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Development of Dynamic/Quasi-Static Fracture Toughness Testing Apparatus Using Miniaturized Specimens and Application to Evaluation of Local Toughness in Materials

Research Project

Project/Area Number 10555224
Research Category

Grant-in-Aid for Scientific Research (B).

Allocation TypeSingle-year Grants
Section展開研究
Research Field Structural/Functional materials
Research InstitutionMuroran Institute of Technology

Principal Investigator

MISAWA Toshihei  Muroran Institute of Technology, Faculty of Engineering, Professor., 工学部, 教授 (70005982)

Co-Investigator(Kenkyū-buntansha) SUZUKI Masahide  Japan Atomic Energy Research Institute, Senior Researcher., 原子力安全工学部, 主任研究員
KOBAYASHI Hidetoshi  Muroran Institute of Technology, Faculty of Engineering, Associated Professor., 工学部, 助教授 (10205479)
DAIMARUYA Masashi  Muroran Institute of Technology, Faculty of Engineering, Professor., 工学部, 教授 (40002018)
KOMAZAKI Shin-ichi  Muroran Institute of Technology, Faculty of Engineering, Research Associate., 工学部, 助手 (70315646)
KOBAYASHI Yasushi  Tanaka Co., Ltd., chief., 技術部・主任(研究職)
Project Period (FY) 1998 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥11,700,000 (Direct Cost: ¥11,700,000)
Fiscal Year 2000: ¥1,400,000 (Direct Cost: ¥1,400,000)
Fiscal Year 1999: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 1998: ¥8,700,000 (Direct Cost: ¥8,700,000)
KeywordsSmall Specimen Impact Test / Extra-Miniaturized Specimen / Local Fracture Toughness / Strength-Toughness Balance of Japanese Sword / Functional Gradient of Japanese Sword / Hydrogen Assisted Embrittlement / Critical Deformation Rate / Plastic Deformation Area at Crack Tip / 材料局部破壊靱性評価 / 日本刀の強度-靱性 / 日本刀材料試験 / 臨界水素脆化速度 / 微小試験片法 / 衝撃試験 / 微小衝撃試験 / 動的破壊靭性試験機 / 材料局部靭性評価
Research Abstract

From the present research program the following conclusion can be drawn :
1. We successfully developed the dynamic/quasi-static fracture toughness testing apparatus using miniaturized V-notch specimens where the fracture toughness can be evaluated under wide variety of deformation rate(4〜10^<-5>m/s).
2. Small specimen impact tests using miniaturized specimens with 1.5, 1.0 and 0.7 mm square and 20 mm length were carried out to evaluate the toughness of a laser welded metal. The DBTTs and FATTs given by the miniaturized and standard specimens showed a simple linear correlation. The laser welded metal composed of an extremely fine acicular ferrite structure was estimated to have such an excellent toughness as 168K DBTT in conversion to the standard size specimen.
3. Micro-structure, micro-hardness and micro-absorbed impact energy in the Japanese sword were investigated to clarify excellent mechanical properties of the Japanese sword. The HASAKI side had a lower value while the MUNE side showed a higher value in the micro-absorbed impact energies obtained with the 1.0 and 0.7 mm square miniaturized specimens. It was shown clearly that the TSUKURIKOMI and the TSUCHIOKI processes gave the excellent gradated balance of strength-toughness to the Japanese sword.
4. In order to clarify influence of deformation rate on susceptibility to hydrogen assisted embrittlement(HAE)in low alloy steels, three points bend test using v-notched small specimen with a dimension of 1.5×1.5×20mm was applied high strength low alloy steels with cathodically hydrogen charged. The test was carried out at room temperature under a wide variety of deformation rates, i.e., from 2.0×10^0to 1.7×10^<-8>m・s^<-1>. The test results showed that there was a critical deformation rate for the HAE in the high stength low alloy steels, where the fracture energy suddenly drops off and the fracture mode also transits from ductile fracture to brittle one.

Report

(4 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • Research Products

    (31 results)

All Other

All Publications (31 results)

  • [Publications] S. Watanabe: "Influence of Deformation Rate and Phosphorus/Boron Addition on Susceptibility to Hydrogen Assisted Embrittlement in High Strength Low Alloy Steels"Proceedings of APCFS 01 and ATEM'01. to be published. (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T. Misawa: "Ductile-Brittle Transition Evaluation of Japanese Sword, Welded Metal and Hydrogen Charged Steel Using Miniaturized Impact Specimens"Proceedings of CHARPY CENTENARY CONFERENCE. to be published . (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 駒崎 慎一: "高強度綱の内部水素による水素助長脆化(HAE)の臨界変形速度およびき裂先端塑性域減少の観察"文部科学省金属材料研究所 第5回超鉄鋼ワークショップ報告書. 284-285 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 佐々木 直彦: "日本刀の強度-塑性バランスと刃金用玉綱の折返し鍛練による炭素量、焼入れ硬さの変化"鉄と綱. Vol.86. 45-50 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 三澤 俊平: "吸着水素電位依存型侵入水素による脆化および内部チャージ水素による臨界脆化変形速度の出現"平成11年度科学技術振興調整費総合研究報告書「構造材料の環境脆化における水素の機能に関する研究-II」. 21-31 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 三澤 俊平: "鉄鋼材料にみる機能傾斜化の2事例-耐候性綱さび層と日本刀の断面解析"21世紀の新素材-産業界を活性化させる傾斜機能材料,第14回「大学と科学」公開シンポジウム組織委員会編,クバプロ. 81-95 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 川嶋 崇: "水素チャージした高強度綱の水素助長脆化臨界変形速度の出現"日本鉄鋼協会講演論文集「材料とプロセス」. Vol.13. 1371 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 川嶋 崇: "水素チャージした高強度綱の水素脆化臨界変形速度の出現"日本金属学会&日本鉄鋼協会両北海道支部合同夏期講演大会. 35 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 三澤 俊平: "微小衝撃試験片を用いた日本刀および折返し鍛練組織の傾斜破壊靭性評価"日本鉄鋼協会講演論文集「材料とプロセス」. Vol.11. 519 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 三澤 俊平: "微小衝撃試験片法による溶接部および日本刀断面の局部組織動的靭 性評価"日本金属学会講演概要. 123. 88 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 三澤 俊平: "微小衝撃試験法による鉄鋼レーザー溶接金属の延性脆性遷移の評価"鉄と綱. Vol.82. 707-712 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Watanabe, S.Komazaki and T.Misawa: "Influence of Deformation Rate and Phosphorus/Boron Addition on Susceptibility to Hydrogen Assisted Embrittlement in High Strength Low Alloy Steels"Proceeding of APCFS '01 and ATEM '01(to be published.). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa and S.Komazaki: "Ductile-Brittle Transition Evaluation of Japanese Sword, Welded Metal and Hydrogen Charged Steel Using Miniaturized Impact Specimens"Proceedings of CHARPY CENTENARY CONFERENCE(to be published.). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Komazaki, T.Kawashima, S.Watanabe and T.Misawa: "Observation of Critical Deformation Rate and Decrease in Plastic Deformation Area at Crack Tip of Hydrogen Assisted Embrittlement(HAE)by Internal Hydrogen in High Strength Steel"Proceedings of Fifth Workshop on the Ultra-Steel, National Research Institute for Metals. 284-285 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Sasaki, T.Horii, M.Fujiwara, H.Saitoh and T.Misawa: "Strength-Toughness Balance of the Japanese Sword and Changes in Carbon Content and as Quenched Hardness of HAGANE Steel with Cyclic Folding Forging"Tetsu-to-Hagane. Vol.86, No.1. 45-50 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa, R.Maruyama, M.Kudo and T.Kawashima: "Electrochemical Adsorbed-Hydrogen Induced Embrittlement and Critical Deformation Rate of Hydrogen Assisted Embrittlement(HAE)by Internal Hydrogen in High Strength Steel"Report on Functions of Hydrogen in Environmental Degradation of Structural Materials, Special Coordination Funds for Promoting Science and Technology, The Science and Technology Agency of Japan. 21-31 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa: "Two Examples of Functional Gradient in Steel-Observation of Cross Sections of Rust-Layer on Weathering Steel and Japanese Sword"New Materials of 21th Century, ISBN4-906347-98-3, Kuba Pro.. 81-95 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Kawashima, S.Komazaki and T.Misawa: "Appearance of Critical Deformation Rate in Hydrogen Assisted Embrittlement of Hydrogen Charged High Strength Steel"CAMP-ISIJ. Vol.13. 1371 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Kawashima and T.Misawa: "Appearance of Critical Deformation Rate in Hydrogen Embrittlement of Hydrogen Charged High Strength Steel"Proceedings of JIM & ISIJ Hokkaido Branch Summer Meeting 2000. 35 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa, N.Sasaki and T.Horii: "Evaluation of Functionally Graded Fracture Toughness in Japanese Sword and Fold-Forged Structures Using Miniaturized Impact Specimens"CAMP-ISIJ. Vol.11. 519 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa and N.Sasaki: "Evaluation of Local Dynamic Fracture Toughness in weld and Japanese Sword by Means of Small Specimen Impact Test"Proceedings of JIM Autumn Meeting 1998. 88 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Misawa, S.Takasa, Y.Nakano and K.Yasuda: "Ductile-Brittle Transition Evaluation of Laser Welded Steel Metal by Means of Small Specimen Impact Test"Tetsu-to-Hagane. Vol.82, No.8. 707-712 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 駒崎慎一,川嶋嵩,渡辺真悟,三澤俊平: "高強度鋼の内部水素による水素助長脆化(HAE)の臨界変形速度およびき裂先端塑性域減少の観察"文部科学省金属材料技術研究所 第5回超鉄鋼ワークショップ報告書. 284-285 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 三澤俊平,丸山理絵,工藤真紀子,川嶋嵩: "吸着水素電位依存型侵入水素による脆化および内部チャージ水素による臨界脆化変形速度の出現"日本鉄鋼協会 環境脆化プロジェクトチーム 平成11年度研究報告書. 21-31 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 三澤俊平: "鉄鋼材料にみる機能傾斜化の2事例-耐候性鋼さび層と日本刀の断面解析"21世紀の新素材,第14回「大学と科学」公開シンポジウム組織委員会編,クバプロ. 81-95 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 佐々木直彦,堀井胤匡,藤原幹男,斎藤英之,三澤俊平: "日本刀の強度-靭性バランスと刃金用玉鋼の折返し鍛練による炭素量,焼入れ硬さの変化"鉄と鋼. 86・1. 45-50 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 三澤俊平,高佐成樹,中野善文,安田功一: "微小衝撃試験法による鉄鋼レーザー溶接金属の延性脆性遷移の評価"鉄と鋼. 82・8. 73-78 (1996)

    • Related Report
      2000 Annual Research Report
  • [Publications] 佐々木直彦,堀井胤臣,藤原幹男,斎藤英之,三沢俊平: "日本刀の強度-靱性バランスと刃金用玉綱の折返し鍛錬による炭素量,焼入れ硬さの変化"鉄と綱. 86・1. 45-50 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 三澤 俊平: "微小衝撃試験片法による鉄鋼レーザー溶接金属の延性脆性遷移の評価" 鉄と鋼. 82・8. 707-712 (1996)

    • Related Report
      1998 Annual Research Report
  • [Publications] 三澤 俊平: "微小衝撃試験片法による溶接部および日本刀断面の局部組織動的靭性評価" 日本金属学会講演概要. 123. 88 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 三澤 俊平: "微小衝撃試験片を用いた日本刀および折返し鍛練組織の傾斜破壊靭性評価" 日本鉄鋼協会講演論文集(材料とプロセス)CAMP-ISIJ. 11. 519 (1998)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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