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Study on low temperature and high deposition rate preparation method of Cobalt containing ferrite thin-film media using ECR sputtering

Research Project

Project/Area Number 11650349
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 電子デバイス・機器工学
Research InstitutionYamaguchi University

Principal Investigator

YAMAMOTO Setsuo  Yamaguchi University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (30182629)

Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥3,100,000 (Direct Cost: ¥3,100,000)
Fiscal Year 2000: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 1999: ¥2,000,000 (Direct Cost: ¥2,000,000)
Keywordselectron cyclotron resonance / sputtering method / low temperature / ferrite / magnetic recording / magnetic media / high rate deposition / thin-film / スパッタ成膜 / コバルト含有酸化鉄薄膜 / 酸化鉄薄膜 / フェライト薄膜 / ECRスパッタ法 / 磁気ディスク / 磁気テープ
Research Abstract

In a conventional fabrication method of cobalt containing γ-Fe_2O_3 thin-film magnetic recording media, processing temperature higher than 250 degrees centigrade and two step fabrication process, that is sputter-deposition of CoO-Fe_3O_4 thin-films and transformation to Cobalt containing γ-Fe_2O_3 thin-films by annealing in air were necessary. In this study, novel sputtering using reactive and dense microwave plasma generated by electron-cyclotron-resonance (ECR phenomena) was introduced to achieve low-temperature and one step fabrication of these media. It was proved that the cobalt containing spinel ferrite thin-film media with a coercivity higher than 3000 Oe, well crystal orientation and very smooth surface (Ra is 0.2 to 0.4 nm) can be fabricated by using reactive ECR sputtering method at a low processing temperature (room temperature to 150 degrees centigrade) without any post oxidation processes.
Recording and reproducing operation using inductive/MR merged flying head showed the cobalt containing ferrite thin-film media fabricated by the reactive ECR sputtering are utilizable without deposition of protective overlayer and surface polishing. Also, cobalt containing ferrite thin-films with high coercivity of about 2000 Oe were successfully deposited on organic flexible substrate such as PET and polyimide films by using ECR sputtering method. This experiment showed that application of the ferrite thin-films to the tape media was feasible. An ECR sputtering apparatus with high deposition rate was designed and developed.
To summarize, the research goal of this study which was to develop low temperature and high rate fabrication method of ferrite thin-film media was satisfactorily achieved.

Report

(3 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • Research Products

    (42 results)

All Other

All Publications (42 results)

  • [Publications] Setsuo Yamamoto: "High Coercivity Ferrite Thin-Film Tape Media for Perpendicular Recording"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "High Rate Deposition of Co-Cr Perpendicular Magnetic Anisotropy Films by ECR Sputtering"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Fabrication of High-Permeability Ferrite by Spark-Plasma-Sintering Method"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 山本節夫: "垂直および長手記録方式に対応可能な酸化鉄薄膜メディア"日本応用磁気学会誌. 23・5. 1739-1745 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Mn-Zn Ferrite Fabricated by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Fabrication of Ferrite/Permalloy Laminated Core by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 山本節夫: "放電プラズマ焼結法による軟磁性コア材の作製"粉体および粉末冶金. 47・7. 757-762 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 山本節夫: "ECRスパッタ法で作製したCo-Cr-Ta垂直磁気ディスク"日本応用磁気学会誌. 23・S2. 55-58 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 千々松孝: "チタン製真空容器の真空特性"真空. 42・3. 200-203 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Development of small height inductors for DC-DC converter"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Small height inductor for DC-DC converter"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 山本節夫: "平坦化したフェライト基板に作製した薄膜インダクタ"粉体および粉末冶金. 48・2. 150-154 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "Preparation of ferrite thin-film media by ECR sputtering"IEICE transactions on Electronics. September(発表予定). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "High Coercivity Ferrite Thin-Film Tape Media for Perpendicular Recording"Journal of Magnetism and Magnetic Materials. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "High Rate Deposition of Co-Cr Perpendicular Magnetic Anisotropy Films by ECR Sputtering"Journal of Magnetism and Magnetic Materials. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Fabrication of High-Permeability Ferrite by Spark-Plasma-Sintering Method"Journal of Magnetism and Magnetic Materials. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Co-γ Fe_2O_3/NiO Thin-Film Media for Perpendicular and Longitudinal Magnetic Recording"Journal of the Magnetics Society of Japan. Vol.23, No.5. 1739-1745 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Mn-Zn Ferrite Fabricated by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Fabrication of Ferrite/Permalloy Laminated Core by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Fabrication of Soft Magnetic Core Using Spark Plasma Sintering"Journal of the Japan Society of Powder and Powder Metallurgy. Vol.47, No.7. 757-762 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "ECR-sputter-deposited Co-Cr-Ta perpendicular recording disk"Journal of the Magnetics Society of Japan. Vol.23, No.S2. 55-58 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Takashi CHIJIMATSU: "Vacuum Characteristics of Titanium Chamber"Journal of Vacuum Society of Japan. Vol.42, No.3. 200-203 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Development of small height inductors for DC-DC converter"Proceedings of the 8^<th> International Conference on Ferrite. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Small height inductor for DC-DC converter"Prcoeedings of the 8^<th> International Conference on Ferrite. (in press). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Thin-Film Inductor Micro-Formed on Smoothed Ferrite Substrate"Journal of the Japan Society of Powder and Powder Metallurgy. Vol.48, No.2. 150-154 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo YAMAMOTO: "Preparation of ferrite thin-film media by ECR sputtering"IEICE transactions on Electronics. (to be published). (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] Setsuo Yamamoto: "High Coercivity Ferrite Thin-Film Tape Media for Perpendicular Recording"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "High Rate Deposition of Co-Cr Perpendicular Magnetic Anisotropy Films by ECR Sputtering"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "Fabrication of High-Permeability Ferrite by Spark-Plasma-Sintering Method"Journal of Magnetism and Magnetic Materials. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 山本節夫: "垂直および長手記録方式に対応可能な酸化鉄薄膜メディア"日本応用磁気学会誌. 23・5. 1739-1745 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "Mn-Zn Ferrite Fabricated by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "Fabrication of Ferrite/Permalloy Laminated Core by Spark Plasma Sintering"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 山本節夫: "放電プラズマ焼結法による軟磁性コア材の作製"粉体および粉末冶金. 47・7. 757-762 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 山本節夫: "ECRスパッタ法で作製したCo-Cr-Ta垂直磁気ディスク"日本応用磁気学会誌. 23・S2. 55-58 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 千々松孝: "チタン製真空容器の真空特性"真空. 42・3. 200-203 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "Development of small height inductors for DC-DC converter"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Setsuo Yamamoto: "Small height inductor for DC-DC converter"Proceedings of the 8^<th> International Conference on Ferrite. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 山本節夫: "平坦化したフェライト基板に作製した薄膜インダクタ"粉体および粉末冶金. 48・2. 150-154 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 山本節夫: "酸素イオン照射によるCo含有酸化鉄薄膜メディアの作製"日本応用磁気学会誌. 23・4-2. 1021-1024 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 山本節夫: "垂直および長手記録方式に対応可能な酸化鉄薄膜メディア"日本応用磁気学会誌. 23・5. 1739-1745 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 千々松孝: "チタン製真空容器の真空特性"真空. 42・3. 200-203 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 山本節夫: "ECRスパッタ法で作製したCo-Cr-Ta垂直磁気ディスク"日本応用磁気学会誌. 23・S2. 55-58 (1999)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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