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Laser-Raman Measurement and Analytical Evaluation of Matrix Creep Induced Stress Relaxation in Broken Fibers

Research Project

Project/Area Number 11650086
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionNagoya University

Principal Investigator

OHNO Nobutada  Grad. School of Eng., Nagoya Univ., Professor, 工学研究科, 教授 (30115539)

Co-Investigator(Kenkyū-buntansha) BIWA Shiro  Grad. School of Eng., Nagoya University, Lecturer, 工学研究科, 講師 (90273466)
Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2000: ¥1,300,000 (Direct Cost: ¥1,300,000)
Fiscal Year 1999: ¥2,400,000 (Direct Cost: ¥2,400,000)
KeywordsComposite Material / Creep / Raman Spectroscopy / Variational Method / Fiber Breakage / Fiber Pull-Out / レーザラマン
Research Abstract

Unidirectional metal-matrix and polymer-matrix composites reinforced forced with long brittle fibers may suffer from creep rupture under constant applied stress, since the stress in broken fibers is relaxed with time. In the present work, laser-Raman stress measurement and analytical evaluation were performed to investigate such stress relaxation, resulting in the following findings :
1. Fiber pull-out tests were done using single-fiber model composites for the purpose of clarifying the effect of matrix creep on the stress profile of fiber stress. The stress of carbon fibers embedded in polymers was measured by means of Raman spectroscopy. Three kinds of polymer matrices, i.e., normal epoxy, flexible epoxy and UV-curable acrylic, were employed. It turned out that the profile of fiber stress changes with time more markedly if the matrix creeps more significantly.
2. Moreover, the stress relaxation in broken fibers was measured using single-fiber model composites and Raman spectroscopy. It was found that the stress relaxation in broken fibers also occurs more markedly if the matrix creeps more significantly.
3. A functional based on complementary energy was presented in an incremental form. It was shown that the functional has a stationary function satisfying a shear lag differential equation. Then, by employing the bilinear approximation of fiber stress profiles, analytical solutions for axisymmetric fiber breakage and fiber pull-out models were obtained from the stationary condition.
4. The analytical solutions mentioned above were applied to the present experimental results. The creep constants were identified from creep tests of the polymers employed. It was thus shown that the analytical solutions represent well the tendencies observed in the experiments.

Report

(3 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • Research Products

    (14 results)

All Other

All Publications (14 results)

  • [Publications] 三宅卓志: "定荷重繊維引抜き試験における繊維応力分布の時間変化のラマン分光による評価"日本機械学会論文集(A編). 66・643. 464-471 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 大野信忠: "母材クリープを有する一方向繊維強化複合材の繊維応力分布解析に対する変分法"日本機械学会論文集(A編). 66・643. 472-479 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno: "A Variational Method for Fiber Stress Profiles in Unidirectional Composites with Matrix Creep"Key Engineering Materials. 177-180. 315-320 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno: "Effects of Matrix Creep on Fiber Stress Profiles in Unidirectional Composites : Mesoscopic Analysis Based on a Variational Method"Proceeding of IUTAM Symposium on Creep in Structures (Kluwer Academic Publishers). 439-452 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Miyake S.Kokawa and N.Ohno: "Evaluation of Time-Dependent Change of Fiber Stress Profiles in Constant Load Single-Fiber Pull-Out Tests Using Raman Spectroscopy"Transactions of JSME, Ser.A. 66-643 (in Japanese). 464-471 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno, T.Ando, T.Miyake and S.Biwa: "A Variational Method for Analysis of Fiber Stress Profiles in Unidirectional Composites with Matrix Creep"Transactions of JSME, Ser.A. 66-643 (in Japanese). 472-479 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno, T.Ando, T.Miyake and S.Biwa: "A Variational Method for Fiber Stress Profiles in Unidirectional Composites with Matrix Creep"Key engineering Materials. 170-180. 315-320 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno, T.Ando, T.Miyake and S.Biwa: "Effects of Matrix Creep on Fiber Stress Profiles in Unidirectional Composites Mesoscopic Analysis Based on a Variational Method"Proceeding of IUTAM Symposium on Creep in Structures (Kluwer Academic Publishers). 439-452 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Ohno: "Effects of Matrix Creep on Fiber Stress Profiles in Unidirectional Composites : Mesoscopic Analysis Based on a Variational Method"Proceeding of IUTAM Symposium on Creep in Structures (Kluwer Academic Publishers). 439-452 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 大野信忠: "母材クリープを有する一方向繊維強化複合材の繊維応力分布解析に対する変分法"日本機械学会論文集(A編). 66・643. 472-479 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] N.Ohno: "A Variational Method for Fiber Stress Profiles in Unidirectional Composites with Matrix Creep"Key Engineering Materials. 177-180. 315-320 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] N.Ohno: "Effects of Matrix Creep on Fiber Stress Profiles in Unidirectional Composites : Mesoscopic Analysis Based on a Variational Method"Proceeding of IUTAM Symposium on Creep in Structures (Kluwer Academic Publishers). 439-452 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 三宅卓志: "定荷重繊維引抜き試験における繊維応力分布の時間変化のラマン分光による評価"日本機械学会論文集(A編). 66・643(印刷中). (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 大野信忠: "母相クリープを有する一方行繊維強化複合材の繊維応力分布解析に対する変分法"日本機械学会論文集(A編). 66・643(印刷中). (2000)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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