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Basic Study on the high-Temperature Deformation in Thin Metallic Films and Wires

Research Project

Project/Area Number 10650688
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionIbaraki University (2000)
Nagaoka University of Technology (1998-1999)

Principal Investigator

ITOH Goroh  Ibaraki University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (80158758)

Project Period (FY) 1998 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2000: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1999: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1998: ¥2,500,000 (Direct Cost: ¥2,500,000)
KeywordsAl-1%Si-0.5%Cu alloy / creep / high-temperature deformation mechanism / grain size / specimen thickness / stress exponent / subgram / stress induced voiding / 試験片厚さ / 転位クリープ / しきい応力 / 亜結晶粒 / 分散相 / 粒内延性破壊 / 再結晶集合組織 / 拡散クリープ
Research Abstract

To elucidate the difference in the deformation and fracture mechanisms between connect lines in microelectronic circuits and bulk materials, effects of specimen thickness, t, and grain size, d, on the high-temperature creep deformation behavior in Al-1%Si-0.5%Cu alloy thin sheets and foils have been investigated. The alloy is frequently used for connect lines in the form of sputtered thin film line. The primary issue of this study is whether the high-temperature deformation mechanism of simply thin aluminum materials is different from that of the bulk material or not, and whether the same type of fracture as in what is called stress induced voiding takes place in such thin materials or not.
The results showed that steady-state creep rate was proportional to the -α-th power of t/d, and that the exponent α was approximately constant and unity at the applied stress σ of 30 MPa and over. The value of α decreased with decreasing the applied stress but was always positive in the range of the … More present experimental condition. This means that the creep rate increases with increasing grain size and with decreasing specimen thickness. Although apparent stress exponent was a value as high as from 7.9 to 10.4, taking the threshold stress into account, true stress exponent was deduced to be 5. The result that the dispersion of silicon phase particles was observed supports the existence of threshold stress, and the true stress exponent of 5 (dislocation creep controlled by recovery or dislocation climb ) was supported by the TEM observation that the microstructure during the steady-state creep consists of subgrains. Fractograpy showed that intergranular fracture as was observed in the case of stress induced voiding did not occur. The fracture morphology was dimple-forming type in the near-bulk specimens where t≧200μm, and chisel-line type, typical to the extremely ductile materials, in thinner specimens where t≦100μm. From these results, it has been deduced that high-temperature deformation in such thin materials proceeds in a newly proposed model based on heterogeneity in the subgrain structure during the deformation, where subgrains are finer in the vicinity of the grain boundary and coarser near the free surface. This model is expected to become one of the fundamental theories in the field of high- temperature deformation in metallic materials where merely homogeneous microstructure has been taken into account so far. Less

Report

(4 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • Research Products

    (14 results)

All Other

All Publications (14 results)

  • [Publications] 新田隆憲,伊藤吾朗: "アルミニウム合金箔のクリープ変形に及ぼす試料厚さと結晶粒径の影響"日本金属学会誌. 63. 196-200 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou,G.Itoh,T.Yamashita: "Further study on the effects of specimen thickness and grain size on the behavior of aluminum alloy foils"Materials Transactions of the Japan Institute of Metals. 40. 443-446 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou,G.Itoh: "Creep behavior of aluminum alloy foils for microelectronic circuits"Key Engineering Materials. 171-174. 633-638 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou,G.Itoh,T.Yamashita: "Creep mechanism of aluminum alloy thin foils"Thin Solid Films. 375. 104-108 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Nitta and G.Itoh: "Effects of specimen thickness and grain size on creep deformation of aluminum alloy foils"J.Japan Instit.Metals. Vol.63, No.2. 196-200 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou, G.Itoh and T.Yamashita: "Further study on the effects of specimen thickness and grain size on the creep behavior of aluminum alloy foils"Mater.Trans.JIM. Vol.40, No.5. 443-446 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou and G.Itoh: "Creep behavior of aluminum alloy foils for microelectronic circuits"Key Eng.Mater.. Vols.171-174. 633-638 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Q.Zhou, G.Itoh and T.Yamashita: "Creep mechanism of aluminum alloy thin foils"Thin Solid Films. Vol.375, No.1-2. 104-108 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 新田隆憲,伊藤吾朗: "アルミニウム合金箔のクリープ変形に及ぼす試料厚さと結晶粒径の影響"日本金属学会誌. 63巻・2号. 196-200 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] Q.Zhou,G.Itoh,T.Yamashita: "Further study on the effects of specimen thickness and grain size on the creep behavior of aluminum alloy foils"Materials Transaction of the Japan Institute of Metals. 40巻・5号. 443-446 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] Q.Zhou,G.Itoh: "Creep behavior of aluminum alloy foils for microelectronic circuits"Key Engineering Materials. 171-174巻. 633-638 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Q.Zhou,G.Itoh,T.Yamashita: "Creep mechanism of aluminum alloy thin foils"Thin Solid Films. 375巻1-2号. 104-108 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Q.Zhou,G.Itoh and T.Yamashita: "Further Study on the Effects of Specimen Thickness and Grain Size on the Creep Behavior of Aluminum Alloy Foils"Materials Transactions, JIM. 40・5. 443-446 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Q.Zhou and G.Itoh: "Creep Behavior of Aluminum Alloy Foils for Microelectronic Circuits"Key Engineering Materials. 171. 633-638 (2000)

    • Related Report
      1999 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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