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Investigation of ductile-to-brittle transitions on ultra-precision machining of single crystal silicon

Research Project

Project/Area Number 11650753
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionHiroshima Kokusai Gakuin University

Principal Investigator

SUMOMOGI Tsunetaka  Hiroshima Kokusai Gakuin University, Faculty of Engineering, Professor, 工学部, 教授 (10136129)

Co-Investigator(Kenkyū-buntansha) ENDO Toshiro  Hiroshima Kokusai Gakuin University, Faculty of Engineering, Professor, 工学部, 教授 (60069200)
NAKATA Mikiko  Hiroshima Kokusai Gakuin University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (60237302)
SAKAI Hisashi  Hiroshima Kokusai Gakuin University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (70170561)
Project Period (FY) 1999 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥2,800,000 (Direct Cost: ¥2,800,000)
Fiscal Year 2000: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 1999: ¥2,100,000 (Direct Cost: ¥2,100,000)
Keywordsnano-scale machining / ductile mode machining / single crystal silicon / ductile-brittle transition / surface crack / subsurface crack / scanning force microscope / scanning laser microscope / 超微細胞加工 / ぜい性材料 / ダイヤモンド工具 / 原子間力顕微法
Research Abstract

The studies on nano-scale machining of brittle materials such as silicon and glass, have come into notice in recent years. A material removal with plastic deformation, known as ductile mode machining, has been achieved by a very small depth of cut. When surface cracks occurred with being increased the depth of cut, the machining has been commonly considered to be brittle mode. The workpiece materials used in the present experiment was single crystal silicon with (100) surface. A single crystal Vickers diamond pyramid indentor with an apex angle of 136° was used as the cutting tool. The ultra precision turning machine consists of an aerostatic bearing spindle for workpiece revolution and a roller bearing slide for tool feed. Face-turning of the workpiece was done from the center to the outside with a constant cutting speed between 150 m/min and 1500 m/min and a constant feed rate of 0.03 mm/revolution, and a spiral groves were formed. An inclination was given to the mounted workpiece by a partly inserted spacer between the workpiece and the chuck surface in order to generate various depth of grooves. The ductile-brittle transition points were examined by the observations not only on the surface cracks but also on the subsurface cracks. The scanning force microscope is used for measuring the depth of the grooves and observing the surface cracks. The distance from the surfaces to the deepest point of the subsurface cracks on obliquely sectioned and then etched surfaces are measured by the. The subsurface cracks are generated under the cutting grooves in some case, even if the depth is less than the ductile-brittle transition point based on the surface cracks. It is detected that the ductile-brittle transition point determined by the subsurface cracks is shallower than that determined by the surface cracks. Therefore the evaluation of the subsurface cracks would be important especially in finishing.

Report

(3 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] T.Sumomogi et al: "Nanotribological Effects due to the presence of water in Scanning Force Microscope"Proceedins of STM/STS '99,July 18-23,1999,Seoul, Korea. 427-428 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Kaji et al: "The study of ductile-brittle transition on micro-cutting of single crystal silicon"Proceedings of 14^<th> ASPE, Oct.31-Nov.5,1999,Monterey, USA. 107-110 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi et al: "Study of Nano-tribology using Scanning Force Microscope"Proceedings of 14^<th> ASPE, Oct.31-Nov.5,1999,Montery, USA. 424-427 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Endo et al: "STM Study on Nanostructures of Au and Al Deposits on HOPG and Amorphous Carbon"Materials Transactions, JIM. 40. 903-906 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 中村格芳 他: "単結品シリコンの延性モード切削加工に関する研究"広島国際学院大学研究報告. 32. 51-58 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi et al: "Evaluation of surface and subsurface cracks on nano-scale machined single crystal silicon by scanning force microscope and scanning laser microscope"Materials Characterization. (印刷中). (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi, T.Endo and S.Matsuo: "Nanotribological Effects due to the presence of water in Scanning Force Microscopy"Preliminary Proceedings of STM '99 (10th International Conference on Scanning Tunneling Microscopy/Spectroscopy and Related Proximal Probe Microscopy), Seoul, Korea, July 19-23. 427-428 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fujiyama, T.Sumomogi and T.Endo: "Effect of O_2 gas on grain size and mechanical properties of SiO_2 films by RF magnetron sputtering"Preliminary Proceedings of STM '99 (10th International Conference on Scanning Tunneling Microscopy/Spectroscopy and Related Proximal Probe Microscopy), Seoul, Korea, July 19-23. 429-430 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] S.Kaji, T.Goto, T.Sumomogi and M.Nakamura: "The study of ductile-brittle transition on micro-cutting of single crystal silicon"Proceedings of ASPE 1999 Annual Meeting, Monterey, USA. 107-110 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi, T.Endo and S.Matsuo: "Study of Nano-tribology using Scanning Force Microscope"Proceedings of ASPE 1999 Annual Meeting, Monterey, USA. 424-427 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Endo, T.Sumomogi, M.Nakata S.Ohara and H.Fujita: "STM Study on Nanostructures of Au and Al Deposits on HOPG and Amorphous Carbon"Materials Transactions, JIM. 40. 903-906 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi, M.Nakamura, T.Endo, T.Goto and S.Kaji: "Evaluation of surface and subsurface cracks on nano-scale machined single crystal silicon by scanning force microscope and scanning laser microscope"Materials Characterization. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Sumomogi et al: "Nanotriblogical Effects due to the presence of water in Scanning Force Microscope"Proceedings of STM/STS '99, July 18-23, 1999, Seoul, Korea. 427-428 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Kaji et al: "The study of ductile-brittle transition on micro-cutting of single crystal silicon"Proceedings of 14^<th> ASPE, Oct.31-Nov.5, 1999, Monterey, USA. 107-110 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Sumomogi et al: "Study of Nano-tribology using Scanning Force Microscope"Proceedings of 14^<th> ASPE, Oct.31-Nov.5, 1999, Monterey, USA. 424-427 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Endo et al: "STM Study on Nanostructures of Au and Al Deposits on HOPG and Amorphous Carbon"Materials Transactions, JIM. 40. 903-906 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] 中村格芳 他: "単結晶シリコンの延性モード切削加工に関する研究"広島国際学院大学研究報告. 32. 51-58 (1999)

    • Related Report
      2000 Annual Research Report
  • [Publications] T.Sumomogi et al: "Evaluation of surface and subsurface cracks on nano-scale machined single crystal silicon by scanning force microscope and scanning laser microscope"Materials Characterization. (印刷中). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 李木経孝 他: "単結晶シリコンの微小加工における延性・ぜい性遷移点の検討"1999年度精密工学会春季大会講演論文集. 357 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] T.Sumomogi et al.: "Nanotribological Effects due to the presence of water in Scanning Force Microscope"Proceedings of STM/STS'99,July 18-23,1999,Seoul,Korea. 427-428 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 中村格芳 他: "単結晶シリコンの微小加工における延性・ぜい性遷移点の検討"1999年度砥粒加工学会講演論文集. 421-422 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] T.Sumomogi et al.: "Study of Neno-tribology using Scanning Force Microscope"Proceedings of 14^<th> ASPE,Oct.,31-Nov.5,1999,Monterey,USA. 424-427 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] S.Kaji et al.: "The study of ductile-brittke transition on micro-cutting of single crystal silicon"Proceedings of 14^<th> ASPE,Oct.,31-Nov.5,1999,Monterey,USA. 107-110 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 中村格芳 他: "単結晶シリコンの延性モード切削加工に関する研究"広島国際学院大学研究報告. 32. 51-58 (1999)

    • Related Report
      1999 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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