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Fabrication of Field Emitter Arrays Using Beam Assisted Processing and Their Stabilization

Research Project

Project/Area Number 12135205
Research Category

Grant-in-Aid for Scientific Research on Priority Areas

Allocation TypeSingle-year Grants
Review Section Science and Engineering
Research InstitutionOsaka University

Principal Investigator

TAKAI Mikio  Osaka University, Research Center for Materials Science at Extreme Conditions, Professor, 極限科学研究センター, 教授 (90142306)

Co-Investigator(Kenkyū-buntansha) YANAGISAWA Junichi  Osaka University, Graduate School of Engineering Science, Associate Professor, 大学院・基礎工学研究科, 助教授 (60239803)
Project Period (FY) 2000 – 2003
Project Status Completed (Fiscal Year 2003)
Budget Amount *help
¥33,500,000 (Direct Cost: ¥33,500,000)
Fiscal Year 2003: ¥7,000,000 (Direct Cost: ¥7,000,000)
Fiscal Year 2002: ¥11,500,000 (Direct Cost: ¥11,500,000)
Fiscal Year 2001: ¥15,000,000 (Direct Cost: ¥15,000,000)
Keywordsnanometer-sized field emission electron source / cathode / dual beams / electron emission / field emitter array / UV laser cleaning / cabon nanotube (CNT) / electron emission site / 電界放出電子源 / 電子源の高輝度化 / 電子源の安定化 / FED / ディスプレイ / 陰極材料 / 真空マイクロエレクトロニクス / 超微構造電子源 / 表面改質 / ナノメートル / 集束イオンビーム / UVレーザ / CNT / カーボンナノチューブ / 真空マイクロエレクトニクス / 局所加工プロセス
Research Abstract

A fabrication process of a nanometer-sized field emission electron source and its arrays using focused electron and ion beams (dual beams) with beam diameters of down to a few nanometers combined with metal-organic gas species has been developed. Pt based gate and emitter structures together with insulating hayers have been fabricated for a several to hundreds seconds. The nanometer-sized emitters worked as field emitters with an emission current of up to 1 uA/tip. A minimum feature size of down to 10 nm with Pt and insulating layer could be obtained only by electron-induced deposition processes, which realized a nanometer-sized field emitter and its arrays. A nanometer-gapped emitter could be fabricated using electron beam induced processes for future experiment on electron interference for emitted electrons from nanometer-gapped emitters.
A laser cleaning technique using ultra-violet (UV) wavelength has been developed for Spindt-type and Si-type field emitter arrays. The laser irradiation with a wavelength of 350 nm resulted in improvement in electron emission, while visible and/or shorter-wavelength such as 300 mn did not improve the emission behavior. The desorption of water components was found to be removed from field emitter arrays by laser clearning.
The number of electron emission site in carbon nanotube (CNT) cathodes was found to be controlled by UV laser or low energy electron irradiation. The UV laser irradiation to printed CNT cathodes resulted in the enhancement of electron emission by four orders of magnitude and a homogeneous emission pattern was observed at a phosphor screen on the anode. the working vacuum for CNT cathodes

Report

(5 results)
  • 2003 Annual Research Report   Final Research Report Summary
  • 2002 Annual Research Report
  • 2001 Annual Research Report
  • 2000 Annual Research Report
  • Research Products

    (58 results)

All Other

All Publications (58 results)

  • [Publications] A.Seidl: "Accuracy Problems in Simulation of Field Emitter Devices Using Finite Elements"J.Computational Physics. 166. 159-164 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] C.Ochiai: "Wedge Emitter Fabrication Using Focused Ion Beam"J.Vac.Sci.Technl.. B19,No.3. 904-906 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] C.Ochiai: "Fabrication Process of Field Emitter Arrays Using Focused Ion and Electron Beam Induced Reaction"J.Vac.Sci.Technl.. B19,No.3. 933-935 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Sawada: "Emission Site Control in Carbon Nanotube Filed Emitters by Focused Ion and Laser Beam Irradiation"J.Vac.Sci.Technol.. B21. 362-365 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Jarupoonphol: "Prototyping of Field emitter Array Using Focused Ion and Electron Beams"Jpn.J.Appl.Phys.. 41. 4311-4313 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Zhao: "Field Emission Characteristics of Screen-Printed Carbon Nanotube After Laser Irradiation"Jpn.J.Appl.Phys.. 41. 4314-4316 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Takai: "Processing of Vacuum Microelectronic Devices by Focused Ion Beam"Appl.Phys.. A76. 1007-1012 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Jarupoonphol: "Optimization of Pt Tip Field Emitter Array Fabricated Using Focused Ion and Electron Beams"J.Vac.Sci.Technol.. B21. 1598-1601 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.J.Zhao: "Field Emission From Screen-Printed Carbon Nanotubes Irradiated by Tunable Ultraviolet Laser in Different Atmospheres"J.Vac.Sci.Technol.. B21. 1734-1737 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa: "Wavelength Dependence of UV Laser Cleaning for Silicon Field Emitter Arrays"Jpn.J.Appl.Phys.. 42,No.6B. 4041-4043 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Murakami: "Fabrication of Nano Electron Source Using Beam Assisted Process"Jpn.J.Appl.Phys.. 42,No.6B. 4037-4040 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa: "Growth of Carbon Nanotube by Thermal Chemical Vapor Deposition at Low Temperature with FeZrN Film"Jpn.J.Appl.Phys.. 42,No.10A. L1205-L1207 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Murakami: "Characteristics of Nano Electron Source Fabricated Using Beam Assisted Process"J.Vac.Sci.Technol.. B(in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa: "Improvement in Electron Emission from CNT Cathodes after Ar Plasma Treatment"J.Vac.Sci.Technol.. B(in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.J.Zhao: "Field Emission From Carbon Nanotube Mat"J.Vac.Sci.Technol.. B(in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Shiroishi: "Low Temperature Growth of Carbon Nanotube by Thermal CVD with FeZrN Catalyst"J.Vac.Sci.Technol.. B(in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Seidl, M.Takai: "Accuracy Problems in Simulation of Field Emitter Devices Using Finite Elements"J. Computational Physics. 166. 159-164 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] C.Ochiai, A.Sawada, H.Noriyasu, M.Takai, A.Hosono, S.Okuda: "Wedge Emitter Fabrication Using Focused Ion Beam"J. Vac. Sci. Techno.. B19, No.3. 904-906 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] C.Ochiai, O.Yavas, M.Takai, A.Hosono, S.Okuda: "Fabrication Process of Field Emitter Arrays Using Focused Ion and Electron Beam Induced Reaction"J. Vac. Sci. Technl.. B19, No.3. 933-935 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Sawada, M.Iriguchi, W.J.Zhao, C.Ochiai, M.Takai: "Emission Site Control in Carbon Nanotube Filed Emitters by Focused Ion and Laser Beam Irradiation"J. Vac. Sci. Technol.. B21. 362-365 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Jarupoonphol, C.Ochiai, M.Takai, A.Hosono, S.Okuda: "Prototyping of Field emitter Array Using Focused Ion and Electron Beams"Jpn. J. Appl. Phys.. 41. 4311-4313 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Zhao, A.Sawada, M.Takai: "Field Emission Characteristics of Screen-Printed Carbon Nanotube After Laser Irradiation"Jpn. J. Appl. Phys.. 41. 4314-4316 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Takai: "Processing of Vacuum Microelectronic Devices by Focused Ion Beam"Appl. Phys.. A76. 1007-1012 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.Jarupoonphol, K.Murakami, K.Sakata, M.Takai, A.Hosono, S.Okuda: "Optimization of Pt Tip Field Emitter Array Fabricated Using Focused Ion and Electron Beams"J. Vac. Sci. Technol.. B21. 1598-1601 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.J.Zhao, N.Kawakami, A.Sawada, M.Takai: "Field Emission From Screen-Printed Carbon Nanotubes Irradiated by Tunable Ultraviolet Laser in Different Atmospheres"J. Vac. Sci. Technol.. B21. 1734-1737 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa, A.Sawada, W.J.Zhao, W.Jarupoonphol, M.Takai: "Wavelength Dependence of UV Laser Cleaning for Silicon Field Emitter Arrays"Jpn. J. Appl. Phys.. 42, No.6B. 4041-4043 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Murakami, W.Jarupoonphol, K.Sakata, M.Takai: "Fabrication of Nano Electron Source Using Beam Assisted Process"Jpn. J. Appl. Phys.. 42, No.6B. 4037-4040 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa, T.Shiroishi, T.Sawada, A.Hosono, S.Nakata, M.Takai: "Growth of Carbon Nanotube by Thermal Chemical Vapor Deposition at Low Temperature with FeZrN Film"Jpn. J. Appl. Phys.. 42, No.10A. L1205-L1207 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Murakami, M Takai: "Characteristics of Nano Electron Source Fabricated Using Beam Assisted Process"J. Vac Sci. & Technol., in press. B. (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa, T.Oyama, K.Murakami, M.Takai: "Improvement in Electron Emission from CNT Cathodes after Ar Plasma Treatment"J. Vac Sci. & Technol., in press. B. (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] W.J.Zhao, W.Rochanachivapar, M.Takai: "Field Emission From Carbon Nanotube Mat"J. Vac Sci. & Technol., in press. B. (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Shiroishi, T.Sawada, A.Hosono, S.Nakata, Y.Kanazawa, M.Takai: "Low Temperature Growth of Carbon Nanotube by Thermal CVD with FeZrN Catalyst"J. Vac Sci. & Technol., in press. B. (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Kanazawa: "Wavelength Dependence of UV Laser Cleaning for Silicon Field Emitter Arrays"Jpn.J.Appl.Phys.. 42,No.6B. 4041-4043 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.Murakami: "Fabrication of Nano Electron Source Using Beam Assisted Process"Jpn.J.Appl.Phys.. 42,No.6B. 4037-4040 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.Takai: "Processing of Vacuum Microelectronic Devices by Focused Ion Beam"Appl.Phys.. A76. 1007-1012 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y W.Jarupoonphol: "Optimization of Pt Tip Field Emitter Array Fabricated Using Focused Ion and Electron Beams"J.Vac.Sci.Technol.. B21. 1598-1601 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] W.J.Zhao: "Field Emission From Screen-Printed Carbon Nanotubes Irradiated by Tunable Ultraviolet Laser in Different Atmospheres"J.Vac.Sci.Technol.. B21. 1734-1737 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] A.Sawada: "Emission Site Control in Carbon Nanotube Filed Emitters by Focused Ion and Laser Beam Irradiation"J. Vac. Sci. Technol.. B21. 362-365 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] W.Jarupoonphol: "Prototyping of Field Emitter Array Using Focused Ion and Electron Beams"Jpn. J. Appl. Phys.. 41. 4311-4313 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] W.Zhao: "Field Emission Characteristics of Screen-Printed Carbon Nanotube After Laser Irradiation"Jpn. J. Appl. Phys.. 41. 4314-4316 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] M.Takai: "Wavelength Dependence of Laser Cleaning for Field Emitter Arrays"the 2^<nd> Intern. Symp. On Laser Precision Microfabrication (LPM2001), Singapoe, May 16 -18, 2001(invited Paper). SPIE. 4426. 302-307 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] M.Takai: "Processing of Vacuum Microelectronic Devices by Focused Ion Beam"to be published in Appl. Phys.. A(In press). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] W.Jarupoonphol: "Optimization of Pt Tip FEA Fabricated Using Focused Ion and Electron Beams"to be published in J. Vac. Sci. Technol.. B(In press). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] W.Zhao: "Field Emission From Screen-Printed Carbon Nanotubes Irradiated by Tunable UV Laser in Different Atmospheres"to be published in J. Vac. Sci. Technol.. B(In press). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] Y.Kanazawa: "Wavelength Dependence of UV Laser Cleaning for Silicon Field Emitter Arrays"to be published in Jpn. J. Appl. Phys.. (In press). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Murakami: "Fabrication of Nano Electron Source Using Beam Assisted Process"to be published in Jpn. J. Appl. Phys.. (In press). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] C.Ochai: "Wedge Emitter Fabrication Using Focused Ion Beam"J.Vac.Sci.Technol.. B19. 904-906 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] C.Ochai: "Fabrication Process of Field Emitter Arrays Using Focused Ion and Electron Beam Induced Reaction"J.Vac.Sci.Technl.. B19. 933-935 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Takai: "Wavelength Dependence of Laser Cleaning for Field Emitter Arrays"The 2nd Intern.Symp. On Laser Precision Microlfabrication (LPM2001). (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] A.Sawada: "Emission Site Control in Carbon Nanotube Field Emitters by Focused Ion Beam Irradiation"The 14th Intern.Conf. On Ion Beam Analysis (IBA2001). (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Takai: "Ion Beam Application to Field-Emitter-Array Fabrication for Field Emission Display"the 7th European Conference on Accelerators in Applied Research and Technology (ECAART 7). (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Takai: "Processing of Vacuum Microelectronic Devices by Focused Ion Beam"Symposium on Ion Beam Processing of Semiconductor Devices. (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] C.Ochiai: "Ion Beam Processing of Metal Gated Field Emitter Arrays"The Proc. of the 13th Intern. Conf On Ion Implantation Technology (IIT 2000). (2000)

    • Related Report
      2001 Annual Research Report
  • [Publications] A.Seidl: "Accuracy Problems in Simulation of Field Emitter Devices Using Finite Elements"J.Computational Physics. 166. 159-164 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] C.Ochiai: "Fabrication Process of Field Emitter Arrays Using Focused Ion and Electron Beam Induced Reaction"J.Vac.Sci.Technl.. B19(in press). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] C.Ochiai: "Wedge Emitter Fabrication Using Focused Ion Beam"J.Vac.Sci.Technl.. B19(in press). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] C.Ochiai: "Fast Prototyping of Metal Gated Field Emitter Arrays Using Dual Beam System"Technical Digest of the 7^<th> Intern. Display Workshops, November 29-December 1,2000, Kobe, Japan. 967-970 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Okuda: "Double-Gated Field-Emitter Arrays for CRT Applications"Technical Digest of the 7^<th> Intern. Display Workshops, November 29-December 1,2000, Kobe, Japan. 525-528 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 2001-04-01   Modified: 2018-03-28  

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