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Development of Soft-X-Ray Emission Microscopy

Research Project

Project/Area Number 10555012
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Applied optics/Quantum optical engineering
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

YANAGIHARA Mihiro  Res. Inst. for Sci. Meas., Tohoku University, Assoc. Prof, 科学計測研究所, 助教授 (40174552)

Co-Investigator(Kenkyū-buntansha) EJIMA Takeo  Res. Inst. for Sci. Meas., Tohoku University, Res. Assoc., 科学計測研究所, 助手 (80261478)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥13,000,000 (Direct Cost: ¥13,000,000)
Fiscal Year 1999: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 1998: ¥11,900,000 (Direct Cost: ¥11,900,000)
Keywordsmicroscopy / soft X-ray emission / Schwarzschild mirror / multilayer / normal incidence / imaging
Research Abstract

Soft-X-ray emission microscopy is a novel tool to obtain a magnified image of a small spot of a sample by imaging soft X-ray emission from the atoms under irradiation of soft X-rays or electrons using a multilayer-coated Schwarzschild objective. It provides an image very sensitive to the kind of atoms because the soft X-ray emission is selectively reflected by the narrow band pass of the multilayer. The aim of this research is to develop a soft X-ray emission microscopy of a 0.5-μm resolution and to demonstrate its basic advantages.
I constructed a soft-X-ray emission microscope with a Schwarzschild objective of 50 x magnification coated with a Mo/Si multilayer. Using it, I observed a test sample under electron beam irradiation and obtained a distribution image of Si atoms. The result demonstrates the primary advantage of the microscope that the Si L emission is selectively reflected by the Mo/Si multilayer.
A multilayer objective reflects visible light as well as soft X-rays. Thus I carried out an imaging test for the microscope by observing a test sample with visible light and obtained a spatial resolution of 0.7μm. The resolution is very close to the diffraction limit of visible light. This result shows that the microscope has been successfully adjusted with high precision. Because the diffraction limit of soft X-rays is smaller than that of visible light, it was expected to achieve 0.5μm in the resolution. However, a resolution from 1.5μm to 2.0 μm was finally obtained. The most probable reason for the resolution under 0.7μm was the low resolution of the soft X-ray detector employed in this study. To overcome the disadvantage, I should employ a Schwarzschild objective of high magnification and/or X-ray film of high resolution. The usefulness of this microscopy will be demonstrated from now on by observing biological samples and mineral samples.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (25 results)

All Other

All Publications (25 results)

  • [Publications] M.Toyoda: "A Soft-X-Ray Imaging Microscope with a Multilayer-Coated Schwarzschild Objective : Imaging Tests"Jpn. J. Appl. Phys.. 39・4A(印刷中). (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 豊田光紀: "多層膜対物鏡を用いた結像型軟X線蛍光顕微鏡の開発と評価"東北大学科学計測研究所報告. 48・1. 39-61 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Toyoda: "A Soft-X-Ray Imaging Microscope with Multilayer-coated Schwarzschild Optics"Proc. VIth Int'nl Conf. on X-Ray Microscopy. (印刷中). (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Toyoda: "A Soft-X-Ray Imaging Microscope Based on a Multilayer-Coated Schwarzschild Objective"Abst. 5th Int'nl Conf. on Phys. X-Ray Multilayer Structures. p-11.1 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 志谷能崇: "結像型軟X線発光顕微鏡の製作と性能評価"応物学会東北支部第54回学術講演会予稿集. 137-138 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 豊田光紀: "結像型軟X線発光顕微鏡の開発"第46回応用物理学関係連合講演会予稿集No.2. p-727 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 波岡武、山下広順: "X線結像光学"培風館. 309 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Toyoda, et al.: "A Soft-X-Ray Imaging Microscope with a Multilayer-Coated Schwarzschild Objective : Imaging Tests"Jpn. J. Appl. Phys.. 39(in press). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Toyoda, et al.: "Development and Tests of an Imaging-Type Soft-X-Ray Emission Microscope with a Multilayer-Coated Objective (in Japanese)"Bulletin of the Research Institute for Scientific Measurements, Tohoku University. Vol .48, No. 1. 39-61 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Toyoda, et al.: "A Soft-X-Ray Imaging Microscope with Multilayer-coated Schwarzschild Optics"Proceedings of VIィイD1thィエD1 International Conference on X-Ray Microscopy. (in press). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Toyoda, et al.: "A Soft-X-Ray Imaging Microscope based on a Multilayer-Coated Schwarzschild Objective"Abstracts of the 5ィイD1thィエD1 International Conference on the Physics of X-Ray Multilayer Structures. 11.1 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Shintani, et al.: "Development and Performance Tests of an Imaging-Type Soft-X-Ray Emission Microscope (in Japanese)"Abstracts of the 54ィイD1thィエD1 Annual Meeting of the Japan Society of Applied Physics, Tohoku Branch. 137-138 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Toyoda, et al.: "Development of an Imaging-Type Soft-X-Ray Emission Microscope (in Japanese)"Extended Abstracts (The 46ィイD1thィエD1 Spring Meeting, 1999) No. 2 ; The Japan Society of Applied Physics and Related Societies. 727 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] T. Namioka and K. Yamashita: "X-Ray Imaging Optics"(in Japanese) Baifu-kan, Tokyo. 1-309 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Yanagihara: "§4.2.2. Effects of the Surface Roughness"73-74

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Yanagihara: "§8.3. Evaluation Using Laser-Produced Plasma X-Rays"261-265

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M. Yanagihara: "Appendix 1. Measurements of the Optical Constants for Thin Films in the Soft X-Ray Region"296-299

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Mitsunori Toyoda: "A Soft-X-Ray Imaging Microscope with a Multilayer-Coated Schwarzschild Objective"Jpn. J. Appl. Phys.. 39・4A(印刷中). (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 豊田 光紀: "多層膜対物鏡を用いた結像型軟X線蛍光顕微鏡の開発と評価"東北大学科学計測研究所報告. 48・1(印刷中). (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] Mitsunori Toyoda: "A Soft-X-Ray Imaging Microscope Based on a Multilayer-Coated Schwarzschild Objective"Abstracts of the 5th Int'nl Conf. On Phys.of XMS. (印刷中). (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] Mitsunori Toyoda: "A Soft-X-Ray Imaging Microscope with Multilayer-Coated Schwarzchild Optics"Abstracts of the VI th Int'nl Conf. On X-Ray Microsc.. 93-94 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 志谷 能崇: "結像型軟X線発光顕微鏡の製作と性能評価"応用物理学会東北支部第54回学術講演会講演予稿集. 137-138 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 志谷 能崇: "結像型軟X線発光顕微鏡の開発II"第60回応用物理学会学術講演会講演予稿集. 第2分冊. 564 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 波岡 武: "X線結像光学"培風館. 309 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 豊田光紀: "結像型軟X線発光顕微鏡の開発" 平成11年春季応用物理学会学術講演会予稿集. 29a-ZC19 (1999)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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