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Cyclic Deformation and Fracture Behavior of L1_2-Type Intermetallic Compounds Using Magnetic Properties

Research Project

Project/Area Number 12450283
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionOsaka University

Principal Investigator

UMAKOSHI Yukichi  Osaka University, Graduate School of Engineering, Professor, 大学院・工学研究科, 教授 (00029216)

Co-Investigator(Kenkyū-buntansha) YASUDA Hiroyuki  Osaka University, Graduate School of Engineering, Research Associate, 大学院・工学研究科, 助手 (60294021)
Project Period (FY) 2000 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥15,100,000 (Direct Cost: ¥15,100,000)
Fiscal Year 2001: ¥5,100,000 (Direct Cost: ¥5,100,000)
Fiscal Year 2000: ¥10,000,000 (Direct Cost: ¥10,000,000)
KeywordsIntermetallic compound / Magnetic anisotropy / Dislocation / Fatigue / Fracture / Fatigue life
Research Abstract

Cyclic deformation behavior and fracture mechanism in Ni_3Fe and Ni_3(Al,Ti) single crystals with the L1_2 structure were examined focusing on the cyclic hardening/softening curves, the deformation substructure and changes in magnetic properties due to dislocations and planar faults.
In a disordered state, Ni_3Fe showed monotonically cyclic hardening during cyclic loading. In contrast, ordered Ni_3Fe single crystals exhibited cyclic softening after initial cyclic hardening. In the stage of cyclic hardening, the well-developed persistent slip bands were observed by transmission electron microscopy. Magnetic properties were influenced by the interaction between magnetic spins and internal stress around dislocations. Using the magnetic anisotropy in fatigued Ni_3Fe single crystals, dislocations and planar faults were determined. At the initial stage of cyclic hardening, the to-and-fro motion of dislocations as a pair combined by an anti-phase boundary occurred. Deformation was concentrated in the PSB region and the disordering occurred in the localized PSB region. The localized disordering induced the cyclic softening. The localized deformation initiated a micro crack resulting in fracture of crystals.

Report

(3 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • Research Products

    (41 results)

All Other

All Publications (41 results)

  • [Publications] H.Y.Yasuda, A.Behgozin, Y.Umakoshi: "Katigue Behaviour of Fe-48at%Al Polycrystals with B2 Structure"J. Mater. Sci. Lett.. 40. 203-207 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi: "Intermetallic Compounds-Development of Refractory Materials For Air Planes"Basis of Science and Techndogy. 1. 49-58 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, D.Furuta, Y.Umakoshi: "Effect of Long-Range Order on The Cyclec-Debermetin Behaviour of N_<13>Fe Single Crystals"Acta mater.. 48. 3401-3408 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] L.Xieo, Y.Umakoshi, J.Sun: "Bioxial Low Cycle fotigue Properties and dislocation Suhstructores of Zirceloy-4 under Ln-Phase"Maerials Science & Engineering. A292. 40-48 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi, H.Y.Yasuda, D.Furuta, A.Sasaki, S.Takahashi: "Observation of Distocations and Planer Fouelts in Fatigueddbtermetallics by means of Magnetic Technigue"Relationshig between Magnetic and Structual. 23-32 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, D.Furuta, A.Sasaki, Y.Umakoshi: "Magnetic Observation of Detormation Substructurl in Cyclically Pepormed N_<13>Fe Single Crystals"J. Appl. Phys.. 88. 5909-5914 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi: "Anomalous Strengthering Behavior of Latermetallic Compounds"J. ISIJ. 5. 9-14 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] K.Hagihara, T.Nakano, Y.Umakoshi: "Cyclic Detormation Behavior of N_<13>Nb Single Crystals kebormed by Slip on (010)[100]"Intermetallics. 9. 239-244 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, A.Sasaki, Y.Umakoshi, S.Takahashi: "Fatigue Benavior and Magnetic Property of N_<13>(Al, Ti) Single Crystals Dotormed at High Temperature"Scripta mater. 44. 581-586 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Nakano, H.Biermann, H.Mughrabi, Y.Umakoshi: "Clessification of ∂-∂ and ∂-α_2 Lamellar Boundaries on the Basis of contiruity of Strains and Slip-Twinning"Phil. Mag. A. 81. 1447-1471 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda, Y.Umakoshi: "Control of microstructure and Orientation Distribution in Ni-Al Based β/∂'Tu_<10> Phase Alloys by Thermonechamicel"Acta mater. 49. 4231-4239 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] L.Xiao, Y.Umakoshi, J.Sun: "Cyclic Deformation Behavior and microstructures of Hydrided Zircaloy-4 Under Bioxial Loading"Met. Mater. Trans. A. 32. 2841-2850 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda, Y.Umakoshi: "Control of microstructure and Crystal Orientation Distribution in NiAl-Based β/∂'Tu_<10> Phase Alloys"PRICM4. 859-862 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi: "Fatigue and Fracture at Intermetallic Compounds"Science and Industry. 75. 261-265 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda, Y.Umakoshi: "Formation of Deformation Bands and Precipitation of Ni_3Al(γ')Phase in NiAl(β)-Based crystals"Intermetallics. 10. 139-147 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, R.Jimba, Y.Umakoshi: "Cyclic Deformation Behaviour of γ'-Ni_3(Al, Ti) Single Crystal containing disordered precipitates"Acta Materia.. 50. 161-169 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, A.Behgozin and Y.Umakoshi: "Fatigue Behavior of Fe-48 at.%Al Polycrystals with B2 Structure"J. Mater. Sci. Letter. 40[2]. 203-207 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi: "Intermetallic Compounds-Development of Refractory Materials For Air Planes"Basis of Science and Technology. 1. 49-58 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, D.Furuta and Y.Umakoshi: "Effect of Long-Range Order on the Cyclic Deformation Behavior of Ni_3Fe Single Crystals"Acta mater. 48. 3401-3408 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] L.Xiao, Y.Umakoshi and J.Sun: "Bioxial Low Cycle Fatigue Dislocation Substructures of Zircaloy-4 Under In-Phase and Out-Of-Phase Loading"Materials Science & Engineering. A292. 40-48 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi, H.Y.Yasuda, D.Furuta, A.Sasaki and S.Takahashi: "Observation of Dislocations and Planar Faults in Fatigued Intermetallics by Means of Magnetic Technique"Relationship between Magnetic and Structural Properties. 23-32 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, D.Furuta, A.Sasaki and Y.Umakoshi: "Magnetic Study on Cyclically Deformed Ni_3Fe Single Crystals"Relationship between Magnetic and Structural Properties. 77-80 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, D.Furuta, A.Sasaki and Y.Umakoshi: "Magnetic Observation of Deformation Substructure in Cyclically Deformed Ni_3Fe Single Crystals"Journal of Applied Physics. 88[10]. 5909-5914 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Umakoshi: "Anomalous Strengthening Behavior of Intermetallic Compounds"J. of ISIJ. 5. 9-14 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] K.Hagihara, T.Nakano and Y.Umakoshi: "Cyclic Deformation Behavior of Ni_3Nb Single Crystals Deformation by Slip on (010)[100]"Intermetallics. 9. 239-244 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, A.Sasaki, Y.Umakoshi and S.Takahashi: "Fatigue Behavior and Magnetic Property of Ni_3(Al, Ti) Single Crystals Deformed at High Temperature"Scripta mater. 44. 581-586 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Nakano, H.Biermann, H.Mugrabi, Y.Nakai and Y.Umakoshi: "Classification of γ-γ and γ-α_2 lamellar boundaries on the basis of continuity of strains and slip-twinning planes in fatigued TiAl polysynthetically twinned crystals"Philosophical Magazine A. 81[6]. 1447-1471 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda and Y.Umakoshi: "Control of Microstructure and Orientation Distribution in Ni-Al Based (β/γ') Two Phase Alloys by Thermomechanical Processing"Acta mater. 49. 4231-4239 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] L.Xiao, Y.Umakoshi and J.Sun: "Cyclic Deformation Behavior and Microstructures of Hydrided Zircaloy-4 Under Biaxial Loading"Metallurgical and Materials Transactions A. 32A. 2841-2850 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda and Y.Umakoshi: "Control of Microstructure and Crystal Orientation Distribution in NiAl-based (β/γ') Two Phase Alloys by Thermomechanical Processing"PRICM. 4. 859-862 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Umakoshi: "Fatigue and Fracture of Intermetallic Compounds"Science and Industry. 75. 261-265 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Sakata, H.Y.Yasuda and Y.Umakoshi: "Formation of Deformation Bands and Precipitation of Ni_3Al(γ') Phase in NiAl(β)-based Single Crystals by Thermomechanical Processing"Intermetallics. 10. 139-147 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, R.Jimba and Y.Umakoshi: "Cyclic Deformation Behavior of γ'-Ni_3(Al, Ti) Single Crystal Containing Disordered γ Precipitates"Acta Materialia. 50. 161-169 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] H.Y.Yasuda, A.Sasaki, Y.Umakoshi, S.Takahashi: "Fatigue behavior and magnetic property of Ni_3(Al, Ti)single crystals deformed at high temperature"Scripta materialia. 44・6. 581-586 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] T.Sakata, H.Y.Yasuda, Y.Umakoshi: "Formation of deformation bonds and precipitation of Ni_3A(δ')place in NiAl(β)-bosed single crystals"Intermetallics. 10. 139-147 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] 馬越佑吉: "金属間化合物の疲労と破壊"科学と工業. 75・[6]. 261-265 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] H.Y.Yasuda, R.Jinbma, Y.Umakoshi: "Cyclis deformation behaviour of δ'Ni_3(Al, Ti)single crystal containing disordered δ precrpitates"Acta materialia. 50. 161-169 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Umakoshi,H.Y.Yasuda,D.Furuta,A.Sasaki,S.Takahashi: "Observation of dislocation and planar faults in fatigued intermetallics by means of magnetic technique"Relationship between Magnetic and Structural Properties. 23-32 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Y.Yasuda,D.Furuta,A.Sasaki,Y.Umakoshi: "Magnetic study on cyclically deformed Nia Fe single crystals"Relationship between Magnetic and Structural Properties. 77-80 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Y.Yasuda,D.Furuta,Y.Umakoshi: "Effect of long-range order on the cyclic deformation behaviors, of Nia Fe single crystals"Acta materialia. 48. 3401-3408 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Y.Yasuda,D.Furuta,A.Sasaki,Y.Umakoshi: "Magnetic observation of deformation substructure in cyclically deformed Nia Fe single crystals"J.Applied Physics. 88・Na10. 5909-5914 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 2000-04-01   Modified: 2016-04-21  

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