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Processing for multi-functions・Materials development

Research Project

Project/Area Number 11221202
Research Category

Grant-in-Aid for Scientific Research on Priority Areas (B)

Allocation TypeSingle-year Grants
Review Section Science and Engineering
Research InstitutionTohoku University

Principal Investigator

HANADA Shuji  Tohoku University, Institute for Materials Research, Professor, 金属材料研究所, 教授 (10005960)

Co-Investigator(Kenkyū-buntansha) YOSHIMI Kyosuke  Institute for Materials Research, Research Assoc., 金属材料研究所, 助手 (80230803)
MURAYAMA Yonosuke  Institute for Materials Research, Research Assoc., 金属材料研究所, 助手 (60111308)
MASAHASHI Naoya  Tohoku University, Institute for Materials Research, Assoc. Professor, 金属材料研究所, 助教授 (20312639)
NOMURA Naoyuki  Institute for Materials Research, Research Assoc., 金属材料研究所, 助手 (90332519)
相原 智康  東北大学, 金属材料研究所, 助手 (00231100)
Project Period (FY) 1999 – 2001
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥55,700,000 (Direct Cost: ¥55,700,000)
Fiscal Year 2001: ¥5,600,000 (Direct Cost: ¥5,600,000)
Fiscal Year 2000: ¥28,000,000 (Direct Cost: ¥28,000,000)
Fiscal Year 1999: ¥22,100,000 (Direct Cost: ¥22,100,000)
Keywordsharmonic material design / very high temperature structural material / high temperature strength / fracture toughness / oxidation resistance / in-situ composite / interface / microstructure / 強度 / 靭性 / 複合鋼板 / 耐酸化コーティング / 生体用形状記憶合金
Research Abstract

Strength, fracture toughness and oxidation resistance were selected among many properties for high temperature structural materials and harmonic material design was studied.
In-situ composites consisting of ductile particle-dispersion refractory intermetallics and ceramics in which both the phases are thermodynamically equilibrated were synthesized by controlling alloying behavior and microstructure. Directionally solidified eutectic ZrC/Mo in-situ composite, which is prepared by the high frequency floating zone melting method, shows the room temperature fracture toughness of about 20 MPam^<1/2> and high strength at 1500C of 420 MPa. The high fracture toughness is attributable to crack deflection arising from decohesion between ZrC and Mo and the high strength at 1500C is due to solid solution strengthening and microstructure refinement.
High temperature strength of Mo-Si-B alloys is shown to increase significantly by alloying without sacrificing room temperature fracture toughness. The new concept of "pseudo in-situ composite" is presented and pseudo in-situ Mo-Si-B-O composite is found to exhibit excellent oxidation resistance at 1400C.
Based on the fundamental research of the diffusion bonding, clad hot rolling is successfully carried out using Fe_3Al base alloys and CrMo steel. The clad hot rolled sheet shows harmonically high strength, good oxidation resistance and high fracture toughness.

Report

(4 results)
  • 2002 Final Research Report Summary
  • 2001 Annual Research Report
  • 2000 Annual Research Report
  • 1999 Annual Research Report
  • Research Products

    (45 results)

All Other

All Publications (45 results)

  • [Publications] 松原 学, 岩崎敏彦, 花田修治: "傾斜機能させたNb-Al/Al_2O_3皮膜のプラズマ溶射による作製"日本金属学会誌. 64. 677-683 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] C.L.Ma, A.Kasama, H.Tanaka, Y.Tan, R.Tanaka, Y.Mishima, S.Hanada: "Microstructures and Mechanical Properties of Nb/Nb-Silicide in-situ Composites Synthesized by Reactive Hot Pressing of Ball Milled Powders"Mater.Trans.,JIM. 41. 444-451 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 平井寿敏, 田原竜夫, 上野英俊, 北原 晃, 花田修治: "一方向凝固したNb-xMo-22Ti-18Si系In-Situ複合材料の組織と機械的性質"日本金属学会誌. 64. 474-480 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 沙 江波, 平井寿敏, 田原竜夫, 北原 晃, 上野英俊, 花田修治: "アーク溶解および一方向凝固法により作製したNb-Mo-Ti-Si-C系in-situ複合材料の組織と機械的性質"日本金属学会誌. 64. 331-334 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] S.Hanada, W.Fang: "Superplasticity in Nb_3Al/Nb in-situ composites"Superplasticity-Current status and future. 601. 15-24 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] C.L.Ma, Y.Tan, H.Tanaka, A.Kasama, R.Tanaka, S.Miura, Y.Mishima, S.Hanada: "Phase Equilibria in Nb-Mo-Rich Zone of the Nb-Si-Mo Ternary System"Mater.Trans.,JIM. 41. 1329-1336 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Naoya Masahashi, Sadao Watanabe, Shuji Hanada: "Microstructure and Oxidation Behavior of Low Pressure Plasma Sprayed Iron Aluminides"ISIJ International. Vol.41 No.9. 1010-1017 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Naoya Masahashi, Naoyuki Kondo, Sadao Watanabe, Shuji Hanada: "Composite Steel based on Iron Aluminides"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing(PRICM 4),ed.by S.Hanada, Z.Zhong, S.W.Nam, and R.N.Wright, JIM. 819-822 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Kyosuke Yoshimi, Shinya Nakatani, Tomokazu Suda, Shuji Hanada: "Strength and Oxidation of Mo_5SiB_2-based In-situ Composites at High Temperatures"Transactions of the Materials Research Society of Japan. 26. 141-144 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Yuetsu Danzaki, Kazuaki Wagatsuma, Tsutomu Syoji, Kyosuke Yoshimi: "Dissolution of molybdenum-silicon (-boron) alloys using a mixture of sulfuric, nitric and hydrofluoric acids and a sequential correction method for ICP-AES analysis"Fresenius J Anal Chem. 369. 184-186 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Yoshimi, M.H.Yoo, A.A.Wereszczak, S.M.Borowicz, E.P.Georre, R.H.Zee: "Yielding and flow behavior of Mo_5Si_3 single crystals"Scripts Materialia. 45. 1321-1326 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Kyosuke Yoshimi, Shuji Hanada, Eiji Aoyagi: "Analysis of Protective Oxide Scale on Mo_5SiB_2-based Alloy Oxidized at High Temperature"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed.by S.Hanada, Z.Zhong, S.W.Nam and R.N.Wright, JIM. 975-978 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Shinya Nakatani, Kyosuke Yoshimi, Shuji Hanada, Se-Hyon Ko, Yong-Ho Park: "Design of Mo-Si-B-O Pseudo In-situ Composites for High Temperature Applications"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed.by S.Hanada, Z.Zhong, S.W.Nam and R.N.Wright, JIM. 971-974 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Kyosuke Yoshimi, Shuji Hanada: "Microstructures and Mechanical Properties of Eutectic Mo-XC(X=Ti, Zr, Hf) In-situ Composites"Transactions of the Materials Research Society of Japan. 26. 307-310 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Naoya Masahashi, Shuji Hanada: "Microstructures and Fracture Toughness of Mo-ZrC Eutectic Composites"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed.by S.Hanada, Z.Zhong, S.W.Nam and H.N.Wright, JIM. 2763-2766 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Manabu Matsubara, Toshihiko Iwasaki, Shuji Hanada: "Synthesis of Functionally Graded Nb-Al/Al_2O_3 Coatings by Plasma Spraying (in Japanese)"Nippon Kinzoku Gakkaishi (J. Jpn. Inst. Met.). 64[8]. 677-683 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] C.L.Ma, A.Kasama, H.Tanaka, Y.Tan, R.Tanaka, Y.Mishima, S.Hanada: "Microstructures and Mechanical Properties of Nb/Nb-Silicide in-site Composites Synthesized by Reactive Hot Pressing of Ball Milled Powders"Mater. Trans., JIM. 41. 444-451 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Hisatoshi Hirai, Tatsuo Tabaru, Hidetoshi Ueno, Akira Kitahara, Shuji Hanada: "Microstructures and Mechanical Properties of Directionally Solidified Nb-xMp-22Ti-18Si In-Situ Composites (in Japanese)"Nippon Kinzoku Gakkaishi (J. Jpn. Inst. Met.). 64[6]. 474-480 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Sha Jiang Bo, Hisatoshi Hirai, Tatsuo Tabaru, Akira Kitahara, Hidetoshi Ueno, Shuji Hanada: "Microstructure and Mechanical Properties of Nb-Mo-Ti-Si-C in-situ Composites Prepared by Arc Melting and Directional Solidification (in Japanese)"Nippon Kinzoku Gakkaishi (J. Jpn. Inst. Met.). 64[5]. 331-334 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] S.Hanada, W.Fang: "Superplasticity in Nb_3Al/Nb in-situ composites"Superplasticity-Current status and future. 601. 15-24 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] C.L.Ma, Y.Tan, H.Tanaka, A.Kasama, R.Tanaka, S.Miura, Y.Mishima, S.Hanada: "Phase Equilibria in Nb-Mo-Rich Zone of the Nb-Si-Mo Ternary System"Mater. Trans., JIM. 41. 1329-1336 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Naoya Masahashi, Sadao Watanabe, Shuji Hanada: "Microstructure and Oxidation Behavior of Low Pressure Plasma Sprayed Iron Aluminides"ISIJ International. Vol.41, No.9. 1010-1017 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Naoya Masahashi, Naoyuki Kondo, Sadao Watanabe, Shuji Hanada: "Composite Steel based on Iron Aluminides"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S. Hanada, Z. Zhong, S. W. Nam, and R. N. Wright, JIM, Sendai, Japan. 819-822 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Kyosuke Yoshimi, Shinya Nakatani, Tomokazu Suda, Shuji Hanada: "Strength and Oxidation of Mo_5SiB_2-based In-situ Composites at High Temperatures"Transactions of the Materials Research Society of Japan. 26[1]. 141-144 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Yuetsu Danzaki, Kazuaki Wagatsuma, Tsutomu Syoji, Kyosuke Yoshimi: "Dissolution of molybdenum-silicon (-boron) alloys using a mixture of sulfuric, nitric and hydrofluoric acids and a sequential correction method for ICP-AES analysis"Fresenius J Anal Chem. 369. 184-186 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Yoshimi, M.H.Yoo, A.A.Wereszczak, S.M.Borowicz, E.P.George, R.H.Zee: "Yielding and flow behavior of Mo_5Si_3 single crystals"Scripta Materialia. 45. 1321-1326 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Kyosuke Yoshimi, Shuji Hanada, Eiji Aoyagi: "Analysis of Protective Oxide Scale on Mo_5SiB_2-based Alloy Oxidized at High Temperature"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S.Hanada, Z.Zhong, S.W.Nam and R.N.Wright, JIM, Sendai, Japan. 975-978 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Shinya Nakatani, Kyosuke Yoshimi, Shuji Hanada, Se-Hyon Ko, Yong-Ho Park: "Design of Mo-Si-B-O Pseudo In-situ Composites for High Temperature Applications"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S.Hanada, Z.Zhong, S.W.Nam and R.N.Wright, JIM, Sendai, Japan. 971-974 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Kyosuke Yoshimi, Shuji Hanada: "Microstructures and Mechanical Properties of Eutectic Mo-XC (X=Ti, Zr, Hf) In-situ Composites"Transactions of the Materials Research Society of Japan. 26[1]. 307-310 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Naoya Masahashi, Shuji Hanada: "Microstructures and Fracture Toughness of Mo-Zrc Eutectic Composites"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S.Hanada, Z.Zhong, S.W.Nam and R.N.Wright, JIM, Sendai, Japan. 2763-2766 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Naoya Masahashi, Sadao Watanabe, Shuji Hanada: "Microstructure and Oxidation Behavior of Low Pressure Plasma Sprayed Iron Aluminides"ISIJ International. Vol.41 No.9. 1010-1017 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Naoya Masahashi, Naoyuki Kondo, Sadao Watanabe, Shuji Hanada: "Composite Steel based on Iron Aluminides"Proceedings of 4th Pacific Rim International Conference of AdvancedMaterials and Processing (PRICM 4), ed. by S. Hanada, Z. Zhong, S. W. Nam, and R. N. Wright, JIM. 819-822 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Kyosuke Yoshimi, Shinya Nakatani, Tomokazu Suda, Shuji Hanada: "Strength and Oxidation of Mo_5SiB_2-based In-situ Composites at High Temperatures"Transactions of the Materials Research Society of Japan. 26. 141-144 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Yuetsu Danzaki, Kazuaki Wagatsuma, Tsutomu Syoji, Kyosuke Yoshimi: "Dissolution of molybdenum-silicon (-boron) alloys using a mixture of sulfuric nitric and hydrofluoric acids and a sequential correction method for ICP-AES analysis"Fresenius J Anal Chem. 269. 184-186 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Yoshimi, M.H.Yoo, A.A.Wereszczak, S.M.Borowicz, E.P.George, R.H.Zee: "Yielding and flow behavior of Mo_5Si_3 single crystals"Scripta Materialia. 45. 1321-1326 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Kyosuke Yoshimi, Shuji Hanada, Eiji Aoyagi: "Analysis of Protective Oxide Scale on Mo_5SiB_2-based Alloy Oxidized at High Temperature"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S. Hanada, Z. Zhong, S. W. Nam and R. N. Wright, JIM. 975-978 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Shinya Nakatani, Kyosuke Yoshimi, Shuji Hanada, Se-Hyon Ko, Yong-Ho Park: "Design of Mo-Si-B-O Pseudo In-situ Composites for High Temperature Applications"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S. Hanada, Z. Zhong. S. W. Nam and R. N. Wright, JIM. 971-974 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Kyosuke Yoshimi, Shuji Hanada: "Microstructures and Mechanical Properties of Eutectic Mo-XC(X=Ti, Zr, Hf) In-situ Composites"Transactions of the Materials Research Society of Japan. 26. 307-310 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Teppei Suzuki, Hiroaki Matsumoto, Naoyuki Nomura, Naoya Masahashi, Shuji Hanada: "Microstructures and Fracture Toughness of Mo-ZrC Eutectic Composites"Proceedings of 4th Pacific Rim International Conference of Advanced Materials and Processing (PRICM 4), ed. by S. Hanada, Z.Zhong, S. W. Nam and R. N. Wright, JIM. 2763-2766 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] 松原学,岩崎敏彦,花田修治: "傾斜機能させたNb-Al/Al_2O_3皮膜のプラズマ溶射による作製"日本金属学会誌. 64. 677-683 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] C.L.Ma,A.Kasama,H.Tanaka,Y.Tan,R.Tanaka,Y.Mishima and S.Hanada,41(2000): "Microstructure and mechanical properties of Nb/Nb-silicide in-situ composites synthesized by reactive hot pressing of ball milled powders"Mater.Trans.,JIM. 41. 444-451 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 平井寿敏,田原竜夫,上野英俊,北原晃,花田修治: "一方向凝固したNb-xMo-22Ti-18Si系In-Situ複合材料の組織と機械的性質"日本金属学会誌. 64. 474-480 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 沙江波,平井寿敏,田原竜夫,北原晃,上野英俊,花田修治: "アーク溶解および一方向凝固法により作製したNb-Mo-Ti-Si-C系in-situ複合材料の組織と機械的性質"日本金属学会誌. 64. 331-334 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Hanada and W.Fang: "Superplasticity in Nb_3Al/Nb in-situ composites"Superplasticity-Current status and future. 601. 15-24 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] C.L.Ma,Y.Tan,H.Tanaka,A.Kasama,R.Tanaka,S.Miura,Y.Mishima and S.Hanada: "Phase equilibria in Nb-Mo-Rich Zone of the Nb-Si-Mo Ternary System"Mater.Trans.,JIM. 41. 1329-1336 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 1999-04-01   Modified: 2018-03-28  

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