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Development of high-functional materials by surface treatment and its evaluation of gigacycle fatigue strength

Research Project

Project/Area Number 12650077
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionToyama University

Principal Investigator

SHIOZAWA Kazuaki  Faculty fo Engineering Professor, 工学部, 教授 (90019216)

Co-Investigator(Kenkyū-buntansha) OKANE Masaki  Faculty fo Engineering, Research Assistant, 工学部, 助手 (90262500)
NISHINO Seiichi  Faculty fo Engineering, Associate Professor, 工学部, 助教授 (00218174)
Project Period (FY) 2000 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2002: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2001: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2000: ¥1,900,000 (Direct Cost: ¥1,900,000)
KeywordsGigacycle fatigue / Surface treatment / Internal crack initiation / Shot-peening / Nitriding / Anodizing / High-strength steel / Aluminurn alloy / コンピュータ・シミュレーション / 高速度工具鋼 / 低合金鋼 / 疲労 / 超長疲労寿命 / 軸受鋼
Research Abstract

Some surface modifications are applied to the surfaces of mechanical elements and engineering components for the purpose of increasing fatigue strength and extending lifetime of engineering materials in various kinds of environments, because the surface is usually the most sensitive part for strength and failure resistance. In this study, gigacycle fatigue behavior of metals surface-treated with ceramics thin film, nitriding and shot-peening is investigated through the cantilever-type rotary-bending fatigue tests and discussed the rules of surface layer on fatigue strength. Main results are summarized as follows :
(1) The S-N curve obtained for a high carbon-chromium bearing steel, JIS SUJ2, high speed tool steel, JIS SKH51, and low-alloy steel, JIS SNCM439, clearly classified the fracture modes into two groups each with a different crack origin. One was governed by crystal slip on the specimen surface at high-stress amplitude level and low number of cycles and the other was governed by … More a non-metallic inclusion at subsurface at high number of cycles. The remarkable shape of the S-N curve was named a 'duplex S-N curve'.
(2) Fatigue crack initiation site changed from the surface of untreated specimen to the subsurface of the specimen because of hardening and compressive residual stress with surface treatment in the region of high-stress amplitude. On the other hand, no difference in fatigue life controlled by the subsurface crack initiation between untreated specimen and surface treated one was observed in high-cycle region. It was suggested that the S-N curve corresponding to the internal fracture mode is inherent in the material, as compared with the S-N curve of surface fracture mode, which is affected by surface conditions, environmental conditions and so on.
(3) A distinctive feature of the fracture surface, named as a granular-bright facet (GBF), was observed in the vicinity of a non-metallic inclusion at the subsurface fracture origin inside the fish-eye zone. From the discussion based on fracture mechanics, it is pointed out that an internal crack is able to grow after formation of the GBF during the long fatigue process. Mechanisms of the GBF formation was proposed as 'disperse decohesion of spherical carbide' model.
(4) The effect of anodized coating on fatigue strength of aluminum alloys was investigated under repeated tensile fatigue test. Fatigue strength of the anodized specimens decreased as compared with uncoated one, because the fracture of anodized coating film occurred at the critical strain formed by the accumulation of plastic deformation of substrate metal and crack was induced in the substrate at the flaw of the anodized film. Less

Report

(4 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • 2000 Annual Research Report
  • Research Products

    (72 results)

All Other

All Publications (72 results)

  • [Publications] K.Shiozawa: "Effect of Testing Frequency on Corrosion Fatigue of a Squeeze-Cast Aluminum Alloy"Metallurgical and Materials Transactions, A. 31A・4. 1137-1145 (2000)

    • Description
      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] 西野精一: "遮熱コーティングを施したNi基超合金の低サイクル疲労強度に及ぼす試験温度の影響"日本機械学会論文集,A編. 66・646. 1178-1184 (2000)

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      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] 河村新吾: "複合表面改質した合金工具鋼のアルミニウム合金とのしゅう動におけるTiN被膜の寿命向上"日本機械学会論文集,C編. 66・646. 1988-1995 (2000)

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      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 酒井達雄: "高炭素クロム軸受鋼の広寿命域における特徴的回転曲げ疲労特性に関する実験的検証"材料. 49・7. 779-785 (2000)

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      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] 塩澤和章: "アルマイト処理を施したアルミニウム合金A2014-T6の疲労強度特性"日本機械学会論文集,A編. 66・652. 2170-2175 (2000)

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      2002 Final Research Report Summary
  • [Publications] 塩澤和章: "材料力学-疲労研究の最近の動向(特集 機械工学年鑑,解説)"日本機械学会誌. 103・981. 494-495 (2000)

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      2002 Final Research Report Summary
  • [Publications] 魯 連涛: "高炭素クロム軸受鋼の超長寿命疲労強度に及ぼすショットピーニングの影響"日本機械学会論文集,A編. 67・662. 1630-1638 (2001)

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      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 塩澤和章: "アルミニウム合金の疲労強度に及ぼすアルマイト被覆の影響"日本機械学会論文集,A編. 67・662. 1639-1646 (2001)

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      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] 酒井達雄: "高炭素クロム軸受鋼の超広寿命域における回転曲げ疲労特性と破面形態"日本機械学会論文集,A編. 67・663. 1805-1812 (2001)

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      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] S.Kawamura: "Life improvement of TiN-duplex-treated tool steel by tempering"Tribology Research : From Model Experiment to Industrial Problem. 587-597 (2001)

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    • Related Report
      2002 Final Research Report Summary
  • [Publications] K.Shiozawa: "S-N Curve Characteristics and Subsurface Crack Initiation behaviour in Ultra-Long Fatigue Life Fatigue of a High Carbon-Chromium Bearing Steel"Fatigue Fracture Eng. Mater. and Struct.. 24・12. 781-790 (2001)

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      2002 Final Research Report Summary
  • [Publications] K.Shiozawa: "Very High Cycle Fatigue Behaviour of Shot-Peened High Carbon-Chromium Bearinig Steel"Fatigue Fracture Eng. Mater. and Struct.. 25・8/9. 813-822 (2002)

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      2002 Final Research Report Summary
  • [Publications] 魯 連涛: "高炭素クロム軸受鋼の超長寿命疲労挙動に及ぼす二段二重変動荷重の影響と内部き裂進展挙動"日本機械学会論文集,A編. 68・675. 1666-1673 (2002)

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      2002 Final Research Report Summary
  • [Publications] 魯 連涛: "高速度工具鋼SKH51の超長寿命疲労挙動と破壊形態"日本機械学会論文集,A編. 69・679(掲載予定). (2003)

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      2002 Final Research Report Summary
  • [Publications] K.Shiozawa: "Characteristics of Fatigue Behavior of Surface Modified Materials"Macro and Microscopic Approach to Fracture. (掲載予定). (2003)

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      2002 Final Research Report Summary
  • [Publications] K.Shiozawa: "Effect of Anodized Coatings on Fatigue Strength in Aluminum Alloy"Surface Treatment V, Computer Methods and Experimental Measurements for Surface Treatment Effects. 397-406 (2001)

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      「研究成果報告書概要(和文)」より
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      2002 Final Research Report Summary
  • [Publications] K.Shiozawa: "Topographic Analysis for Subsurface Crack Initiation and Propagation of High Strength Steel in Gigacycle Fatigue"Proceedings of the Eighth International Fatigue Congress, Fatigue 2002. 5. 2939-2946 (2002)

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      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 塩澤和章: "介在物を起点とする高硬度鋼の内部疲労き裂の発生・進展機構"日本材料学会題26回疲労シンポジウム講演論文集. 141-144 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "Effect of Testing Frequency on the Corrosion Fatigue of a Squeeze-Cast Aluminum Alloy"Metallur. And Mater. Trans.. 31A-4. 1137-1145 (2000)

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      「研究成果報告書概要(欧文)」より
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      2002 Final Research Report Summary
  • [Publications] S. Nishino: "Influence of Testing Temperature on Low-Cycle Fatigue Strength of Thermal Barrier-Coated Ni-Base Superalloy"Trans. JSME. 66A-646. 1178-1184 (2000)

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      2002 Final Research Report Summary
  • [Publications] S. Kawamura: "Life Improvement of TiN Film Prepared by Duplex Treatment on Alloy Tool Steel Sliding Against Aluminum Alloy"Trans. JSME. 66C-646. 1988-1995 (2000)

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      2002 Final Research Report Summary
  • [Publications] T. Sakai: "Experimental Reconfirmation of Characteristic S-N Property for High Carbon Chromium Bearing Steel in Wide Life Region in Rotating Bending"J. Soc. Mat. Sci., Japan. 49-7. 779-785 (2000)

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      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "Duplex S-N Curve Characteristics and Subsurface Fatigue Crack Initiation behaviour in High Carbon-Chromium Bearing Steel"The 13^<th> European Conference on Fracture, Fracture Mechanics : Applications and Challenges,CD-ROM, Ref.. No.3C.120. (2000)

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  • [Publications] K. Shiozawa: "Characteristics of Fracture Strength on Anodized 2014-T6 Aluminum Alloy"Trans. JSME. 66A-652. 2170-2175 (2000)

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      2002 Final Research Report Summary
  • [Publications] L. Lu: "Characteristics of S-N Curve and Subsurface Crack Initiation Behaviour of High Strength Bearing Steel in Gigacycle Fatigue"Mater. Sci. Res. Inter.. STP-1. 34-40 (2001)

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      2002 Final Research Report Summary
  • [Publications] T. Sakai: "Characteristic S-N Property of High Carbon Chromium Bearing Steel in Ultra-Wide Life Region under Rotating Bending"Mater. Sci. Res. Inter.. STP-1. 41-46 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
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      2002 Final Research Report Summary
  • [Publications] S. Kawamura: "Life Improvement of TiN-Duplex-Treated Tool Steel by Tempering"Tribology Research : From Model Experiment to Industrial Problem (Elsevior). 587-597 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "Effect of Anodized Coatings on Fatigue Strength in Aluminum Alloy"Surface Treatment V, Computer Methods and Experimental Measurements (WIT Press). 397-406 (2001)

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      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "Superlong Fatigue Behavior of Shot-Peened High-Strength Steel"Int. Conf. on Fatigue in the Very High Cycle Regime. 165-172 (2001)

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    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "S-N Curve Characteristics and Subsurface Crack Initiation Behaviour in Ultra-Long Life Fatigue of a High Carbon-Chromium Bearing Steel"Fatigue and Frac. Engng Mater. Struct.. 24-12. 781-790 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "The Effect of Anodized Coating on Fatigue Strength of Aluminum Alloys"Trans. JSME. 67A-662. 1639-1646 (2001)

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      2002 Final Research Report Summary
  • [Publications] L. Lu: "Effect of Shot-Peening on Super-Long-Life Fatigue Behavior in High Carbon-Chromium Bearing Steel"Trans. JSME. 67A-662. 1630-1638 (2001)

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  • [Publications] T. Sakai: "S-N Property and Fractography of High Carbon Chromium Bearing Steel over Ultra Wide Life Region under Rotating Bending"Trans. JSME. 67A-663. 1805-1812 (2001)

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      2002 Final Research Report Summary
  • [Publications] K. Shiozawa: "Topographic Analysis for Subsurface Crack Initiation and Propagation of High Strength Steel in Gigacycle Fatigue"The 8^<th> Inter. Fatigue Congress. 5. 2939-2946 (2002)

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      2002 Final Research Report Summary
  • [Publications] K. Shinozawa: "Very High-Cycle Fatigue Behaviour of Shot-Peened High-Carbon-Chromium Bearing Steel"Fatigue and Frac. Engng Mater. Struct.. 25-8/9. 813-822 (2002)

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  • [Publications] L. Lu: "Effect of Two-Step Load Variation on Super-Long Life Fatigue and Internal Crack Growth Behavior of High Carbon-Chromium Bearing Steel"Trans. JSME. 68A-675. 1666-1673 (2002)

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  • [Publications] Y. Haruyama: "Performance Evaluation of Duplex Treated Tool Steel Sliding Against Aluminum Alloy under Oxidation-Limited Condition"The 10^<th> Nordic Symposium on Tribology, CD-ROM, Reg. Nr 211..

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  • [Publications] K. Shiozawa: "Mechanism of Subsurface Crack Initiation and Propagation from an Inclusion of High Hardness Steel"Proc. of the 26^<th> Symp. On Fatigue. 141-144 (2002)

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  • [Publications] L. Lu: "Gigacycle Fatigue Behavior and Fracture Morphology of High Speed Tool Steel, SKH51"Trans. JSME. 69A-679 to be published. (2003)

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  • [Publications] K. Shiozawa: "Characteristics of Fatigue Behavior of Surface Modified Materials"Macro and Microscopic Approach to Fracture. WIT Press, to be published. (2003)

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      2002 Final Research Report Summary
  • [Publications] K.Shiozawa, L.Lu: "Very High Cycle Fatigue Behaviour of Shot-Peened High Carbon-Chromium Bearing Steel"Fatigue & Fracture of Engineering Materials & Structures. 25・8/9. 813-822 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 魯 連涛, 塩澤和章: "高炭素クロム軸受鋼の超長寿命疲労挙動に及ぼす二段二重変動荷重の影響と内部き裂進展挙動"日本機械学会論文集,A編. 68・675. 1666-1673 (2002)

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      2002 Annual Research Report
  • [Publications] 魯 連涛, 塩澤和章: "高速度工具鋼の超長寿命疲労強度特性に及ぼす表面処理の影響"日本材料学会第51期学術講演会講演論文集. 273-274 (2002)

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      2002 Annual Research Report
  • [Publications] 塩澤和章, 丸山 宏, 遅 愛娜: "SNCM439鋼の超長寿命疲労挙動とショットピーニングの影響"日本機械学会平成14年度材料力学部門講演会講演論文集. No.02-05. 579-580 (2002)

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      2002 Annual Research Report
  • [Publications] 塩澤和章, 森井祐一, 西野精一, 魯 連涛: "介在物を起点とする高硬度鋼の内部疲労き裂の発生・進展機構"日本材料学会第26回疲労シンポジウム講演論文集. 141-144 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Shiozawa, S.Nishino, K.Yamamoto, L.Lu: "Topographic Analysis for Subsurface Crack Initiation and Propagation of High Strength Steel in Gigacycle Fatigue"Proceedings of the Eighth International Fatigue Congress. 5. 2939-2946 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] Y.Haruyama, S.Kawamura, Y.Kimura, K.Shiozawa: "Performance evaluation of duplex treated tool steel sliding against aluminum alloy under oxidation-limited condition"10^<th> Nordic Symposium on Tribology. (CD-ROM). Reg.Nr211 (2002)

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      2002 Annual Research Report
  • [Publications] 魯 連涛, 塩澤和章, 森井祐一: "高速度工具鋼SKH51の超長寿命疲労挙動と破壊形態"日本機械学会論文集,A編. 69・679(掲載予定). (2003)

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      2002 Annual Research Report
  • [Publications] 花田竜一, 塩澤和章, 岡根正樹: "SCM435鋼の超長寿命疲労特性と窒化処理の影響"日本機械学会北陸信越支部第40期総会・講演会講演論文集. No.037-1(発表予定). (2003)

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      2002 Annual Research Report
  • [Publications] 呉 友諠, 塩澤和章, 岡根正樹, 今 裕文: "A6151およびA2014アルミニウム合金の疲労挙動に及ぼすショット・ピーニング処理の影響"日本機械学会北陸信越支部第40期総会・講演会講演論文集. No.037-1(発表予定). (2003)

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      2002 Annual Research Report
  • [Publications] 魯 連涛, 塩澤和章: "高炭素クロム軸受鋼の超長寿命疲労強度に及ぼすショットピーニングの影響"日本機会学会論文集. A67-662. 1630-1638 (2001)

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      2001 Annual Research Report
  • [Publications] 塩澤和章, 小林弘和 他2名: "アルミニウム合金の疲労強度に及ぼすアルマイト被覆の影響"日本機械学会論文集. A67-662. 1639-1646 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Shiozawa, L.Lu: "Superlong Fatigue Behavior of Shot-Peened High-Strength Steel"Proceedings of the International Conference on Fatigue in the Very High Cycle Regime. 165-172 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Shiozawa, L.T.Lu, S.Ishihara: "S-N Curve Characteristics and Subsurface Crack Initiation behaviour in Ultra-Long Fatigue Life Fatigue of a High Carbon-Chromium Bearing Steel"Int. Jour. Fatigue Fracture Eng. Mater. and Struct.. 24. 781-790 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] 塩澤和章, 魯 連涛 他2名: "高速度工具鋼SKH51の超長寿命疲労挙動と破壊形態"日本機械学会平成13年度材料力学部門講演会講演論文集. No.01-16. 243-244 (2001)

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      2001 Annual Research Report
  • [Publications] 魯 連涛, 塩澤和章: "高炭素クロム軸受鋼の超長寿命疲労挙動に及ぼす二段荷重変動の影響"日本機械学会2001年度年次大会講演論文集. 1. 175-176 (2001)

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      2001 Annual Research Report
  • [Publications] L.T.Lu, K.Shiozawa, S.Ishihara: "Characteristics of S-N Curve and Subsurface Crack Initiation Behaviour of High Strength Bearing Steel in Gigacycle Fatigue"Materials Science Research International. STP-1. 35-40 (2001)

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      2001 Annual Research Report
  • [Publications] T.Sakai, M.Takeda, N.Tanaka, M.Kanematsu, N.Oguma, K.Shiozawa: "Characteristic S-N Property of High Carbon Chromium Bearing Steel in Ultra-Wide Life Region under Rotating Bending"Materials Science Research International. STP-1. 41-46 (2001)

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      2001 Annual Research Report
  • [Publications] 酒井達雄, 武田光弘, 田中伸明, 金光学, 小熊規泰, 塩澤和章: "高炭素クロム軸受鋼の超広寿命域における回転曲げ疲労特性と破面形態"日本機械学会論文集. A67-663. 1805-1812 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] K.Shiozawa, H.Kobayashi, M.Terada, A.Matsui: "Effect of Anodized Coatings on Fatigue Strength in Aluminum Alloy"Surface Treatment V, Computer Methods and Experimental Measurements for Surface Treatment. 397-412 (2001)

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      2001 Annual Research Report
  • [Publications] 塩澤和章: "表面改質材の疲労挙動と破壊形態(基調講演)"日本機械学会平成13年度材料力学部門講演会講演論文集. No.01-16. 253-156 (2001)

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      2001 Annual Research Report
  • [Publications] 塩澤和章, 光谷宏太郎, 茂島博司: "表面改質を施した高硬度鋼SKD61の耐食性評価と腐食疲労強度特性"日本機械学会2001年度年次大会講演論文集. 1. 321-322 (2001)

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      2001 Annual Research Report
  • [Publications] 山本薫, 西野精一, 塩澤和章: "トポグラフィ破面解析による高炭素クロム軸受鋼の内部き裂発生挙動に関する研究"日本機械学会北陸信越支部第38期総会・講演会講演論文集. No.017-1. 235-236 (2001)

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  • [Publications] 北澤広樹, 塩澤和章 他2名: "表面改質アルミニウム合金の疲労強度特性に及ぼす応力比の影響"日本機械学会北陸信越支部第38期総会・講演会講演論文集. No.017-1. 243-244 (2001)

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  • [Publications] 西野精一, 塩澤和章, 山本 薫: "トポグラフィ破面解析によるβ型 Ti 合金の内部き裂発生挙動に関する研究"日本機械学会2001年度年次大会講演論文集. No.017-1. 179-180 (2001)

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  • [Publications] K.Shiozawa, L.Lu: "Very High Cycle Fatigue Behaviour of Shot-Peened High Carbon-Chromium Bearing"Int. Jour. Fatigue Fracture Eng. Mater. and Struct.. (投稿中).

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  • [Publications] 酒井達雄,武田光弘,塩澤和章 他3名: "高炭素クロム軸受鋼の広寿命域における特徴的回転曲げ疲労特性に関する実験的検証"材料. 49・7. 779-785 (2000)

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  • [Publications] 塩澤和章,小林弘和 他2名: "アルマイト処理を施したアルミニウム合金A2014-T6の疲労強度特性"日本機械学会論文集. A66・625. 2170-2175 (2000)

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  • [Publications] 魯連涛,塩澤和章: "高炭素クロム軸受鋼の超長寿命疲労強度特性に及ぼす表面処理の影響"日本機械学会2000年度年次大会講演論文集. 3. 151-152 (2000)

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  • [Publications] 塩澤和章,光谷光太郎,茂島博司: "各種表面改質処理を施した工具鋼SKD61の疲労強度特性"日本機械学会2000年度年次大会講演論文集. 3. 37-38 (2000)

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  • [Publications] 塩澤和章,魯連涛: "Duplex S-N Curve Characteristics and Subsurface Fatigue Crack Initiation Behaviour in High Carbon-Chromium Bearing Steel"Proceedings of The 13^<th> European Conference on Fracture, Fracture Mechanics : Applications and Challenges. (CD-ROM版). (2000)

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  • [Publications] 塩澤和章,魯連涛: "高炭素クロム軸受鋼SUJ2の超長寿命疲労強度に及ぼすショットピーニングの影響"日本材料学会第25回疲労シンポジウム講演論文集. 207-210 (2000)

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Published: 2000-04-01   Modified: 2016-04-21  

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