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Evaluation of Si/Ge ALE super lattice with high depth resolution AES method

Research Project

Project/Area Number 10650321
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionTeikyo University of Science and Technology

Principal Investigator

UCHIDA Yasutaka  Teikyo Univ.of Sci. and Tech., Undergraduate School of Science and Engineering, Associate professor, 理工学部, 助教授 (80134823)

Co-Investigator(Kenkyū-buntansha) SUGAHARA Satoshi  Tokyo Institute of Technology, Faculty of Engineering, Research associate, 工学部, 助手 (40282842)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥3,300,000 (Direct Cost: ¥3,300,000)
Fiscal Year 1999: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 1998: ¥2,600,000 (Direct Cost: ¥2,600,000)
KeywordsAES / Si / Ge hetero interface / super lattice / AFM / CAICISS / ALE / XPS / サーファクタント / 組成分布 / 平坦性
Research Abstract

In order to evaluate abruptness of Si/Ge hetero interface, we have developed novel analysis method for depth profile for Auger Electron Spectroscopy (AES). By optimizing accelerating voltage of Ar sputtering, electron-beam current density and electron-beam diameter, we have confirmed that transition region of Si and SiO2 interface which was well known as a atomically flat by using Si(111) just wafer and oxidizing very carefully was lower than 1nm. Further more, escape depth λ of Auger electron has strong influence on the evaluation of atomically abrupt interface although it is a short as 0.5nm in a low kinetic energy region less that 100eV. Then deduced transition region obtained from calculated depth profiles was as narrow as 0.35nm. This value was almost same as 1 atomic layer. Also we have confirmed that flatness of etched surface was kept in a very good condition by AFM measurement.
We have applied this novel method to Si/Ge hereto-super lattice which consists of 3 Mono Layer (ML) of Ge and 7ML of Si by using atomic layer epitaxy (ALE). It was confirmed that observed AES intensity distribution along the depth was represented to the supper lattice structure. Signal intensity of Ge was sharply changed at Si/Ge interfaces and this means that segregation of Ge was well suppressed. According to this experiment, flatness of both Si and Ge buffer layers had important role for suppressing the strain of the supper lattice. Thus we have optimizing the growth condition of buffer layer to suppressing growth rate lower than 0.5nm/min. Runs of Ge and Si buffer layer were 0.15nm and 0.1nm, respectively. Early stage of ALE was investigated by using CAICISS. Layer by layer growth was confirmed for the ALE method.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (13 results)

All Other

All Publications (13 results)

  • [Publications] M.Matsuyama: "Hetero Atomic-Layer Epitaxy of Ge on Se(100)"Jpn. J. Appl. Phys.. 39. (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 松山元彦: "Si(111)へのゲルマニウムへのヘテロ原子層エピタキシー"第59回応用物理学会学術講演会予稿. 330 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 池田圭司: "原子層エピタキシーによるSi/Ge原子層超格子の作製"第59回応用物理学会学術講演会予稿. 330 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 柳瀬慈郎: "Si(100)面上へのGeの単原子層吸着特性評価"第47回応用物理学関連合同講演会予稿. (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 池田圭司: "Ge(100)表面へのSiヘテロ原子層成長初期特性の評価"第47回応用物理学関連合同講演会予稿. (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Matsuyama et al.: "Hetero Atomic-Layer Epitaxy of Ge on Si(100)"Jpn. J. Appl. Phys. (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] M.Matsuyama et al.: "Hetero Atomic-Layer Epitaxy of germanium on Si(111)"1998 Fall Meeting, Jpn.Soc.Appl.Phys.. 15aYK5. 330

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ikeda et al.: "Preparation of Si/Ge Atomic-Layer Superlattices by Atomic-Layer Epitaxy"1998 Fall Meeting, Jpn.Soc.Appl.Phys.. 15aYK6. 330

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Yanase et al.: "Evaluation of Mono Atomic-Layer Deposition Characteristics of Germanium on Si(100) surface"2000 Spring Meeting, Jpn.Soc.Appl.Phys.. 28a-YF-4.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] K.Ikeda et al.: "Characterization of Initial Stage of Si Hetero-ALE on Ge(100)"2000 Spring meeting, Jpn.Soc.Appl.Phys.. 28a-YF-5.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 柳瀬慈郎: "SI(100)面上へのGeの単原子層吸着特性評価"応用物理学関係連合講演会講演予稿集. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 池田圭司: "Ge(100)表面へのSiヘテロ原子層成長初期特性の評価"応用物理学関係連合講演会講演予稿集. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 池田圭司: "原子層エピタキシーによるSi/Ge原子層超格子の作製" 第59回応用物理学会学術講演会講演予稿集. 330 (1998)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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