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Grain Refinement of Al-Mg alloy by Hydrogenation Treatment and Its mechanism Analysis

Research Project

Project/Area Number 12650702
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionChiba Institute of Technology

Principal Investigator

FUNAMI Kunio  Chiba Inst. Of Technology, Faculty of Engineering, Professor, 工学部, 教授 (90010876)

Co-Investigator(Kenkyū-buntansha) 清水 秀治  千葉工業大学, 工学部, 助手 (30178983)
鈴木 浩治  千葉工業大学, 工学部, 講師 (70322427)
河野 紀雄  千葉工業大学, 工学部, 教授 (80083822)
Project Period (FY) 2000 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥3,400,000 (Direct Cost: ¥3,400,000)
Fiscal Year 2001: ¥1,200,000 (Direct Cost: ¥1,200,000)
Fiscal Year 2000: ¥2,200,000 (Direct Cost: ¥2,200,000)
KeywordsSociology of Organizations / Organizational Ecology / New institutionalism / Population Ecology / Community Ecology / Network / Australia / Organizational Evolution / 疲労 / 腐食 / 加工ひずみ法 / 脱水素処理
Research Abstract

The grain refinement is noticed, as method to enhance the strength of materials and to be appeared the superplasticity behavior. The subject of this study has shown that, in 5083AI (AI-Mg) alloy, this microstructure with fine grain size can be achieved by imposing extremely large plastic strains during work processing using characteristic properties such as hydrogen absorption and dehydrogenation at high temperature. Hydride precipitations MgH_2 obtained in this treatment were more useful to develop the high-density dislocation structure in alloy as dislocation pileup sources.
The following results of this study were obtained :
2001〜2001
1 : Hydrogenation treatment was carried out in 773K for 14. 4ks and in hydrogen atmosphere under 0. 4MPa. The hydrogenated samples were carried out heavy cold rolling with the 90% reduction ratio An existence of hydrides was determined by an X-ray diffraction analysis and TEM observation using tritium technique An induced hydrogen content was about 107×10 … More ^2 mass%. Then, to obtain the fine grain sized material, heat treatment was performed to do rapid recrystallization in salt bath. The materials were finally heated at 523K in vacuum (0. 1Pa) for dehydrogenation for 30hr. The residual hydrogen content was 0. 9×10^2 mass%. The hydrogenated samples indicates wavy deformation traces to be prevented easy deformation and shows more fine grain structure (2. 5 u m). Yield strength and tensile strength increased more than 1. 5times in comparison with that of non-hydrogenated specimen.
2 : An existence of hydrides was determined by an x-ray diffraction analysis and TEM observation using tritium technique. The grain size is finer with induced hydrogen content.
2001〜2002
1 : For superplasticity behavior of hydrogenated specimen, elongation was about 300% at 625K and 5×10^3 s^1 strain rate. The fatigue strength of these samples was 1. 8times higher than that of non-hydrogenated samples. However, in corrosion test, these samples did not indicate remarkable improvement. Less

Report

(3 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • Research Products

    (6 results)

All Other

All Publications (6 results)

  • [Publications] Kunio FUNAMI: "Grain Refinement and Superplasticity of Al-Mg Allou by Hydrogenation Treatment"Proceeding of Int. Cod. of PRICM4. 1983-1986 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 野田雅史: "アルミニウム合金の結晶粒微細化へ及ぼすひずみ負荷様式の影響"日本金属学会誌. 66. 101-108 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Kunio.FUNAMI and Ryusei.SANO: "gGrain Refinement and Superplasticity of AI-Mg Alloy by Hydrogenation Treatment"Iternational conference of PRICM4. 11. 1983-1986 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Masahumi Noda, Mitsuji Hirohashi, Kunio Funami, Yutaka SUWAHARA and Masaru KOBAYASHI: "Effect of Strain Loading Process on Grain Refinement in Aluminium Alloy"J.japan Inst.metals. 66. 101-108 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] 船見国男, 佐野龍聖: "水素吸蔵処理による5083A1材の結晶微細化と機械的特性"日本金属学会講演概要. 166

    • Related Report
      2001 Annual Research Report
  • [Publications] 佐野龍聖,船見国男: "水素吸蔵処理によるAl-Mg材の機械的特性"日本機械学会機械材料・材料加工技術講演会. 169-170 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 2000-04-01   Modified: 2016-04-21  

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