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Development of Static and Fatigue Strength Characterization System for Composite Interface using In-situ Observation

Research Project

Project/Area Number 11555032
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Materials/Mechanics of materials
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

HOJO Masaki  Kyoto University, Dept. Mechanical Eng., Professor, 工学研究科, 教授 (70252492)

Co-Investigator(Kenkyū-buntansha) TANAKA Mototsugu  Guest Lecturer for Advanced Research, 工学研究科, 講師(研究機関研究員)
MATSUBARA Teruji  Shimadzu Co., Research & Development Dept., Group Head, 主任
OCHIAI Shojiro  Kyoto University, Mesoscopic Materials Res. Ctr., Professor, 工学研究科, 教授 (30111925)
フィードラー ボドー  京都大学, 大学院・工学研究科, 講師
Project Period (FY) 1999 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥6,400,000 (Direct Cost: ¥6,400,000)
Fiscal Year 2001: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2000: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 1999: ¥4,800,000 (Direct Cost: ¥4,800,000)
KeywordsComposite materials / Inter facial strength / Model composites / Mesoscopic structure / In-situ observation / Static strength / Fatigue strength / Numerical analysis
Research Abstract

Macroscopic fracture properties of fiber reinforced composite materials depend on the properties of mesoscopic components such as fiber, matrix, fiber/matrix interface and their spacial distribution. Then, the direct measurements of the fracture behavior of these mesoscopic components are important for the understanding of the fracture process in mesoscopic scale. In the present study, two types of model composites were used to evaluate the inter facial strength of glass fiber/epoxy composites. One is microcomposite, in which one central fiber was pulled out from six surrounding fibers was The other is couple fiber shear specimen, in which a pair of fibers was pulled away. The latter was specially designed for in-situ observation. Tests were carried out under static and fatigue loadings using low-load capacity fatigue testing machine attached to scanning electron microscope. Two and three dimensional finite element analyses were carried out to find out the mechanism and criterion of th … More e inter facial fracture.
The results are summarized as follows :
(1) In microcomposite tests, the fracture surface indicated the transition point of stable opening mode crack propagation to unstable shear mode crack propagation. This can be correlated to the maximum pullout load in the experiments. This condition can be expressed by the constant intensity of stress singularity without respect to the fiber diameter and the resin impregnated length.
(2) In couple fiber shear tests, in-situ observation showed stable crack growth before final unstable fracture. The three-dimensional finite element analysis indicated that the controlling mode of the fracture was mode I without respect to the crack length. The transition of stable to unstable crack growth was correlated to the minimum values of the mode I stress intensity factor with the crack length. .
(3) Couple fiber tests were carried out with fibers of different fiber diameters. The comparison of the results indicated that the above criterion was valid without respect to the fiber diameter.
(4) The tests were also carried out under fatigue loading with automated controlling and data acquisition systems. Less

Report

(4 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • 1999 Annual Research Report
  • Research Products

    (34 results)

All Other

All Publications (34 results)

  • [Publications] Masaki Hojo: "Interfacial Fracture in Model Composites under Static and Fatigue Loadings-Mechanism Consideration by Experimental and Analytical Approaches"Materials Science Research International. STP-2. 189-196 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masaki Hojo: "Interfacial Fracture of GF and CF/epoxy Model Composites under Static and Fatigue Loadings"Proc. 8th International Fatigue Congress, Fatigue 2002. (In press). (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masaki Hojo: "Mode II Interlaminar Properties under Static and Fatigue Loadings for CF/Epoxy Laminates with Different Fiber Surface Treatment"Advanced Composite Materials. 10. 237-246 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masaki Hojo: "Mode I and II Delamination Fatigue Crack Growth Behavior of Alumina Fiber/Epoxy Laminates in Nitrogen"International journal of Fatigue. 24. 109-118 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masaki Hojo: "Effect of Interface Control on Mode I Interlaminar Fracture Toughness of Woven C/C Composite Laminates"JSME International Journal, Ser. A.. 44. 573-581 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 牧野一成: "Push-out 試験での界面き列進展における母材弾性率の影響の数値解析およびその実験評価への応用"日本接着学会誌. 37,7. 266-272 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 落合庄治郎: "材料特性と材料選択,岩波講座,現代工学の基礎,材料系III"岩波書店. 162 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Hojo, M., Terashima, K., Igarashi, Y., Sfiida, M., ucnui, ic, T. and Suzuki, Y.: "Interfacial Fracture in Model Composites under Static and Fatigue Loadings -Mecnanism Consideration by Experimental and Analytical Approaches-"Materials Science Research International. STP-2. 189-196 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Hojo, M., Tanaka, M., Hobbiebrunken, T., Ochiai, s., inoue, T. and Sawada, Y.: "Inter facial Fracture of GF and CF/epoxy Model Composites under Static and Fatigue Loadings"Proc. 8th International Fatigu e Congress, Fatigue 2002, St ockholm. (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Hojo, M., Matsuda, S., Ochiai, S., Tsujioka, N., Nakanishi,Y, Maekawa, Z.and Murakami, A.: "Mode II Interlaminar Static and Fatigue Loadings for CF/Epoxy Laminates with Different Fiber Surface Treatment"Advanced Composite Material. Vol.10, Nos. 2-3. 237-246 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Hojo, M., Matsuda, S., Fiedler, B., Kawada, T., Moriya, K., Ochiai, S. and Aoyama, H.: "Mode I and II Delamination Fatigue Crack Growth Behavior of Alumina Fiber/Epoxy Laminates in Liquid Nitrogen"Int. J. of Fatigue. Vol.24, Nos,2-4. 109-118 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Hojo, M., Yamao, Tanaka, M., Ochiai, S., iwasnita, N. and Sawada, Y.: "Effect of Interface Control on Mode I Fiterlaminar Fracture Toughness of Woven C/C Composite Laminates"JSME International Journal, S er. A.. Vol.44. No.4. 573-581 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Makino, K., Igarasni, Y., inoue, I., hojo, M., lanaka, M. and Ochiai, S.: "Numerical Analysis of Effect of Matrix Modulus on ifiterfacial Crack Propagation and Its Application to Experimental Evaluation in Push-out Test"Journal of the Adhesion Society of Japan. Vol.37, No.7. 266-272 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Olchiai, S., Hojo, M., Fujita, S. and Itoh, Y.: "Materials Properties and Material Selection, Fundamentals of Modern Technology, Materials Vol. III"Iwanami Shoten Publishers. 162 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masaki Hojo: "Interfacial Fracture in Model Composites under Static and Fatigue Loadings-Mechanism Consideration by Experimental and Analytical Approaches"Materials Science Research International. STP-2. 189-196 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Masaki Hojo: "Effect of Interface Control on Mode I Interlaminar Fracture Toughness of Woven C/C Composite Laminates"JSME International Journal, Ser. A.. 44. 573-581 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Masaki Hojo: "Mode II Interlaminar Properties under Static and Fatigue Loadings for CF/Epoxy Laminates with Different Fiber Surface Treatment"Advanced Composite Materials. 10. 237-246 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Masaki Hojo: "Mode I and II Delamination Fatigue Crack Growth Behavior of Alumina Fiber/Epoxy Laminates in Nitrogen"International journal of Fatigue. 24. 109-118 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] Fiedler, B.: "FEM Modeling of the Initial Matrix Failulure in CFRP under Static Transverse Tensile Load"Composite Science and Technology. 61. 95-105 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Fiedler: "Failure Behavior of Epoxy Matrix under Different Kinds of Static Loading"Composite Science and Technology. 61. 1615-1624 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] 日本材料学会編: "材料と評価の最前線"培風館. 318 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Masaki Hojo: "Effect of Interface on Fracture Behavior of Woven C/C Composites"Int.J.of Materials and Product Technology. 16. 156-164 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Masaki Hojo: "Mode II Interlaminar Properties under Static and Fatigue Loadings for CF/Epoxy Laminates with Different Fiber Surface Treatment"Proc. Ninth United States-Japan Conference on Composite Materials. 291-298 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Masaki Hojo: "Effects of Interface Control and Heat-Treatment Temperature on Interlaminar Shear Strength and Mode II Interlaminar Fracture Toughness of Woven C/C Composites"Materials Science Research International. 7. 34-40 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 松田聡: "アイオノマーインターリーフ炭素繊維/エポキシ積層板のモードII層間破壊じん性"日本接着学会誌. 36. 45-52 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 田中基嗣: "一方向強化Si-Ti-C-O/BMAS複合材料の引張破壊挙動のその場観察およびシミュレーション"材料. 49. 502-505 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Masaki Hojo: "Mode II Static and Fatigue Delamination of Interlayer-Toughened CFRP in Air and in Water"Proc.of the Second Asian-Australasian Conference on Composite Materials. 987-992 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 落合庄治郎: "材料特性と材料選択,岩波講座,現代工学の基礎,材料系III"岩波書店. 162 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 北條正樹: "アルミナ繊維/エポキシ一方向積層板の室温大気中におけるモードI・II層間破壊じん性および疲労き裂伝ぱ"材料. 48. 1400-1407 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 北條正樹: "液体窒素中におけるアルミナ繊維/エポキシ積層板のモードII静的・疲労層間破壊"日本機械学会論文集,A編. 65. 2405-2410 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Masaki Hojo: "The Role of Interleaf/Base Lamina Interphase in Toughening Mechanism of Interleaf-Toughened CFRP"Proc. 12th International Conference on Composite Materials. (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Masaki Hojo: "Interlaminar Fracture Toughness and Delamination Fatigue of Alumina Giber/Epoxy Laminates in Air and in Liquid Nitrogen"Proceedings of 7th Euro-Japanese Symposium. 1-6 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] Satoshi Matsuda: "Effect of Ionomer Thickness on Mode I Interlaminar Fracture Toughness for Ionomer Toughened CFRP"Composites: Part A. 30. 1311-1319 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 松田聡: "CF/エポキシ積層板のモードII層間はく離疲労に及ぼす繊維表面処理の影響"材料. 48. 438-445 (1999)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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