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In-situ X-ray Diffraction Study of Hydrogen Atoms in Metals and Semiconductors

Research Project

Project/Area Number 11650685
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

TSUKUDA Noboru  Reseach Institute for Applied Mechanics, KYUSHU UNIVERSITY Ass.Prof., 応用力学研究所, 助教授 (90038563)

Co-Investigator(Kenkyū-buntansha) KURAMOTO Eiichi  Reseach Institute for Applied Mechanics, KYUSHU UNIVERSITY Prof, 応用力学研究所, 教授 (30013519)
Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥3,400,000 (Direct Cost: ¥3,400,000)
Fiscal Year 2000: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1999: ¥2,900,000 (Direct Cost: ¥2,900,000)
KeywordsHydrogen / In-situ X-ray diffraction / Metals / Diffusion / Lattice Parameter / Hydride / in situ measurement / lattice parameter / X ray diffraction / hydrogen charging / Pd / Ni
Research Abstract

A device for in-situ X-ray diffraction measurements during cathodic hydrogen charging has been developed. Diffracted X-rays are detected through 0.3 mm thick H_2SO_4 flow. The charging current is 1-100 mA/cm^2. The change of lattice parameter for Pd during hydrogen charging and after charging has been clearly demonstrated. Diffusion coefficient of hydrogen atoms in Pd was determined by the time dependence of the lattice parameter and is 3x10^<-7> cm^2s^<-1> at 295K The device is widely applicable for understanding metal-hydrogen systems under various constrained hydrogen environments

Report

(3 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • Research Products

    (16 results)

All Other

All Publications (16 results)

  • [Publications] 古賀三井,蔵元英一,佃昇: "時間分割X線回折法の開発"九大総理工報告. 21. 333-336 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Ohkubo,S.Sugiyama,K.Fukuzono,M.Takenaka,N.Tsukuda,E.Kuramot: "Positron-lifetime Study of Electrically Hydrogen Charged Ni, austenitic stainless Steel and Fe"J.Nucl.Mater.. 283-287. 858-862 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Sugiyama,H.Ohkubo,M.Takenaka,K.Ohsawa,N.Tsukuda,E.Kuramoto: "The Effect of Electrical Hydrogen Charging on the Strength of 316 Stainless Steel"J.Nucl.Mater.283-287,863-867 (2000).. 283-287. 863-867 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Onitsuka,H.Ohkubo,M.Takenaka,N.Tsukuda,E.Kuramoto: "Positron Lifetime Calculation for Defects and Defect Clusters in Graphite"J.Nucl.Mater.. 283-287. 922-926 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Tsukuda,K.Itoh,N.Morioka,H.Ohkubo,E.Kuramoto: "In situ Measurement of Lattice Parameter Change on Pd and Ni during Cathodic Hydrogen Charging"J.Alloys and Compounds 293-295,174-177 (1999).. 174-177. 174-177 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Ohkubo, S.Sugiyama, K.Fukuzono, M.Takenaka, N.Tsukuda, E.Kuramoto: "Positron-lifetime Study of Electrically Hydrogen Charged Ni, austenitic stainless Steel and Fe"J.Nucl.Mater. 283-287. 858-862 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Sugiyama, H.Ohkubo, M.Takenaka, K.Ohsawa, N.Tsukuda, E.Kuramoto: "The Effect of Electrical Hydrogen Charging on the Strength of 316 Stainless Steel"J.Nucl.Mater. 283-287. 863-867 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Onitsuka, H.Ohkubo, M.Takenaka, N.Tsukuda, E.Kuramoto: "Positron Lifetime Calculation for Defects and Defect Clusters in Graphite"J.Nucl.Mater. 283-287. 922-926 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] M.Koga, E.Kuramoto, N.Tsukuda: "Development of a Time-resolved X-ray Diffractometry"Rep.Interdis.Eng.Sci., Kyushu Univ.. 21. 333-336 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] N.Tsukuda, K.Itoh, N.Morioka, H.Ohkubo, E.Kuramoto: "In situ Measurement of Lattice Parameter Change on Pd and Ni during Cathodic Hydrogen Charging"J.Alloys and Compounds. 293-295. 174-177 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 古賀三井,蔵元英一,佃昇: "時間分割X線回折法の開発"九大総理工報告. 21. 333-336 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Ohkubo,S.Sugiyama,K.Fukuzono,M.Takenaka,N.Tsukuda,E.Kuramot: "Positron-lifetime Study of Electrically Hydrogen Charged Ni,austenitic stainless Steel and Fe"J.Nucl.Mater.. 283-287. 858-862 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Sugiyama,H.Ohkubo,M.Takenaka,K.Ohsawa,N.Tsukuda,E.Kuramoto: "The Effect of Electrical Hydrogen Charging on the Strength of 316 Stainless Steel"J.Nucl.Mater.. 283-287. 863-867 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Onitsuka,H.Ohkubo,M.Takenaka,N.Tsukuda,E.Kuramoto: "Positron Lifetime Calculation for Defects and Defect Clusters in Graphite"J.Nucl.Mater.. 283-287. 922-926 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] N.Tsukuda,K.Itoh,N.Morioka,H.Ohkubo,E.Kuramoto: "In situ Measurement of Lattice Parameter Change on Pd and Ni during Cathodic Hydrogen Charging"J.Alloys and Compounds. 293-295. 174-177 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] N.Tsukuda: "In situ measurement of lattice parameter change on Pd and Ni during cathodic hydrogen charging"J. Alloys and Compounds. 293. 295. 174-177 (1999)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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