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Verification of the Displasive-Diffusion-less Mechanism in Bainitic Phase Transformations by a High Resolution Fractography

Research Project

Project/Area Number 10650655
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionKanazawa Institute of Technology

Principal Investigator

SHIMIZU Kenichi  Kanazawa Institute of Technology, Department of Engineering, Professor, 工学部, 教授 (60029832)

Co-Investigator(Kenkyū-buntansha) KISHI Yoichi  Kanazawa Institute of Technology, Department of Engineering, Assistant Professor, 工学部, 講師 (70265370)
YAJIMA Zenjiro  Kanazawa Institute of Technology, Department of Engineering, Professor, 工学部, 教授 (60148145)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥4,000,000 (Direct Cost: ¥4,000,000)
Fiscal Year 1999: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 1998: ¥2,400,000 (Direct Cost: ¥2,400,000)
KeywordsBainite / Phase Transformation / Atomic Diffusion Type / Displasive-Diffusionless Type / Cu-Zn-Al Alloy / High Resolution Fractography / 高分解能フラクトグラフィ / 高分解能フラクトグラフイ
Research Abstract

The bainitic transformation is believed to finally proceed by a diffusion mechanism of atoms. However, there has also been proposed another idea where a displasive-diffusionless mechanism is operated in the nucleation stage and early stage of growth of bainitic transformations. The present investigation was carried out to verify which of the two mechanisms, diffusion or displeasures and atomic compositions of the bainitic plate and its matrix confronted along their interphase boundary on tensile-fractured surfaces, that is, by doing fractography with a high resolution scanning electron microscope (SEM) equipped with a field emission electron gun.
The materials used for the verification are carbon steels (JIS S25C and S%%C) and Cu-28.3Xn-6.0Al(at .%) alloy, and the results obtained for the latter alloy will be reported below, because those for carbon steels were previously reported. In order to observe certainly a bainite plate and its matrix confronted on tensile-fractured surfaces, the volume ration of bainite plates to the matrix must be appropriate. The ratio was first examined by changing both isothermal holding temperature and time for the bainitic transformation, and 473 K and 28.8 Ks were found to be appropriate. The bainitic specimens subjected to this heat-treatment were tensile-fractured, and the fractured surfaces were observed by the high resolution fractography. Areas, where a bainite plate and its matrix seem to be confronted, were search, and EDX analyses were performed for the confronted bainite plates and matrices. As a result, it was found that atomic compositions of the plate and matrix were the same, and therefore the displasive-diffusionless mechanism is supposed to be really operated. However, more detailed examination is needed, because a little ambiguity is remained for the identification of bainite plates and matrices confronted on fractured surfaces.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (23 results)

All Other

All Publications (23 results)

  • [Publications] T.Kakeshita, T.Saburi, K.Shimizu: "Kinetics of Martensitic Transformations in Some Ferrous and Non-Ferrous Alloys"Philosophical Magazine B. 80・2. 71-81 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & K.Morii: "Fatigue Crack Growth Properties and Scanning Electron Microscopy of Fatigue Surface of Ti-Ni-Co SMA's"Proc. Intern'l. Symp. & Exhib. On Shape Memory Mater. (Mater. Sci. Forum). 327-328. 123-126 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & M.Asai: "Mechanical Fatigue Crack Growth Characteristics of A Ti-Ni-Cu Shape Memory Alloy"Proc. of Solid-Solid Phase Transformations (PTM'99). 1052-1055 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & K.Morii: "Effect of Microstructures on Mechanical Fatigue Crack Growth Character. of a Ti-Ni-Co Shape Mem. Al."Intern'l Conf. on Martensitic Transformations (ICOMAT'98). 654-657 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima and K.Shimizu: "Effect of Microstructures on Fatigue Behavior of Ti-49.7at.%Ni-1.38at.%Co Shape Memory Alloy"Proc. Japan-China Bilateral Symp. on Shape Memory Alloys. 75-80 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 清水謙一: "変位型原子無拡散変態に関する研究の流と学界の動き"日本鉄鋼協会誌"ふぇらむ". 3・2. 31-36 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] T.Kakeshita, T.Saburi and K.Shimzu: "Kinetics of Martensitic Transformations in Some Ferrous and Non-Ferrous Alloys"Phil.Mag.B. Vol.80, No.2. 71-81 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & K.Morii: "Fatigue Crack Growth Properties and Scanning Electron Microscopy of Ti-Ni-Co Shape Memory Alloy"Proc.Intern'l. Symp. & Exhib.on Shape Mem.Mater. (Mater.Sci.Forum). Vol.327-328. 123-126 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & M.Asai: "Mechnical Fatigue Crack Growth Characteristics of a Ti-Ni-Cu Shape Memory Alloy"Proc.Intern'l.Conf.on Solid-Solid Phase Trans. 1052-1055 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu & K.Morii: "Effects of Microstructure on Mechanical Fatigue Crack Growth Characteristics of a Ti-Ni-Co Shape Memory Alloy"Proc.Intern'l Conf.on Martens.Transf. (ICOMAT'99). 654-657 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Kishi, Z.Yajima, K.Shimizu: "Effects of Microstructure on Fatigue Behavior of Ti-49.7 at.%Ni-1,38at.%Co Shape Memory Alloy"Proc.Japan-China Bilat.Symp.on Shape Mem.Allogys. 75-80 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] T.Kakeshita,T.Saburi,K.Shimizu: "Kinetics of Martensitic Transformations in Some Ferrous and Non-Ferrous Alloys"Philosophical Magazine B. 80・2. 71-81 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Kishi,Z.Yajima,K.Shimizu & K.Morii: "Fatigue Crack Growth Properties and Scanning Electron Microscopy of Fatigue Surface of Ti-Ni-Co SMA's"Proc.Intern'l.Symp.& Exhib.On Shape Memory Mater.(Mater.Sci.Forum). 327-328. 123-126 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Kishi,Z.Yajima,K.Shimizu & M.Asai: "Mechanical Fatigue Crack Growth characteristics of A Ti-Ni-Cu Shape Memory Alloy"Proc.of Solid-Solid Phase Transformations(PTM'99). 1052-1055 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Kishi,Z.Yajima,K.Shimizu & K.Morii: "Effect of Microstructures on Mechanical Fatigue Crack Growth Character.of a Ti-Ni-Co Mem.Al."Intern'l.Conf.on Martensitic Transformations(ICOMAT'98). 654-657 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Kishi,Z.Yajima and K.Shimizu: "Effect of Microstructures on Fatigue Behavior of Ti-49.7at.%Ni-1.38at.%Co Shape Memory Alloy"Proc.Japan-China Bilateral Symp.on Shape Memory Alloys. 75-80 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] 清水 謙一: "変位型原子無拡散相変態に関する研究の流と学界の動き"日本鉄鋼協会誌"ふぇらむ". 3・2. 31-36 (1998)

    • Related Report
      1999 Annual Research Report
  • [Publications] T.Kakeshita,Y.Sato,T.Saburi,K.Shimizu et al.: "Effects of Magnetic Field on Athrmal and Isothermal Martensitic Transformations in Fe-Ni-Cr Alloys" Mater.Transactions,Jpn.Inst.Metals. 40,2. 100-106 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] T.Kakeshita,Y.Sato,T.Saburi,K.Shimizu et al.: "Effects of Static Magnetic Field na Hydrostatic Pressure on the Isothermal Martensitic Transformations in an Fe-Ni-Cr Alloy" Mater.Transactions,Jpn.Inst.Metals. 40,2. 107-111 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] K.Shimizu: "Recent Activities of the Japan Association of Shape Memory Alloys" Proc.Japan-China Bilat.Symp.on Shape Mem.Alloy. 1-8 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.KIshi,Z.Yajima and K.Shimizu: "Effect of Microstructures on Fatigue Behavior of Ti-49.7at%Ni1.38at%Co Shape Memory Alloy" Proc.Japan-China Bilat.Symp.on Shape Mem.Alloys. 75-80 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 清水謙一: "マルテンサイト変態結晶学の歴史-西山・Kurdjumovの業績を中心に" 日本金属学会会報“まてりあ". 37,8. 655-658 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 清水謙一: "変位型原子無拡散相変態に関する研究の流れと学界の動き" 日本鉄鋼協会誌“ふえらむ". 3,2. 31-36 (1998)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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