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DEVELOPMENT OF GRAZING-EXIT MICRO X-RAY FLUORESCENCE INSTRUMENT AND SINGLE PARTICLE ANALYSIS SUCH AS AEROSOLS

Research Project

Project/Area Number 12554030
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field 分離・精製・検出法
Research InstitutionOSAKA CITY UNIVERSITY (2002)
Tohoku University (2000-2001)

Principal Investigator

TSUJI Kouichi  OSAKA CITY UNIVERSITY, GRADUATE SCHOOL OF ENGINEERING, ASSOCIATE PROFESSOR, 大学院・工学研究科, 助教授 (30241566)

Co-Investigator(Kenkyū-buntansha) WAGATSUMA Kazuaki  TOHOKU UNIVERSITY, INSTITUTE FOR MATERIALS RESEARCH, PROFESSOR, 金属材料研究所, 教授 (30158597)
KOMETANI Noritsugu  OSAKA CITY UNIVERSITY, GRADUATE SCHOOL OF ENGINEERING, LECTURER, 大学院・工学研究科, 講師 (80295683)
YONEZAWA Yoshirou  OSAKA CITY UNIVERSITY, GRADUATE SCHOOL OF ENGINEERING, PROFESSOR, 大学院・工学研究科, 教授 (10026346)
TAKAHASHI Hideyuki  JEOL, RESEARCHER, 電子光学機器技術本部・応用研究センター, 主任研究員(研究職)
ASAMI Kazuhiko  TOHOKU UNIVERSITY, INSTITUTE FOR MATERIALS RESEARCH, ASSOCIATE PROFESSOR, 金属材料研究所, 助教授 (20005929)
Project Period (FY) 2000 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥13,700,000 (Direct Cost: ¥13,700,000)
Fiscal Year 2002: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2001: ¥5,300,000 (Direct Cost: ¥5,300,000)
Fiscal Year 2000: ¥7,600,000 (Direct Cost: ¥7,600,000)
KeywordsGRAZING EXIT X-RAY MEASUREMENT / ELECTRON PROBE MICRO ANALYSIS / MICRO ANALYSIS / SURFACE ANALYSIS / PARTICLE ANALYSIS / AEROSOLS / 表面分析 / 微粒子分析
Research Abstract

We have studied EPMA under grazing-exit conditions, which is called GE-EPMA. We developed a GE-EPMA apparatus based on a commericial EPMA. We evaluated the analytical characterization of GE-EPMA. It was foue analysis and single-particle analysis are possible by GE-EPMA with extremely low background. By analyzing exit-angle dependence of EPMA intensity, we can evaluate thickness and density of him films. The advantage of GE-EPMA is the use of an electron beam with a small diameter at an incident angle of 90 degrees, which makes it possible to perform localized analysis. Element mapping is possible by scanning the electron beam or the sample stage. In addition, depth analysis is possible by varying the exit angle, which could finally result in 3-dimensional EPMA

Report

(4 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • 2000 Annual Research Report
  • Research Products

    (32 results)

All Other

All Publications (32 results)

  • [Publications] Z.Spolnik, K.Tsuji, etc.: "Quantitative analysis of metallic ultra-thin films by grazing-exit electron probe x-ray microanalysis"X-Ray Spectrometry. 31. 178-183 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Z.Spolnik, K.Tsuji, etc.: "Grazing-exit electron probe x-ray microanalysis of ultra-thin films and single particles"Anal. Chim. Acta. 455. 245-252 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Tsuji, K.Satio, etc.: "Localized Thin-Film Analysis by Grazing-Exit EPMA (GE-EPMA)"Spectrochim. Acta. B. 57. 897-906 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Tsuji, F.Delalieux: "Micro x-ray fluorescence using a pinhole aperture in quasi-contact mode"J. Anal. At. Spectrom.. 17. 1405-1407 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J.Injuk, K.Tsuji, etc.: "Airborne particles in the Miyagi Museum of Art in Sendai, Japan, Studied by Electron Probe X-Ray Microanalysis"Anal. Sci.. 18. 561-566 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Tsuji, K.Wagatsuma: "Enhancement of TXRF Intensity by Using a Reflector"X-Ray Spectrom. 31. 358-362 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 辻 幸一(分担執筆): "新訂版・表面科学の基礎と応用"日本表面科学会編(印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Z. Solnik, K. Tsuji, etc: "Quantitative analysis of metallic ultra-thin films by grazing-exit electron probe x-ray microanalysis"X-Ray Spectrometry. 31. 178-183 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Z. Spolnik, K. Tsuji, etc: "Grazing-exit electron probe x-ray microanalysis of ultra-thin films and single particles"Anal. Chim. Acta. 455. 245-252 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Tsuji, K. Saito, etc: "Localized Thin-Film Analysis by Grazing-Exit EPMA (GE-EPMA)"Spectrochim. Acta. B. 57. 897-906 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Tsuji, and F. Delalieux: "Micro x-ray fluorescence using a pinhole aperture in quasi-contact mode"J. Anal. At. Spectrom. 17. 1405-1407 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J. Injuk, K. Tsuji, etc: "Airborne particles in the Miyagi Museum of Art in Sendai, Japan, Studied by Electron Probe X-Ray Microanalysis"Anal. Sci. 18. 561-566 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Tsuji, K. Wagatsuma: "Enhancement of TXRF Intensity by Using a Reflector"X-Ray Spectrom. 31. 358-362 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Z.Spolnik, K.Tsuji, et al.: "Quantitative analysis of metallic ultra-thin films by grazing-exit electron probe x-ray microanalysis"X-Ray Spectrometry. 31. 178-183 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] Z.Spolnik, K.Tsuji, et al.: "Grazing-exit electron probe x-ray microanalysis of ultra-thin films and single particles"Anal.Chim.Acta. 455. 245-252 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Tsuji, K.Saito, et al.: "Localized Thin-Film Analysis by Grazing-Exit EPMA (GE-EPMA)"Spectrochim.Acta.B. 57. 897-906 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Tsuji, F.Delalieux: "Micro x-ray fluorescence using a pinhole aperture in quasi-contact mode"J.Anal.At.Spectrom.. 17. 1405-1407 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] J.Injuk, K.Tsuji, et al.: "Airborne particles in the Miyagi Museum of Art in Sendai, Japan, Studied by Electron Probe X-Ray Microanalysis"Anal.Sci.. 18. 561-566 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Tsuji, K.Wagatsuma: "Enhancement of TXRF Intensity by Using a Reflector"X-Ray Spectrom. 31. 358-362 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 辻 幸一(分担執筆): "新訂版・表面科学の基礎と応用"日本表面科学会編(印刷中).

    • Related Report
      2002 Annual Research Report
  • [Publications] Z.Spolnik et al.: "Quantitative analysis of metalic ultra-thin films by grazing-exit electron Aobe X-ray analysis"X-Ray Spectrom. 31. 178-183 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Tsuji et al.: "New experimental equipment for grazing-exit electron probe microanalysis"Rev. Sci. Lustrum. 72. 3933-3936 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Tsuji et al.: "Continuous X-ray background in grazing-exit electron probe X-ray microanalysis"Spectrochim. Acta B. 56. 2497-2504 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] 辻 幸一: "斜出射XSW線測定型の電子線プローグマイクロアナリンス"X線分析の進歩. 32. 25-44 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Z.Spolnik et al.: "Grazing-exit electro probe X-ray microanalysis of ultra-thin films and single particles"Aral. Chim. Acta. (印刷中). (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Tsuji et al.: "Localized Thin-Film Analysis by Grazing-Exit EPMA(GE-EPMA)"Spectro chim. Acta B. (印刷中). (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] 辻幸一: "斜出射X線測定型の電子線プローブマイクロアナリシス"X線分析の進歩(アグネ技術センター編). 32集(印刷中). 20 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 辻幸一: "斜出射X線測定による微小領域の表面分析と微粒子分析"まてりあ(日本金属学会 編). 39. 586-593 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Tsuji: "Grazing-Exit X-Ray Spectrometry for Surface and Thin-Film Analysis"Anal.Sci.. 17. 145-148 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Tsuji: "Surface Studies by Grazing-Exit Electron Probe Microanalysis (GE-EPMA)"X-Ray Spectrom.. 30(印刷中). 5 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Tsuji: "Comparison of Grazing-Exit Particle-induced X-ray Emission with other Related Methods"Spectrochim.Acta B. 55. 1009-1016 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] K.Tsuji: "Detection Limit of Grazing-Exit Electron Probe Microanalysis (GE-EPMA) for Particles Analysis"Microchim.Acta. 132. 357-360 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 2000-04-01   Modified: 2016-04-21  

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