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Study on Effect of Environment on Strength and Life of Micromaterials in Fatigue

Research Project

Project/Area Number 12650087
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKobe University

Principal Investigator

NAKAI Yoshikazu  Department of Mechanical Engineering, Kobe University, Professor, 工学部, 教授 (90155656)

Co-Investigator(Kenkyū-buntansha) HIWA Chiaki  Graduate School of Science and Technology, Kobe University, Research Associate, 自然科学研究科, 助手 (80294198)
Project Period (FY) 2000 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥3,800,000 (Direct Cost: ¥3,800,000)
Fiscal Year 2001: ¥1,300,000 (Direct Cost: ¥1,300,000)
Fiscal Year 2000: ¥2,500,000 (Direct Cost: ¥2,500,000)
KeywordsMicromaterial / Fatigue / Environment / Thin Film / Natotechnology / AFM / Fractography / Crack initiation / 交流電位差法
Research Abstract

Fatigue test systems were developed to study the fatigue mechanisms in metallic micro-materials. This system has an electro-dynamic actuator or an audio speaker as a loading device. Fatigue tests were conducted with commercially pure iron, or pure aluminum either in air or in sodium chloride solution, and fatigue life and fracture morphologies were observed. In either materials, and in either environment, scattering of fatigue lives were very large compared with conventional size specimens, and they were larger for smaller specimens. The effect of environment was not observed for short life region, and they were appreciable in long life region. Two types of fracture morphologies were observed.
For monitoring fatigue damage of micro materials, an A.C. potential method was developed. In iron, the value of potential were almost constant during fatigue process except for just before final fracture, while they continuously increased up to final unstable fracture in aluminum.
Fatigue test system for pure aluminum thin film was also developed in the present study. Two types of fatigue test specimen were made by electrolytic polishing and mechanical machining from aluminum foil whose thickness was 12 urn. The strength of specimen made by mechanical machining was larger than that of specimen made by electrolytic polishing. The variation in fatigue life of specimen made by electrolytic polishing was large compared with specimen made by mechanical machining. Both before and after the fatigue tests, slip-bands were observed by using optical microscopy and AFM. The spacing of slip bands in the thin film was found to be much larger than that of the bulk specimen.

Report

(3 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • Research Products

    (35 results)

All Other

All Publications (35 results)

  • [Publications] 中井善一: "CFRP積層板のモードII層間はく離疲労き裂伝ぱに及ぼす荷重繰返し速度及び環境の影響"日本機械学会論文集(A). 66. 1695-1702 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 中井善一: "70-30黄銅における疲労すべり帯の成長とき裂発生条件のAFMによる定量的評価"日本機械学会論文集(A). 67. 476-482 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 中井善一: "原子間力顕微鏡による疲労き裂発生の観察"材料試験技術. 46. 8-14 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Nakai: "Observations of Corrosion Fatigue Crack Initiation Processes in Metals by Means of AFM"Materials Science Research International, Special Technical Publication. 1. 101-106 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] A.Hashimoto: "Measurement of Fatigue Damage in Metallic Micro-Materials by an A.C. Potential Method"Materials Science for the 21st Century. Vol.B. 237-240 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Nakai: "Prediction of Fatigue Crack Initiation Life with Atomic-Force Microscopy"Proceedings of the SEM Annual Conference on Experimental and Applied Mechanics. 650-653 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Nakai: "Evaluation of Fatigue Damage and Fatigue Crack Initiation Process by Means of Atomic-Force Microscopy"Materials Science Research International. Vol.7,No.2. 73-81 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Nakai: "Scanning Atomic-force Microscopy on Initiation and Growth Behavior of Fatigue Slip-Bands in α-Brass"Fatigue and Fracture Mechanics : 32nd Volume, ASTM STP 1406. 122-135 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Taketoshi Kadowaki, and Chiaki Hiwa: "Effects of Frequency and Environment on Mode II Delamination Fatigue Crack Growth in CFRP Laminates"Transactions of Japanese Society of Mechanical Engineers (A). 66-649. 1695-1702 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Yoshikazu Nakai, Teppei Kusukawa: "Quantitative Evaluation of Slip-Band Growth and Crack Initiation in Fatigue of 70-30 Brass by Means of Atomic-Force Microscopy"Transactions of Japanese Society of Mechanical Engineers (A). 67-655. 476-482 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Yoshikazu NAKAI, Sanji FUJIWARA, Tomohiro OGAWA, and Yasuki SHIMIZU: "Observations of Corrosion Fatigue Crack Initiation Processes in Metals by Means of AFM"Materials Science Research International. Special Technical Publication-1. 101-106 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Akihisa Hashimoto and Yoshikazu Nakai: "Measurement of Fatigue Damage in Metallic Micro-Materials by an A.C. Potential Method"Materials Science for the 21st Century. Vol.B. 237-240 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Nakai, T. Kusukawa, and K. Maeda: "Prediction of Fatigue Crack Initiation Life with Atomic-Force Microscopy"Proceedings of the SEM Annual Conference on Experimental and Applied Mechanics. 650-653 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Yoshikazu Nakai: "Evaluatiion of Fatigue Damage and Fatigue Crack Initiation Process by Means ofr Atomic-Force Microscopy"Materials Science Research International. Vol.7, No.2. 73-81 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Nakai and T. Kusukawa: "Scanning Atomic-force Microscopy on Initiation and Growth Behavior of Fatigue Slip-Bands in α-Brass"Special Technical Publication of American Society for Testing and Materials. (ASTM STP1406). 122-135 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Nakai, T. Kusukawa, and K. Maeda: "Grain-Size Effect on Fatigue Crack Initiation Condition Observed by Using Atomic-Force Microscopy"Advances in Fracture Research (Proceedings of 10th International Conference on Fracture). CD-ROM. (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Nakai, Y. Shimizu, S. Fujiwara, and T. Ogawa: "Atomic-Force Microscopy of Corrosion Pits and Crack Initiation in Fatigue of Metals"Advances in Fracture Research (Proceedings of 10th International Conference on Fracture). CD-ROM. (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Yoshikazu Nakai and Chiaki Hiwa: "Effects of Loading Frequency and Environment on Delamination Fatigue Crack Growth of CFRP"International Journal of Fatigue. Vol.24. 161-170 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Nakai and K. Maeda: "Prediction of Crack Initiation under Cyclic Normal and Shear Stresses by Means of Atomic-Force Microscopy"Fatigue 2002. (to be published). (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Nakai: "Observations of Corrosion Fatigue Crack Initiation Processes in Metals by Means of AFM"Materials Science Research International, Special Technical Publication. 1. 101-106 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] A.Hashimoto: "Measurement of Fatigue Damage in Metallic Micro-Materials by an A.C. Potential Method"Materials Science for the 21st Century. Vol.B. 237-240 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Prediction of Fatigue Crack initiation Life with Atomic-Force Microscopy"Proceedings of the SEM Annual Conference on Experimental and Applied Mechanics. 650-653 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Evaluation of Fatigue Damage and Fatigue Crack Initiation Process by Means of Atomic-Force Microscopy"Materials Science Research International. Vol.7, No.2. 73-81 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Scanning Atomic-force Microscopy on Initiation and Growth Behavior of Fatigue Slip-Bands in α-Brass"Fatigue and Fracture Mechanics:32nd Volume, ASTM STP 1406. 122-135 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Grain-Size Effect on Fatigue Crack Initiation Condition Observed by Using Atomic-Force Microscopy"Advances in Fracture Research, Proceedings of 10th International Conference on Fracture. (CD-ROM). (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Atomic-Force Microscopy of Corrosion Pits and Crack Initiation in Fatigue of Metals"Advances in Fracture Research, Proceedings of 10th International Conference on Fracture. (CD-ROM). (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Nakai: "Prediction of Crack Initiation under Cyclic Normal and Shear Stresses by Means of Atomic-Force Microscopy"Fatigue 2002に掲載予定. (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] 中井善一: "CFRP積層板のモードII層間はく離疲労き裂伝ぱに及ぼす荷重繰返し速度及び環境の影響"日本機械学会論文集(A). 66. 1695-1702 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 中井善一: "70-30黄銅における疲労すべり帯の成長とき裂発生条件のAFMによる定量的評価"日本機械学会論文集(A). 67(3月号に掲載予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] 中井善一: "原子間力顕微鏡による疲労き裂発生の観察"材料試験技術. 46. 8-14 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Yoshikazu NAKAI: "Observations of Corrosion Fatigue Crack Initiation Processes in Metals by Means of AFM"Materials Science Research International, Special Technical Publication. 1(掲載予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Akihisa Hashimoto: "Measurement of Fatigue Damage in Metallic Micro-Materials by an A.C.Potential Method"Materials Science Research International, Special Technical Publication. (掲載予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Y.Nakai: "Prediction of Fatigue Crack Initiation Life with Atomic-Force Microscopy"2001 SEM Proceedings. (掲載予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Y.Nakai: "Grain-Size Effect on Fatigue Crack Initiation Condition Observed by Using Atomic-Force Microscopy"Proceedings of 10th International Conference on Fracture. (掲載予定). (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] Y.Nakai: "Atomic-Force Microscopy on Corrosion Pits and Crack Initiation in Fatigue of Metals"Proceedings of 10th International Conference on Fracture. (掲載予定). (2001)

    • Related Report
      2000 Annual Research Report

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Published: 2000-04-01   Modified: 2016-04-21  

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