two-dimensional hydrogen distribution using electron-stimulated desorption method"Surface Science. 433-435. 244-248 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, T.Ushirosako, M.Yoshimura: "Surfactant effect of atomic hydrogen on silicide-formation of nickel on Si(110) surfaces"Thin Solid Film. 343-344. 612-615 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] I.Ono, M.Yoshimura and K.Ueda: "Atomistic study of nickel silicide structures on Si(100) by tunneling microscopy"J.Vac.Sci. &Tech. B. 16・6. 2947-2951 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Yoshimura, T.An, I.Ono and K.Ueda: "Nickel-induced surface reconstructions on Si(110) studied by scanning tunneling microscopy"Surface Science. 433-435. 470-474 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 上田一之、石川憲一、吉村雅満、境 悠治: "走査型水素検出顕微鏡の開発とその応用"真空. 42・3. 353-356 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 上田一之: "実験物理学講座"表面物性測定" 小間 篤責任編集 第7章"吸着 ・ 脱離""丸善(印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ued, K.Ishikawa, K.Ohgai, M.Yoshimura: "Tow-dimensional analysis of hydrogen on solid surfaces by electron stimulated desorption microscopy"Applied Surface Science. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K.Ishikawa, K.Ogai and M. Yoshimura: "Two-dimensional hydrogen analysis on solid surfaces by Time of flight-electron-stimulated desorption microscopy"Jpn.J.Appli.Phys. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kaoru Ojima and Kazuyuki Ueda: "Oxygen adsorption induced hydrogen segregation on a zirconjum surface"Applied Surface Science. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kaoru Ojima and Kazuyuki Ueda: "Influence of sulfur on oxygen adsorption onto a zirconium surface"Applied Surface Science. (in Press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K.Ishikawa and M.Yoshimura: "Two dimensional hydrogen distribution on solid surfaces studied by electron-stimulated desorption microscopy and Ni-silicide on H-terminated Si(100) surfaces""Appl.Surf.Sci.. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K.Ishikawa, K.Ogai, M.Yoshimura: "Two -dimensional hydrogen analysis of hydrogen storage alloy surface by electron-stimulated desorption microscopy"Jpn.J.Appl.Phys.. 39. 315-317 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda: "Imaging of hydrogen on solid surfaces by desorption spectroscopy""J.Crystal Growth. 210. 416-420 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, K.Ishikawa and M.Yoshimura: "A new method for two-dementional hydrogen analysis and its"J.Alloys and Compound. 293-295. 361-363 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ishikawa, K.Uda and M.Yoshimura: "New development of scanning type microscope for two-dimensional hydrogen distribution using electron-stimulated desorption method"Surf. Sci.. 433-435. 244-248 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ueda, T.Ushirosako and M.Yoshimura: "Surfactant effect of atomic hydrogen on silicide-formation of nickel on Si(119)""Thin Solid Films. 343-344. 612-615 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kazuyuki Ueda, Ke(ichi Ishikawa, Masamichi Yoshimura: "New development of high-resolution scanning ESD system for two-dimensional images of hydrogen and its application"Appl.Surf.Sci.. 130-132. 815-821 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K. Ojima and K. Ueda: "Oxygen adsorption induced hydrogen segragation on zirconium surface."Appl. Surface Sci.. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, K. Ogai, K. Ishikawa and M. Yoshimura: "Two-dimensional Hydrogen Analysis of Hydrogen Storage Alloy Surface by Electron-Stimulated Desorption Microscopy."Jpn. J. Appl. Phys.. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, K. Ogai, K. Ishikawa and M. Yoshimura: "Two-dimensional hydrogen analysis on solid surfaces by TOF-ESD."Jpn. J. Appl. Phys.. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, K. Ishikawa K. Ogai and M. Yoshimura: "Two-dimensional analysis of hydrogen on solid surfaces by electoron stimulated desorption microscopy."Applied Surface Science.. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] Kazuyuki Ueda: "Imaging of hydrogen on solid surfaces by desorption spectroscopy(Invited)"J. of Crystal Growth. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, K. Ishikawa and M. Yoshimura: "Two-dimensional hydrogen distribution on solid surface studied by electron stimulated desorption microscopy,(Invited)"Applied Surface Science,. (in press).

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, K. Ishikawa and M. Yoshimura: "A New System of Two-Dimensonal Hydrogen Analysis and Application to Metal Surfaces,"J. Alloys and Comp. 293-295. 361-363 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ishikawa, K. Ueda, M. Yoshimura: "New development of scanning-type microscope for two-dimensional hydrogen distribution using electron-stimulated desorption method."Surface Science. 433-435. 244-248 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] K. Ueda, T. Ushirosako, M. Yoshimura: "Surfactant effect of atomic hydrogen on silicide-formation of nickel on Si(110) surfaces."Thin Solid Film. 343-344. 612-615 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] I. Ono, M. Yoshimura and K. Ueda: "Atomistic study of nickel silicide structures on Si(100) by tunneling microscopy."J. Vac. Sci. &Tech. B. 16・6. 2947-2951 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] M. Yoshimura, T. An, I. Ono and K. Ueda: "Nickel-induced surface reconstructions on Si(110) studied by scanning tunneling microscopy."Surface Science. 433-435. 470-474 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 上田 一之,石川 憲一,吉村 雅満,境 悠治: "走査型水素検出顕微鏡の開発とその応用"真空. 42・3. 353-356 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M. Yoshimura, T. An, I. Ono and K. Ueda: "Ni-induced surface reconstructions on Si(110) studied by scanning tunneling microscopy,"Surface Science,. 433-435. 470-474 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 上田 一之: "電子励起脱離法による表面上の水素と酸素の挙動"触媒. 41・7. 537-541 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 上田 一之: "電子励起イオン脱離法による水素分析"真空. 42・10. 892-896 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 上田 一之: "実験物理学講座"表面物性測定" 小間 篤責任編集 第7章"吸着・脱離""丸善(印刷中).

    • Related Report
      1999 Annual Research Report
  • [Publications] K.Ishikawa, M.Yoshimura K.Ueda: "New development of scanning type microscope for two-dimensional hydrogen distribution using electron-stimulated desorption method" Surface Science. in press.

    • Related Report
      1998 Annual Research Report
  • [Publications] K.Ueda, K.Ishikawa M.Yoshimura: "A new system of two-dimensional hydrogen analysis and application to metal surfaces" J.Alloys and Compounds. in press.

    • Related Report
      1998 Annual Research Report
  • [Publications] K.Ueda, K.Ushirosako M.Yoshimura: "Surfactant effect of Atomic hydrogen on silicide-formation of nickel on Si(110)" Thin Solid Films. 341. 1-4 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 上田一之: "電子励起イオン脱離法による走査型水素検出顕微鏡" 応用物理. 67,12. 1414-1417 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] K.Ueda, K.Ishikawa M.Yoshimura, Y.Sakai: "Two-dimensional hydrogen analysis system and Application" Proceedings of 4th Special Symposium on Advanced Material. 191-194

    • Related Report
      1998 Annual Research Report
  • [Publications] K.Ueda, K.Ishikawa M.Yoshimura: "A new development of scanning hydrogen imaging system and its application" Material Research Symposium Proceedings. 513. 17-22 (1988)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-11-11  

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