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Development of advanced crystallizar with on-line control of crystal diameter distribution

Research Project

Project/Area Number 10555264
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field 化学工学一般
Research InstitutionYokohama National University

Principal Investigator

KAMIWANO Mitsuo  Yokohama Nat.Unv., Faculty of Engineering, Professor, 工学部, 教授 (70017896)

Co-Investigator(Kenkyū-buntansha) SHIROTA Daigo  Idemitsu Petrochemical Co.Ltd., Research Center, Group Leader, 生産技術センター, 研究グループリーダー
NISHI Kazuhiko  Yokohama Nat.Unv., Faculty of Engineering, Assistant, 工学部, 助手 (20262412)
KAMINOYAMA Meguru  Yokohama Nat.Unv., Faculty of Engineering, Professor, 工学部, 教授 (50233945)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥13,100,000 (Direct Cost: ¥13,100,000)
Fiscal Year 1999: ¥8,000,000 (Direct Cost: ¥8,000,000)
Fiscal Year 1998: ¥5,100,000 (Direct Cost: ¥5,100,000)
Keywordsstirred-type crystallizer / DTB-type crystallizer / crystal size distribution / imaging processing system / 3-D crystal image / On-line measurment / On-line control / リアルタイム高速画像処理システム / 撹拌槽型晶析装置 / 分級型晶析装置 / DTB型晶析装置 / 結晶粒径分布制御 / 攪拌槽型晶析装置 / オンライン計測 / 結晶形態計測
Research Abstract

In this research, we propose an on-line measuring method for determining the crystal size distribution in a crystallizer. This method is to suck liquid including crystals out of the stirred-type crystallizer and to instantly observe a silhouette of the crystal in a multiphasic way using the imaging processing system. A variety of information on the crystals, such as the shape, diameter, agglomeration and/or breakage, can be obtained from the reconstructed 3-D images. In this paper, the crystal diameter distributions which are based on 3-D crystal images were measured in several crystallization conditions and two types of crystallizers. As a result, it is found that quantitative information on crystals in a crystallizer can be obtained using this method.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (8 results)

All Other

All Publications (8 results)

  • [Publications] Kamiwano,M., M.Kaminoyama,K.Nishi: "The Development of an On-Line Measuring. Method to Determine Crystal Size Distribution by Multiphasic. Observation using a Real-Time,High-Speed Image Processing System in the Stirred-Type Crystallizer "Proc. International Symposium of Industrial Crystallization. (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城田大吾,上和野満雄,上ノ山周,仁志和彦,清水一弘: "リアルタイム高速画像処理システムを用いた液々撹拌槽における液滴径分布の測定法"化学工学論文集. 25. 1015-1023 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] NIishi,K., M.Kamiwano, M.Kaminoyama: "The Measurement of Crystal Size Distribution by Multiphasic Observation using a Real-time. High-speed Image Processing System in a Stirred-type Crystallizer"Proc.APCChE99. 3. 1687-1690 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kamiwano, M., M.Kaminoyama K.Nishi: "The Measurement Method of Dispersed State using Real-Time, High Speed Image Processing System in Multiphase Agitated Vessel"Proc. ISMIP-3. 1. 211-218 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kamiwano, M., M.Kaminoyama and K.Nishi: "The Development of an On-Line Measuring Method to Determine Crystal Size Distribution by Multiphasic Observation using a Real-Time, High-Speed Image Processing System in the Stirred-Type Crystallizer"Proc.International Symposium of Industrial Crystallization. D-1. (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Shirota, D., M.Kamiwano, M.Kaminoyama, K.Nishi and K.Shimizu: "The Measurement Method of Drop Size Distribution using a Real-Time, High-Speed Image Processing System in the Liquid-Liquid Dispersed Vessel"Kagaku Kougaku Ronbunshu. 25. 1015-1023 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Nishi, K., M.Kamiwano and M.Kaminoyama: "The Measurement of Crystal Size Distribution by Multiphasic Observation using a Real-time, High-speed Image Processing System in a Stirred-type Crystallizer"Proc.APCChE99. 1687-1690 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Kamiwano, M., M.Kaminoyama and K.Nishi: "The Measurement Method of Dispersed State using Real-Time, High Speed Image Processing System in Multiphase Agitated Vessel"Proc.ISMIP-3. 211-218 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary

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Published: 1998-04-01   Modified: 2016-04-21  

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