• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

Improbement of Oxidation Resistance and Its mechanisms in Fiber Reinforced Ceramic Matrix Composites

Research Project

Project/Area Number 12650895
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Aerospace engineering
Research InstitutionThe University of Tokyo (2001)
The University of Electro-Communications (2000)

Principal Investigator

ZHU Shijie  Institute of Industrial Science, The University of Tokyo, Associate Professor, 生産技術研究所, 助教授 (60283032)

Project Period (FY) 2000 – 2001
Project Status Completed (Fiscal Year 2001)
Budget Amount *help
¥1,800,000 (Direct Cost: ¥1,800,000)
Fiscal Year 2001: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 2000: ¥1,200,000 (Direct Cost: ¥1,200,000)
KeywordsComposite / SiC / Oxidation Resistance / Creep
Research Abstract

Creep and oxidation behavior of SiC/SiC composites were studied using macroscopic and microscopic experimental techniques and analysis methods in the past two years. To treat and analyze experimental data, a personal computer was bought in 2000. The results and achievements are summarized as follows.
(1) Creep tests were carried out in both air and argon to study the effects of oxidation on creep deformation and damage. SEM and EPMA were used to observe microstructures and measure element distribution in fiber, matrix and interfaces between fiber and matrix before and during creep-oxidation tests. The partial unloading technique was used to measure Young's modulus during creep tests, which is a indirect detection method for damage.
(2) Three methods for improving oxidation resistance were evaluated. It was found that the addition of glassy particulates in the matrix and glass-healing on surfaces are effective for improbement of oxidation and creep properties at high temperatures. The effects of the addition of glassy particulates in the matrix on creep crack growth were found. However, both of them were not effective at intermediate temperatures.
(3) The modification of interphase, e. g., using BN to replace carbon coating, is a good method, but BN is still not promising coating materials for fibers.
(4) It was found that stability of microstructure in fiber at high temperatures was also important on creep properties. This is why creep resistance of the composite in argon is lower than that in air if there is no severe oxidation on surfaces by glass-sealing.
(5) Based on experimental results and theoretical analysis, a method was proposed for life prediction at creep-oxidation and how to improve oxidation resistance was pointed out.
(6) The research results of this project were published on conferences and joumals. A few papers will be published in journals in the near future.

Report

(3 results)
  • 2001 Annual Research Report   Final Research Report Summary
  • 2000 Annual Research Report
  • Research Products

    (17 results)

All Other

All Publications (17 results)

  • [Publications] M.Mizuno, S.Zhu, Y.Kagawa: "Creep and cyclic fatigue behavior of SiC/SiC composites"Ceramic Engineering and Science Proceedings. 21. 433-444 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Kaneko, S.Zhu, Y.Ochi, T.Ogasawara, T.Ishikawa: "Effect of frequency on fatigue behavior in Tyranno fiber-reinforced SiC composites"Ceramic Engineering and Science Proceedings. 22. 553-560 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S.Zhu, Y.Kagawa: "Evaluation of creep behavior in SiC/SiC ceramic matrix composites"生産研究. 53. 466-469 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y.Miyashita, K.Kanda, S.Zhu, Y.Mutoh, M.Mizuno, A.J.McEvily: "Observations of fatigue damage process in SiC/SiC composites at room and elevated temperatures"Inter. J. Fatigue. 24. 241-248 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T.Ogasawara, T.Ishikawa, Y.Ohsawa, Y.Ochi, S.Zhu: "Tensile Creep Behavior and Thermal Stability of Orthogonal 3-D Woven Tyranno ZMI Fiber/Si-Ti-C-O Matrix Composites"J. Am. Ceram. Soc.. 85. 393-400 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M. Mizuno, S. Zhu, and Y. Kagawa: "Creep and cyclic fatigue behavior of SiC/SiC composites"Ceramic Engineering and Science Proceedings. Vol. 21, No. 3. 433-444 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] Y. Kaneko, S. Zhu, Y. Ochi, T. Ogasawara, T. Ishikawa: "Effect of frequency on fatigue behavior in Thyanno fiber-reinforced SiC composites"Ceramic Engineering and Science Proceedings. 22 (3). 553-560 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S. Zhu, and Y, Kagawa: "Evakution of creep behavior in SiC/SiC ceramic matrix composites"Seisan-Kenkyu. Vol. 53, No. 9・10. 466-469 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] S. Miyashita, K. Kanda, S. Zhu, Y. Mutoh, M. Mizuno, A. J. McEvily: "Observations of fatigue damage process in SiC/SiC composites at room and elevated temperatures"Inter. J. Fatigue. 24. 241-248 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] T. Ogasawara, T. Ishikawa, Y. Ohsawa, Y. Ochi, and S. Zhu: "Tensile Creep Behavior and Thermal Stability of Orthogonal 3-D Woven Tyranno ZMI Fiber/Si-Ti-C-O Matrix Composites"J. Am. Ceram. Soc. 85 (2). 393-400 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2001 Final Research Report Summary
  • [Publications] M.Mizuno, S.Zhu, Y.Kagawa: "Creep and cyclic fatigue behavior of SiC/SiC composites"Ceramic Engineering and Science Proceedings. 31・3. 433-444 (2000)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Kaneko, S.Zhu, Y.Ochi, T.Ogasawara, T.Ishikawa: "Effect of frequency on fatigue behavior in Tyranno fiber-reinforced SiC composites"Ceramic Engineering and Science Proceedings. 22・3. 553-560 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] S.Zhu, Y.Kagawa: "Evaluation of creep behavior in SiC/SiC ceramic matrix composites"生産研究. 53・9. 466-469 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Y.Miyashita, K.Kanda, S.Zhu, Y.Mutho, M.Mizuno, A.J.McEvily: "Observations of fatigue damage process in SiC/SiC composites at room and elevated temperatures"Inter. J. Fatigue. 24. 241-248 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] T.Ogasawara, T.Ishikawa, Y.Ohsawa, Y.Ochi, S.Zhu: "Tensile Creep Behavior and Thermal Stability of Orthogonal 3-D Woven Tyranno ZMI Fiber /Si-Ti-C-O Matrix Composites"J. Am. Carem. Soc.. 85・2. 393-400 (2002)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Mizuno,S.Zhu,Y.Kagawa: "Creep and cyclic fatigue behavior of SiC/SiC composites"Ceramic Engineering and Science Proc.. 21. 433-444 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] S.Zhu,M.Mizuno,Y.Kagawa: "Creep and Fracture of Engineering Materials and Structures"Trans Tech Publications Ltd. 755-762 (2000)

    • Related Report
      2000 Annual Research Report

URL: 

Published: 2000-04-01   Modified: 2016-04-21  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi