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Development of Conservation Treatment for Wet Organic Archaeological Materials with Supercritical Fluid

Research Project

Project/Area Number 11680167
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Cultural property science
Research InstitutionNational Research Institute Cultural Properties, Nara (2001)
Nara National Research Institute for Cultural Properties (1999-2000)

Principal Investigator

KOHDZUMA Yohsci  Independent Administrative Institution National Research Institute Cultural Properties Nara National Research Institute for Cultural Properties, Center for Archaeological Operations, Senior Researcher, 埋蔵文化財センター, 主任研究官 (80234699)

Co-Investigator(Kenkyū-buntansha) TESHIROGI Miho  Tohoku University, Faculty of Technology, Assistant, 大学院・工学研究科, 助手 (80323070)
INOMATA Hiroshi  Tohoku University, Faculty of Technology, Professor, 大学院・工学研究科, 教授 (10168479)
KOEZUKA Takayasu  Independent Administrative Institution National Research, Institute for Cultural Properties, Nara National Research, Institute for Cultural Properties, Center for Archaeological Operations, Chief of Conservation Scikence Laboratory, 埋蔵文化財センター, 保存修復科学研究室長 (10099955)
Project Period (FY) 1999 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 2001: ¥1,200,000 (Direct Cost: ¥1,200,000)
Fiscal Year 2000: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1999: ¥400,000 (Direct Cost: ¥400,000)
KeywordsArchaeological Waterlogged Wood / Supercritical Fluid Drying / Conservation Treatment / Carbon Dioxide / Ethyl Alcohol / Polyethylen Glycol / Mannitol / Dimensional Stability / 有機質遺物 / 有効拡散係数 / 含浸薬剤
Research Abstract

When a liquid phase in a material is changed to supercritical state or exchanged to a supercritical fluid, it is possible to dry the material without phase change, consequently without the dimensional change. This drying method is called supercritical fluid drying. In this study, we have developed a new conservation technique for wet organic archaeological materials with supercritical carbon dioxide. Since it is difficult to dry wood by extracting water with supercritical carbon dioxide, it is necessary to use ethanol that is soluble to both water and carbon dioxide. The two methods were investigated. In one of them, firstly water in a material was exchanged to ethanol, and then supercritical fluid drying was carried out. In another, both impregnation and drying processes were conducted simultaneously. In former method, it was considered that elevation of elevation control of temperature during drying process effects on wood sample shrinkage. In latter, it was suggested that wet organic archaeological materials were treated successively owing to rapid impregnation of reinforcement chemicals and drying without phase change.
It is significant that supercritical fluid drying was proposed as a new conservation technique for wet organic archaeological materials in this study. A further direction of this study will be to develop appropriate conditions of treatment according to the materials and the degradation degree of the wet organic archaeological objects.

Report

(4 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • 1999 Annual Research Report
  • Research Products

    (9 results)

All Other

All Publications (9 results)

  • [Publications] M.Teshirogi, E.Tahata, M.Kikuchi, H.Inomata, Y.Kohdzuma, T.Koezuka, M.Sawada: "Conservation Treatment of Water-logged Wood with Supercritical Carbon Dioxide"Proceedings of the ICOM-CC WOAM, Stockholm/Sweden. (in printing). (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M.Teshirogi, E.Tahata, M.Kikuchi, H.Inomata, Y.Kohdzuma: "Conservation Treatment and Drying of Water-logged Wood with Supercritical Carbon Dioxide"Preprints of International Congress on the Conservation and Restoration for Archaeological Objects. 117-120 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 手代木美穂, 菊池幹夫, 猪股宏, 高妻洋成: "超臨界CO_2を用いた水浸出土木製品の乾燥"日本文化財科学会第17回大会研究発表要旨集. 44-45 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M. Teshirogi, E. Tahata, M. Kikuchi, H. Inomata, Y. Kohdzuma, T. Koezuka, and M. Sawada: "Conservation Treatment of Water-logged Wood with Supercritical Carbon Dioxide"Proceedings of the ICOM-CC WOAM, Stockholm/Sweden. (in printing). (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M. Teshirogi, E. Tahata, M. Kikuchi, H. Inomata, and Y. Kohdzuma: "Conservation Treatment and Drying of Water-logged Wood with Supercritical Carbon Dioxide"Preprints of Inernational Congress on the Conservation and Restoration for Arcaeological Objects. 117-120 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M. Teshirogi, M. Kikuchi, H. Inoumata, and Y. Kohdzuma: "Drying of Water-logged wood with Supercritical Carbon Dioxide"Nihon Bunkazai Kagakukai Dai 17 Kai Taikai Kenkyu-Happyo Yoshisyu. 44-45 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M.Teshirogi, E.Tahata, M.Kikuchi, H.Inomata, Y.Kohdzuma, T.Koezuka, M.Sawada: "Conservation Treatment of Water-logged Wood with Supercritical Carbon Dioxide"Proceedings of the ICOM-CC WOAM, Stockholm/Sweden. (in printing). (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Teshirogi, E.Tahata, M.Kikuchi, H.Inomata, Y.Kohdzuma: "Conservation Treatment and Drying of Water-logged Wood with Supercritical Carbon Dioxide"Preprints of International Congress on the Conservation and Restoration for Archaeological Objects. 117-120 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] 手代木美穂,菊池幹夫,猪股宏,高妻洋成: "超臨界CO_2を用いた水浸出土木製品の乾燥"日本文化財科学会第17回大会研究発表要旨集. 44-45 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 1999-04-01   Modified: 2016-04-21  

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