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Atomic Force Microscopic Observation on the Surface Morphology of Polycrystalline Materials

Research Project

Project/Area Number 11640325
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 固体物性Ⅰ(光物性・半導体・誘電体)
Research InstitutionIWAKI MEISEI UNIVERSITY

Principal Investigator

TAKASHIGE Masaaki  FACULTY OF SCIENCE AND ENGINEERING, DEPARTMENT OF ELECTRONICS, IWAKI MEISEI UNIVERSITY PROFESSOR, 理工学部, 教授 (70114527)

Co-Investigator(Kenkyū-buntansha) HAMAZAKI Shinichi  FACULTY OF SCIENCE AND ENGINEERING, IWAKI MEISEI UNIVERSITY RESERCH ASSOCIATE, 理工学部, 助手 (20306096)
SHIMIZU Fuminao  FACULTY OF SCIENCE AND ENGINEERING, DEPARTMENT OF ELECTRONICS, IWAKI MEISEI UNIVERSITY LECTURER, 理工学部, 講師 (20206212)
Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2000: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1999: ¥3,000,000 (Direct Cost: ¥3,000,000)
Keywordsdomain / ferroelectric / ferroelastic / AFM / barium titanate / rochelle salt / lead titanate / tungsten oxide / AFM / 非晶質 / 分域
Research Abstract

We applied atomic force microscopy (AFM) for the observation about surface structure of the following five polycrystalline materials, BaTiO_3, NaKC_4H_4O_64H_2O (Rochelle salt), WO_3, PbTiO_3 and Bi_4Ti_3O_<12>.
For multi-domain samples of BaTiO_3, NaKC_4H_4O_64H_2O and WO_3, temperature dependent surface images were investigated. Namely, the topographic images in the creation and disappearance process of 90 degree domains in BaTiO_3, monoclinic domains in NaKC_4H_4O_64H_2O and triclinic domains in WO_3 were taken with variation of temperature including their phase transition tmepratures.
For PbTiO_3 and Bi_4Ti_3O_<12>, the crystallization processes from the amorphous state were investigated. The initial state of these samples is in the amorphous state prepared by rapid quenching. The topographic images in the crystallized samples by annealing at several different temperatures were taken. In this case, the visualization of the surface hardness was also made using the force modulation mode.

Report

(3 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] S.I.Hamazaki他3名: "Observation of Crystallization Process from Amorphous PbTiO_3 by Scanning Probe Microscope"Journal of Korean Physcial Society. 35. 1145-1147 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige他4名: "Temperature Dependent Surface Image of BaTiO_3 Observed by Atomic Force Microscopy "Japanese Journal of Applied Physics. 38. 5686-5688 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige他6名: "Observation of Crystallization Process from Amorphous Bi_4Ti_3O_<12> Prepared by Rapid Quenching Method"Japanese Journal of Applied Physics. 39. 5716-5718 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige他3名: "Temperature Dependent Surface Images of Barium Titanate and Rochelle Salt Observed Atomic Force Microscopy"Ferroelctrics. 240. 93-100 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.I.Hamazaki他3名: "Temperature Dependent Surface Images of Several Ferroic Crystals Observed by Scanning Probe Microscopy"Ferroelectrics. 掲載決定済み. (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige他5名: "Study of Crystallization from Amorphous State of Ferroelectric Oxides by Scanning Probe Microscopy"Ferroelectrics. 掲載決定済み. (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al: "AFM Observation of Domains of WO_3"Ferroelectrics. 231. 43-47 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige et al: "Temperature Dependent Surface Images of BaTiO_3 Observed by Atomic Force Microscopy"Jpn.J.Appl.Phys.. 38. 686-5688 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.I.Hamazaki et al: "Observation of Crystallization Process from Amorphous PbTiO_3 by Scanning Probe Microscope"J.Kor.Phys.Soc.. 35. 145-1147 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige et al: "Temperature Dependent Surface Images of Barium Titanate and Rochelle Salt Observed by Atomic Force Microscopy"Ferroelectrics. 240. 93-100 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige et al: "Observation of Crystallization Process from Amorphous Bi_4Ti_3O_<12> Prepared by Rapid Quenching Method"Jpn.J.Appl.Phys.. 39. 5716-5718 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Hamazaki et al: "Temperature Dependent Surface Images of Several Ferroic Crystals Obeserved by Scanning Probe Microscopy"Ferroelectrics. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige et al: "Study of Crystallization from Amorphous State of Ferroelectric Oxides by Scanning Probe Microscopy"Ferroelectrics. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S-I.Hamazaki et al: "Observation on Creation and Disappearance of 90°Domain in BaTiO_3 by Scanning Probe Microscopy"Ferroelectrics. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Takashige 他6名: "Observation of Crystallization Process from Amorphous Bi_4Ti_3O_<12> Prepared by Rapid Quenching Method"Japanese Journal of Applied Physics. 39. 5716-5718 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Takashige 他3名: "Temperature Dependent Surface Images of Barium Titanate and Rochelle Salt Observed by Atomic Force Microscopy"Ferroelctrics. 240. 93-100 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.I.Hamazaki 他3名: "Temperature Dependent Surface Images of Several Ferroic Crystals Observed by Scanning Probe Microscopy"Ferroelectrics. (掲載決定済み). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] M.Takashige 他5名: "Study of Crystallization from Amorphous State of Ferroelectric Oxides by Scanning Probe Microscopy"Ferroelectrics. (掲載決定済み). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] S. I. Hamazaki et al: "Observation of Crystallization Process from Amorphous Pb Ti O_3 by Scanning Probe Microscopy"J. kor. Phys. Soc.. 35. 1145-1147 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M. Takashige et al: "Temperature dependent Surface Images of BaTiO_3 Observed by Atomic force Microscopy"Jpn. J. Appl. Phys.. 38. 5686-5689 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] M. Takashige et al: "Temperature dependent Surface Images of Barium titanato and Rochelle salt observed by Atomic Force Microscopy"Ferroelectrics. (掲載決定).

    • Related Report
      1999 Annual Research Report
  • [Publications] F. Shimizu et al: "Dielectric and Phase Transitional Properties of A_2BX_4-Type Halides (A=K, Rb, Tl; B=Zn, Co; X=Br, I)"Ferroelectrics. (掲載決定).

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2020-05-15  

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