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Rapid Solidification of Supercooling Binary Molten Metal Droplets

Research Project

Project/Area Number 12650735
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Metal making engineering
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

FUKAI Jun  Department of chemical Engineering, Professor, 工学研究院, 教授 (20189905)

Project Period (FY) 2000 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2002: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2001: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2000: ¥1,800,000 (Direct Cost: ¥1,800,000)
Keywordsrapid solidification / molten metal / impact / binary / supercooling / spray forming / numerical
Research Abstract

A mathematical model describing the deformation and solidification behavior of molten metal droplets impinging on substrates is presented. The mathematical model is numerically solved using a finite element method. In the experiment, a molten tin droplet (2.2-4.3 mm diameter) impacts copper, stainless steel and glass substrates at various impact velocities (1.4-4.0 m/s). The values of the heat transfer coefficient at the droplet/substrate interface are evaluated by comparing the calculated splat diameters to the experimental ones. The estimated values are within the previously reported ranges. The model almost predicts the Weber number dependence of the experimental splat diameters. The time variations of the numerical splat diameters also agree with the experimental results. The simulation reveals that the frozen layer at the splat edge, rather than at the center region, affects the deceleration of the droplet spreading. The effect of the solidification on the splat diameter is explained from the freezing rate at the splat edge.
One-dimensional heat and mass transfer problems are numerically solved to predict microstructure development in alloy splats in rapid solidification. The model accounts for nonequilibrium solidification. The dendrite tip radius is estimated using an interface stability analysis. Model predictions are compared with microstructures of Sn-5wt.%Pb splats produced by depositing mono-size droplets on a Sn substrate. The droplet temperature at impact is controlled by adjusting the flight distance to the substrate. The deposit microstructures primarily match those predicted by the numerical simulation, although not perfectly. The discrepancies between the model predictions and the experimental observation are discussed.

Report

(4 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • 2000 Annual Research Report
  • Research Products

    (15 results)

All Other

All Publications (15 results)

  • [Publications] J.Fukai, T.Ozaki, K.Matsuura, O.Miyatake: "Solidification Phenomena during Collision of a Molten Metal Droplet on a Substrate"Proc.the International Conference on Spray Deposition and Melt Atomization. 627-639 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Y.Morozumi, M.Nakamono, J.Fukai, O.Miyatake: "Numerical Simulation of Coalescence and Separation Behavior during Binary Droplets Collision"Proc.8th International Conference on Liquid Atomization & Spray Systems. 878-885 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J.Fukai, T.Ozaki, H.Asami, O.Miyatake: "Numerical Simulation of Liquid Droplet Solidification on Substrates"Journal of Chemical Engineering of Japan. Vol.33. 630-637 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Y.Morozumi, M.Nakamoto, J.Fukai, O.Miyatake: "Head-On Collision Dynamics of Binary Liquid Droplet"Proc.5th Kyushu/Pusan-Kyoungnam & 4th Kyushu/Taipei Chemical Engineering Conference. 39-40 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 尾崎徹志, 深井 潤, 宮武 修: "壁面に衝突した溶解金属滴の凝固速度に及ぼす操作条件の影響"Thermal Science and Engineering. Vol.9. 9-17 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J.Fukai, T.Ando: "Microstructure development in alloy splats during rapid solidification"Proc.2nd Spray Deposition and Melt Atomization. (in press). (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J. Fukai, T. Ozaki, K. Matsuura and O. Miyatake: "Solidification Phenomena during Collision of a Molten Metal Droplet on a Substrate"Proc. The International Conference on Spray Deposition and Melt Atomization. 627-639 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Y. Morozumi, M. Nakamoto, J. Fukai and O. Miyatake: "Numerical Simulation of Coalescence and Separation Behavior during Binary Droplets Collision"Proc. 8th International Conference on Liquid Atomization & Spray Systems. 878-885 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J. Fukai, T. Ozaki, H. Asami and O. Miyatake: "Numerical Simulation of Liquid Droplet Solidification on Substrates"Journal of Chemical Engineering of Japan. Vol. 33. 630-637 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Y. Morozumi, M. Nakamoto, J. Fukai and O. Miyatake: "Head-On Collision Dynamics of Binary Liquid Droplet"Proc. 5th Kyushu/Pusan-Kyoungnam & 4th Kyushu/Taipei Chemical Engineering Conference. 39-40 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Thermal Science and Engineering. Vol. 9. 9-17 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] J. Fukai, T. Ando: "Microstructure development in alloy splats during rapid solidification"Proc. 2nd Spray Deposition and Melt Atomization. (in press). (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] T.Ozaki: "Effects of Operation Parameters on Freezing Rate of a Molten Metal Droplet Colliding with a Substrate"Thermal Science & Engineering. 9(6). 9-17 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] J.Fukai 他3名: "Solidification Phenomena during Collision of a Molten Metal Droplet on a Substrate"Proc.the International Conference on Spray Deposition and Melt Atomization. 627-639 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] J.Fukai 他3名: "Numerical Simulation of Liquid Droplet Solidification on Substrates"Journal of Chemical Engineering of Japan. 33-4. 630-637 (2000)

    • Related Report
      2000 Annual Research Report

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Published: 2000-04-01   Modified: 2016-04-21  

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