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Research on Fatigue Fracture Mechanisms of Micro Materials

Research Project

Project/Area Number 10650090
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKobe University

Principal Investigator

NAKAI Yoshikazu  Department of Mechanical Engineering, Kobe University, Professor, 工学部, 教授 (90155656)

Co-Investigator(Kenkyū-buntansha) HIWA Chiaki  Graduate School of Science and Technology, Kobe University, Research Associate, 大学院・自然科学研究科, 助手 (80294198)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥3,500,000 (Direct Cost: ¥3,500,000)
Fiscal Year 1999: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 1998: ¥2,800,000 (Direct Cost: ¥2,800,000)
KeywordsMicro material / Fatigue / Micro machine / Fractography / Crack initiation / き裂発生 / クラフトグラフィー
Research Abstract

Fatigue test systems with electrolic-polishing apparatus were developed to study the size effect on the fatigue strength of the micro-materials. This system has an electro-dynamic actuator to load small amplitude cyclic force. Fatigue tests were conducted after manufacturing small cross-sectional specimens by the electrolic-polishing apparatus without removing specimens from the system. Commercially pure aluminum and iron wires of 1.0 mm diameter were employed for the fatigue tests. The minimum diameter of each specimen was from 0.20 to 0.60 mm. To remove the effect of stress gradient, cyclic axial force was applied. The frequency of the cyclic force was 50 Hz with the stress ratio of 0.1. In both materials, the fatigue strength was almost independent of the specimen diameter, and the variations in the fatigue life from specimen to specimen at the same stress amplitude were large, and the crack initiation life is dominant to total fatigue life.
The slip-band formation and fatigue crack-initiation processes in balk material of 70-30 brass were observed by means of atomic-force microscopy (AFM). The slip-band angle relative to the stress-axis at the specimen surface varied from 15 to 90°, and it appeared most frequently around 60°. The depth of the intrusion drastically increased with its outgrowth to a crack, and with coalescence of cracks, the width of cracks increased rapidly. The critical value of the intrusion depth for crack initiation was given as a function of the slip-band angle through a geometrical model for the slip-direction and the slip-step, and the critical value was independent of stress amplitude. From precise observations of slip-band tips, slip-bands had steep slope when they were blocked by grain boundaries, and the slip-bands descended by gradual slopes to plain surfaces when they terminated within grains.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (39 results)

All Other

All Publications (39 results)

  • [Publications] 中井 善一: "CFRP積層板のはく離型疲労き裂伝ぱに及ぼす温度変動及び環境の影響(第1報 130℃硬化型エポキシ樹脂を母材とする場合)"日本機械学会論文集(A編). 64. 584-589 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 中井 善一: "CFRP積層板のはく離型疲労き裂伝ぱに及ぼす温度変動及び環境の影響(第2報 180℃硬化型エポキシ樹脂を母材とする場合)"日本機械学会論文集(A編). 65. 312-319 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 中井 善一: "α黄銅における疲労き裂発生過程のAFMによる観察"日本機械学会論文集(A編). 65. 483-490 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. NaKai: "Observations of Fatigue Slip Band and Stage I Crack Initiation Process in α-brass by Scanning Atomic-force Microscopy"Small Fatigue Cracks : Mechanics and Mechanisms. 343-352 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. NaKai: "Observations of Corrosion Fatigue Process in 13Cr Stainless Steel by Means of AFM"Progress in Mechanical Behavior of Materials. Vol. I. 364-369 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. NaKai: "Size Effect on Fatigue Strength of Metallic Micro-materials"Proc. Asian-Pacific Conf. Fracture & Strength '99 (CD-ROM). SM22 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. NaKai: "Evaluation of Surface Damage in Fatigue and Tension Test of Steel by Laser Speckle Method and Scanning Atomic Force Microscopy"Fatigue '99. Vol. 4. 2771-2776 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. NaKai: "Measurement of Slip Band Size of α-Brass in Fatigue by Means of Scanning Atomic-Force Microscopy"Proceedings of the International Conference on Advanced Technology in Experimental Mechanics '99. Vol. 1. 152-157 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Naoya Sakata, and Chiaki Hiwa: "Delamination Crack Growth of Unidirectional CFRP Laminates under Variable Temperature (1st Report, 130℃ Cure Type Epoxy Resin Matrix)"Transactions of Japanese Society of Mechanical Engineers (A). 64-619. 584-589 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Chiaki Hiwa, Tadanobu Chikamoto, Yoshikazu Nakai, Michihiro Tsuji: "Effect of Surface Treatment for Fibers on Stress Relaxation of Short-Fiber Reinforced Plastics"Journal of Society of Material Science, Japan. 47-5. 484-488 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Chiaki Hiwa, Yoshikazu Nakai, Tadanobu Chikamoto, and Motomi Sugiyama: "Effect of Mixing Pressure in Injection Modeling on Interfacial Shear Stress of GF/PP Short-Fiber Reinforced Plastics"Journal of the Japan Society for Composite Materials. 24-3. 89-95 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Naoya Sakata, and Chiaki Hiwa: "Effects of Environment on Delamination Fatigue Crack Growth of CFRP Laminate under Constant ΔΚ conditions"First Asian-Australasian Conference on Composite Materials. Vol.II. 709-1-709-4 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Chiaki Hiwa, Yoshikazu Nakai, and Takaaki Kawamura: "Effect of Strain Rate on Interfacial Shear Stress of (GF/PP) Fuel Injection Short-Fiber Reinforced Plastics"Journal of The Adhesion Society of Japan. 35-1. 21-26 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Naoya Sakata, Taketoshi Kadowaki, and Chiaki Hiwa: "Delamination Crack Growth of Unidirectional CFRP Laminates under Variable Temperature (2nd Report, 180℃ Cure Type Epoxy Resin Matrix)"Transactions of Japanese Society of Mechanical Engineers (A). 65-630. 312-319 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Kenji Ohnishi, Teppei Kusakawa: "Observation of Fatigue Crack Initiation Process in α-Brass by AFM"Transactions of Japanese Society of Mechanical Engineers (A). 65-631. 483-490 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Chiaki Hiwa, Yoshikazu Nakai, and Takaaki Kawamura: "Effect of Surface Treatment for Fibers on Fatigue Behavior of (GF/PP) Fuel Injection Short-Fiber Reinforced Plastics"Transactions of Japanese Society of Mechanical Engineers (A). 65-631. 643-648 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Nakai, K.Ohnishi, and T.Kusukawa: "Observations of Fatigue Slip Bands and Stage I Crack Initiation Process in α-brass by Scanning Atomic-force Microscopy"Small Fatigue Cracks : Mechanics and Mechanisms, K. S. Ravichandran, R. O. Ritchie, and Y. Murakami, eds., Elsevier. 343-352 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Nakai, Y.Shimizu, and N.Saeki: "Observation of Corrosion Fatigue Process in 13Cr Stainless Steel by Means of AFM"Progress in Mechanical Behavior of Materials (ICM8), Fernand Ellyin and James W. Provan, eds.. Vol.I. 364-369 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Chiaki Hiwa, Takeshi Imanishi, and Akihisa Hashimoto: "Size Effect on Fatigue Strength of Metallic Micro-materials"Proceedings of Asian-Pacific Conf. Fracture & Strength '99 (CD-ROM), SM22. (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Nakai and M.Oida: "Evaluation of Surface Damage in Fatigue and Tension Test of Steel by Laser Speckle Method and Scanning Atomic Force Microscopy"Fatigue '99. 2771-2776 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Teppei Kusukawa, and Naohiko Hayashi: "Measurement of Slip Band Size of α-Brass in Fatigue by Means of Scanning Atomic-Force Microscopy"Proceedings of the International Conference on Advanced Technology in Experimental Mechanics '99 (ATEM'99). Vol.1. 152-157 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Taketoshi Kadowaki, and Chiaki Hiwa: "Effects of Frequency and Environment on Mode II Delamination Fatigue Crack Growth in CFRP Laminates"Transactions of Japanese Society of Mechanical Engineers (A). (To be published). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Teppei Kusukawa: "Quantitative Evaluation of Slip-Band Growth and Crack Initiation in Fatigue of 70-30 Brass by Means of Atomic-Force Microscopy"Transactions of Japanese Society of Mechanical Engineers (A). (To be published). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Yoshikazu Nakai and Chiaki Hiwa: "Effects of Loading Frequency and Environment on Delamination Fatigue Crack Growth of CFRP"Proceedings of the 2nd International Conference on Fatigue of. (To be published).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 中井善一: "レーザースペックル法とAFMによる疲労および引張りすべり変形の観察"日本機会学会講演論文集. No.99-4. 74-77 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Nakai: "Observations of Fatigue Slip Bands and Stage I Crack Initiation Process in α-brass by Scanning Atomic-force Microscopy"Small Fatigue Cracks;Mechanics and Mechanisms. 343-352 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Nakai: "Observations of Corrosion Fatigue Process in 13Cr Stainless Steel by Means of AFM"Progress in Mechanical Behavior of Materials. Vol.I. 364-369 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Nakai: "Size Effect on Fatigue Strength of Metallic Micro-materials"Proc.Asian-Pacific Conf.Fracture & Stength '99(CD-ROM). SM22 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Nakai: "Evaluation of Surface Damage in Fatigue and Tension Test of Steel by Laser Speckle Method and Scanning Atomic Force Microscopy"Fatigue '99. Vol.4. 2771-2776 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Nakai: "Measurement of Slip Band Size of α-Brass in Fatigue by Means of Scanning Atomic-Force Microscopy"Proceedings of the Internationl Conference on Advanced Technology in Experimental Mechanics '99. Vol.1. 152-157 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 中井善一: "α黄銅における疲労すべり帯の形状とき裂発生条件のAFMによる解明"日本機会学会講演論文集. No.99-16. 547-548 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 中井善一: "α黄銅における疲労すべり帯およびステージIき裂発生過程の走査型原子間力顕微鏡による観察" 日本材料学会・第47期学術講演会・講演論文集. 71-72 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 中井善一: "α黄銅における疲労すべり帯の成長および微小き裂発生過程のAFMによる観察" 日本材料学会・第24回疲労シンポジウム. 203-206 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 中井善一: "α黄銅における疲労き裂発生過程のAFMによる観察" 日本機械学会論文集(A編). 第65巻,第631号(掲載予定). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 橋本晃久: "微小な断面を有する試験片の疲労寿命評価とその疲労破壊機構の観察" 日本機械学会関西支部第74期定時総会講演会・講演論文集. No.994-1(掲載予定). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Nakai: "Observations of Fatigue Slip Bands and Stage I Crack Initiation Process in α-brass by Scanning Atomic-force Microscopy" Small Fatigue Cracks:Mechanics and Mechanism. (掲載予定). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Nakai: "Size Effect on Fatigue Strength of Metallic Micro-materials" Proc.Asian-Pacific Conf.Fracture & Strength '99. (発表予定). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Nakai: "Observation of Corrosion Fatigue Process in 13Cr Stainless Steel by Means of AFM" Proc.8^<th> Int.Conf.Mech.Bahav.Mat.(掲載予定). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.NAKAI: "Measurement of Slip Band Size of α-Brass in Fatigue by Scanning Atomic-Force Microscopy" International Conference on Advanced Technology in Experimental Mechanics '99. (発表予定). (1999)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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