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DEVELOPMENT OF IN-SITU ELECTRIC MEASUREMENT OF VULCANIZAION PROCESS OF RUBBER

Research Project

Project/Area Number 10650724
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionKURUME NATIONAL COLLEGE OF TECHNOLOGY

Principal Investigator

MORI Tetsuo  KURUME NATIONAL COLLEGE OF TECHNOLOGY, DEPARTMENT OF BIOCHEM. & APPLIED CHEM. PROFESSOR, 生物応用化学科, 教授 (10037963)

Co-Investigator(Kenkyū-buntansha) OIKI Hirokazu  KURUME NATIONAL COLLEGE OF TECHNOLOGY, DEPARTMENT OF BIOCHEM. & APPLIED CHEM. ASSISTANT, 生物応用化学科, 助手 (00290825)
TSUDA Yusuke  KURUME NATIONAL COLLEGE OF TECHNOLOGY, DEPARTMENT OF BIOCHEM. & APPLIED CHEM. ASSOCIATE PROFESSOR, 生物応用化学科, 助教授 (30270367)
TOH Michiharu  KURUME NATIONAL COLLEGE OF TECHNOLOGY, DEPARTMENT OF BIOCHEM. & APPLIED CHEM. PROFESSOR, 生物応用化学科, 教授 (70037927)
Project Period (FY) 1998 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥2,100,000 (Direct Cost: ¥2,100,000)
Fiscal Year 1999: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1998: ¥1,600,000 (Direct Cost: ¥1,600,000)
KeywordsRubber / Vulcanization / Cure Curve / Dielectric Loss Tangent / Conductivity
Research Abstract

Vulcanization of NBR, BR and SBR rubbers was carried out in a compression mold equipped with two electrodes for the electric measurement. Progress of vulcanization was followed by the measurement of dielectric loss tangent (tanδ) and electric current applying alternating or direct voltage. The conductivity was calculated from electric current, dimension of an electrode, etc. Rubber compounds with 40phr of carbon black to 100phr of rubber, or without carbon black were prepared. The tanδand conductivity-cure time curves were compared with the torque-cure time curve, which is widely used as a cure curve. The following result was obtained. (1)The vulcanization of NBR with and without carbon black could be followed by measuring tanδor conductivity applying alternate or direct voltage. (2)The vulcanization of BR without carbon black could be followed by measuring conductivity applying direct voltage. (3)The vulcanization of SBR without carbon black could be followed by measuring tanδapplying alternate voltage. (4)The vulcanization of BR and SBR with carbon black could not be followed, because much electric current flew at the early stage of vulcanization.

Report

(3 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • Research Products

    (8 results)

All Other

All Publications (8 results)

  • [Publications] 権藤豊彦: "ニトリルゴムの加硫反応中の電流および誘電正接の即時測定"日本ゴム協会誌. 71巻. 281-285 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 森哲夫: "Electric in-situ Measurement of vulcanization"Rubber World. 221巻. 33-36 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Toyohiko GONDOH, Tetsuo MORI, Michiharu TOH, Satoko FUJIE, Daisaburo OKAI: "In Situ Dielectric Loss Tangent and Electric Current Measurement of Vulcanization Process"Nippon Gomu Kyokaishi. 69. 708-710 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Toyohiko GONDOH, Seiji ETOH, Yukiko MATSUOKA, Michiharu TOH, Tetsuo MORI, Daisaburo OKAI: "In Situ Electric Measurement of Vulcanization Process of Rubber"Kobunshi Ronbunshu. 54. 359-361 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Toyohiko GONDOH, Yukiko MATSUOKA, Michiharu TOH, Daisaburo OKAI, Tetsuo MORI: "In Situ Measurement of and Electric Current and Dielectric Loss Tangent During Vulcanization of Nitrile Rubber"Nippon Gomu Kyokaishi. 71. 281-285 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Tetsuo MORI, Seiji ETOH, Yukiko MATSUOKA, Toyohiko GONDOH, Michiharu TOH, Daisaburo OKAI: "Electric in-situ Measurement of Vulcanization Rubber"Rubber World. 221. 33-35 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 森哲夫: "Electric in-situ measurement of vulcanization"Rubber World. 221巻4号. 33-36 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 権藤豊彦: "ニトリルゴムの加硫反応中の電流および誘電正接の即時測定" 日本ゴム協会誌. 71巻5号. 281-285 (1998)

    • Related Report
      1998 Annual Research Report

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Published: 1998-04-01   Modified: 2016-04-21  

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