| Project/Area Number |
13555085
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| Research Category |
Grant-in-Aid for Scientific Research (B)
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| Allocation Type | Single-year Grants |
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| Section | 展開研究 |
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| Research Field |
Electronic materials/Electric materials
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| Research Institution | Tohoku University |
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Principal Investigator |
KUSHIBIKI Jun-ichi Tohoku University, Graduate school of Engineering, Professor, 大学院・工学研究科, 教授 (50108578)
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| Co-Investigator(Kenkyū-buntansha) |
MIYASHITA Masahito Tohoku University, Research Institute of Electrical Communication COE Research Fellow, 電気通信研究所, 非常勤研究員
TAKANAGA Izumi Tohoku University, Graduate school of Engineering, Research Associate, 大学院・工学研究科, 助手 (30323059)
ARAKAWA Mototaka Tohoku University, Graduate school of Engineering, Research Associate, 大学院・工学研究科, 助手 (00333865)
NAGAI Kunihiko Toyo Communication Equipment Co., Ltd., Quartz Products Department, Fundamental R&D Division, Division Manager, 水晶技術本部・技術材料部, 部長(研究職)
NISHINO Hideo Tohoku University, Graduate school of Engineering, Lecturer, 大学院・工学研究科, 講師 (50316890)
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| Project Period (FY) |
2001 – 2002
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| Project Status |
Completed (Fiscal Year 2002)
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| Budget Amount *help |
¥13,900,000 (Direct Cost: ¥13,900,000)
Fiscal Year 2002: ¥2,900,000 (Direct Cost: ¥2,900,000)
Fiscal Year 2001: ¥11,000,000 (Direct Cost: ¥11,000,000)
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| Keywords | Ultrasonic microspectroscopy / LFB / PW ultrasonic material characterization system / Synthetic α-quartz / Natural α-quartz / BAW velocity / LSAW velocity / Acoustical physical constants / Density / LFB超音波材料解析システム / 漏洩弾性表面波 / 誘電率 |
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| Research Abstract |
Ultrasonic microspectroscopy technology, using the line-focus-beam (LFB) and plane-wave (PW) ultrasonic material characterization (UMC) system, has been applied to establish evaluation techniques for synthetic α-quartz crystals for bulk acoustic wave (BAW) and surface acoustic wave (SAW) devices and to accurately measure the acoustical physical constants. The purpose of this study was to provide a new, worldwide guideline and standard for synthetic α-quartz in the industrial and scientific fields.
1. Measurement accuracies of the LFB ultrasonic material characterization system and bulk ultrasonic spectroscopy system have been improved.
2. Development of new methods for determining the acoustical physical constants of class-32 crystals and determination of the constants of synthetic and natural α-quartz:
(1) A new BAW method to accurately determine all of the independent components of the acoustical physical constants for class-32 crystals was developed. This method requires to measure lon
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gitudinal and shear velocities, dielectric constants, and density, using X-, Y-, and Z-cut specimens and several rotated Y-cut specimens. The demonstration was conducted for SAW-grade synthetic α-quartz. The results provided the constants that give BAW velocities within an accuracy of ±0.2 m/s (±0.004%).
(2) To compare the acoustic properties between natural and synthetic α-quartz, longitudinal and shear velocities, and LSAW velocities were measured using X-, Y-, and Z-cut specimens. All the velocity differences were within 1.00 m/s, and it was clarified that the acoustical physical constants of the natural quartz, were, very similar to those of synthetic quartz.
(3) Another new method for determining all the constants for class-32 crystals by measuring LSAW velocities in addition to BAW velocities for there principal X-, K and Z-cut specimens using the LFB/PW UMC system was developed. This method was applied for natural α-quartz.
(4) Precise values of the constants for natural quartz were also determined using the BAW method developed here.
3. BAW velocities. LSAW velocities, density and lattice parameters were measured for the specimens prepared from several synthetic α-quartz crystal ingots with different growth conditions. Slight velocity differences were detected. The velocity changes related to the impurity concentration, especially OH content, were different for the propagation directions and propagation modes. Lattice constant a was constant, but c became larger as the OH content became higher. Less
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