| Project/Area Number |
11650055
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| Research Category |
Grant-in-Aid for Scientific Research (C)
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| Allocation Type | Single-year Grants |
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| Section | 一般 |
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| Research Field |
Applied physics, general
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| Research Institution | Nagoya University |
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Principal Investigator |
HANAI Takaaki Nagoya University, Graduate School of Engineering, Lecturer (00156366)
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| Co-Investigator(Kenkyū-buntansha) |
TANAKA Shigeyasu Nagoya University, Graduate School of Engineering, Research Associate (70217032)
MUROOKA Yoshie Nagoya University, Graduate School of Engineering, Research Associate (40273263)
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| Project Period (FY) |
1999 – 2000
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| Project Status |
Completed (Fiscal Year 2000)
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| Budget Amount *help |
¥3,500,000 (Direct Cost: ¥3,500,000)
Fiscal Year 2000: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1999: ¥2,500,000 (Direct Cost: ¥2,500,000)
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| Keywords | Foil Lens / Spherical Aberration / Correction / Electron Lens / Electron Microscopy / Resolution / 球面収差補正 / 対物レンズ / 5次球面収差 / 高分解能 / 超高分解能 |
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| Research Abstract |
1. Development of a foil lens for the objective lens of a transmission electron microscope (TEM).
In order to design the foil lens which enables us to correct the spherical aberration at a lower electrostatic field than 120 kV/mm, that is the known limit of self-supporting of the foil electrode, optical characteristics of the foil lens were numerically studied. It was found that that the correction is achieved by locating the foil lens at the position 3.6 mm lower from the center of the gap of the objective polepieces. The spherical aberration is corrected at the foil lens voltage of 550 V when the distance of the aperture and foil electrodes. An improved side-entry type foil lens was developed based on the calculation. The foil lens holder has the thickness of 1.7 mm, 0.3 mm thinner than previous one.
2. Observation of crystal lattice images with the improved foil lens.
The foil lens was incorporated with a commercial TEM and the images of Au fine particles were observed at the accelerating voltage of 200 kV. At the foil lens voltage of 300 V, (111) lattice images were observed at nearly in-focus condition where the contrast of the Fresnel fringe was weak. Such reduction of aretefacts shows an effect of correction of spherical aberration.
3. Measurements of spherical aberration of the corrected objective lens.
The spherical aberration was measured with a newly developed method, in which the spherical aberration coefficient and the defocus are simultaneously determined from the deviation of the dark-field TEM images of Au particles from the corresponding bright-field image. It was shown that the improved foil lend yields smaller spherical aberration coefficients than the previous one at the same foil lens voltage.
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