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Fabrication and Properties of Metal-Coated SiTiCO Fiber-Reinforced Ti Matrix Composite

Research Project

Project/Area Number 11555174
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Structural/Functional materials
Research InstitutionUniversity of Tokyo

Principal Investigator

KAGAWA Yutaka  Institute of Industrial Science, University of Tokyo, Professor, 生産技術研究所, 教授 (50152591)

Co-Investigator(Kenkyū-buntansha) SATO Mitsuhiko  Research Laboratory, Ube Industries Co. Ltd., Researcher, 宇部研究所, 主席研究員
HONDA Koichi  Institute of Industrial Science, University of Tokyo, Research Associate, 生産技術研究所, 助手 (80092328)
中安 哲夫  宇部興産株式会社, 宇部研究所, 主任研究員
Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥13,800,000 (Direct Cost: ¥13,800,000)
Fiscal Year 2000: ¥6,200,000 (Direct Cost: ¥6,200,000)
Fiscal Year 1999: ¥7,600,000 (Direct Cost: ¥7,600,000)
KeywordsComposites / Metal coating / SiC fiber / Ti matrix / Interface / Reaction behavior / Mechanical properties / Fabrication / 表面改質とコーティング / SiC繊維強化Ti複合材料 / 金属間化合物 / 界面制御 / 真空ホットプレス / 繊維強化金属 / SiTiCO繊維 / SiTiCO繊維強化Ti複合材料 / 真空ホットプレス法
Research Abstract

The effect of the metal coatings on the tensile strength of the unidirectional SiTiCO fiber-reinforced commercially pure Ti matrix composites in an actual fabrication process was examined. Au coated SiTiCO fiber was incorporated into commercially pure Ti matrix by vacuum hot processing route. The thickness of Au coating was from 0.5 to 1.0 μm and coating was done on the surface of thin (0.1 μm) carbon-coated SiTiCO fiber by continuous electro-deposition process. The interface reaction (diffusion) behavior between coated fiber and Ti matrix after fabrication was examined and the tensile strength of the extracted fiber from Ti matrix was obtained.
It was found that Au coating effectively prevents reaction between SiTiCO fiber and Ti matrix by formation of intermetallic compound Au_xTi_y. This Au_xTi_y layer acts as a diffusion barrier between Ti and SiTiCO fiber. The tensile strength of the extracted fiber was only 10% lower than that of as received one. The interfacial mechanical properties were controlled by thin carbon coating layer and SiTiCO fiber surface. Effects of the thermal exposure on the interface properties was negligibly small. The formed Au_xTi_y also improves Young's modulus of the composite. The studies clearly demonstrated some advantages of the Au coating for SiTiCO fiber-reinforced Ti matrix composites.

Report

(3 results)
  • 2001 Final Research Report Summary
  • 2000 Annual Research Report
  • 1999 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] Y.c.Her, J.-M.Yang, Y.Kagawa: "Growth Behavior of Short Fatigue Cracks in a SCS-6/Ti Composite"Materials Science and Engineering A. 271. 407-415 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.-F.Liu, Y.Kagawa: "Finite Element Analysis of Debonding and Frictional Sliding in Fiber-Reinforced Brittle Matrix Composites : A Parametric Study"Materials Transactions, JIM. 40(12). 1343-1350 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Q.Guo, Y.Kagawa, A.Fukushima, C.Fujiwara: "Tensile Properties of Duplex Metal-Coated SiC Fiber and Titanium Alloy Matrix Composites"Metallurgical and Materials Transactions. 30A(11). 3019-3024 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] K.Sato, H.Kakisawa, Y.Kagawa, H.Kaya, O.Funayama, T.Isoda: "Reaction Between Newly-Developed Si_3N_4 Fiber and Various Ceramics"Journal of Materials Science Letters. 19. 1179-1183 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Q.Guo, Y.Kagawa, A.Fukushima, C.Fujiwara: "Effect of Cu/Ta Duplex Metal Coating on Interface Characterization in SiC Fiber-Reinforced Ti-15wt% V-3wt% Cr-3wt% Al-3wt% Sn Matrix Composite"Philosophical Magazine A. 80(2). 389-409 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Kakisawa, K.Honda, Y.Kagawa: "Effect of Wear on Interface Frictional Resistance in Fiber-Reinforced Composite-Model Experimental"Materials Science and Engineering A. 284. 226-234 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] A.Fukushima, C.Fujiwara, Y.Kagawa, C.Masuda: "Effect of Interfacial properties on Tensile Strength in SiC/Ti-15-3 Composites"Materials Science and Engineering A. 276. 243-249 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Kawazoe, Y.Kagawa, N.Takemura, H.Kakisawa: "Thermal Stress Distribution in Short Fiber-Reinforced Polymer Matrix Composite : Model Experiment and Simple Simulation"Journal of Materials Science Letters. 19. 2227-2229 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.C. Her. J.-M. Yang, and Y. Kagawa: "Growth Behavior of Short Fatigue Cracks in a SCS-6/Ti Composite"Materials Science and Engineering A. 271. 407-415 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.-F. Liu and Y. Kagawa: "Fiber-Reinforced Brittle Matrix Composites: A Parametric Study"Materials Transactions, JIM. 40(12). 1343-1350 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Q. Guo, Y. Kagawa, A. Fukushima, and C. Fujiwara: "Tensile Properties of Duplex Metal-Coated SiC Fiber and Titanium Alloy Matrix Composites"Metallurgical and Materials Transactions A. 30A(11). 3019-3024 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] K. Sato, H. Kakisawa, Y. Kagawa, H. Kaya, O. Funayama and T. Isoda: "Reaction Between Newly-Developed Si_3N_4 Fiber and Various Ceramics.,"Journal of Materials Science Letters. 19. 1179-1183 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Q. Guo, Y. Kagawa, A. Fukushima and C. Fujiwara: "Effect of Cu/Ta Duplex Metal Coating on Interface Characterization in SiC Fiber-Reinforced Ti-15wt% V-3wt% Cr-3wt% Al-3wt% Sn Matrix Composite"Philosophical Magazine A. 80(2). 389-409 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H. Kakisawa, K. Honda, Y. Kagawa: "Effect of Wear on Interface Frictional Resistance in Fiber-Reinforced Composite- Model Experimental"Materials Science and Engineering A. 284. 226-234 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] A. Fukushima, C. Fujiwara, Y. Kagawa and C. Masuda: "Effect of Interfacial properties on Tensile Strength in SiC/Ti-15-3 Composites"Materials Science and Engineering A. 276. 243-249 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S. Kawazoe, Y. Kagawa, N. Takemura, and H. Kakisawa: "Thermal Stress Distribution in Short Fiber-Reinforced Polymer Matrix Composite: Model Experiment and Simple Simulation"Journal of Materials Science Letters. 19. 2227-2229 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Q.Guo,Y.Kagawa,A.Fukushima and C.Fujiwara: "Effect of Cu/Ta duplex metal coating on interface characterization in SiC fiber-reinforced Ti-15wt%V-3wt%Cr-3wt%Al-3wt%Sn"matrix composite Philosophical Magazine. Vol.80,No.2. 389-409 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] Fukushima,C.Fujiwara,Y.Kagawa,C.Masuda: "Effect of interfacial properties on tensile strength in SiC/Ti-15-3 composites"Materials Science and Engineering : A. 276(1-2). 243-249 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.kawazoe,Y.Kagawa,N.Takemura and H.Kakisawa: "Thermal stress distribution in short fiber-reinforced polymer matrix composite : Model experiment and simple estimation"Materials Science and Technology. (印刷中).

    • Related Report
      2000 Annual Research Report
  • [Publications] Y.Tanaka,Y.Kagawa,C.Masuda,Y.F.Liu and S.Q.Guo: "Observation of Fatigue Damage Process in SiC Fiber-Reinforced Ti-15-3 Composite at High Temperature"Metallurgical and Materials Transactions A. Vol.30A・No.1. 221-229 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] S.Q.Guo,Y.Kagawa,A.Fukushima and C.Fujiwara: "Interface Characterization of Duplex Metal-Coated SiC Fiber-Reinforced Ti-15-3 Matrix Composite"Metallurgical and Materials Transactions A. Vol.30A・No.3. 653-666 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] S.Q.Guo,Y.Kagawa,A.Fukushima and C.Fujiwara: "Tensile Properties of Duplex Metal-Coated SiC Fiber and Titanium Alloy Matrix Composites"Metallurgical and Materials Transactions A. Vol.30A・No.11. 3019-3024 (1999)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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