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Milli-second time-resolved HRTEM of absorption / desorption of hydrogen

Research Project

Project/Area Number 13555172
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Inorganic materials/Physical properties
Research InstitutionNagoya University

Principal Investigator

TANAKA Nobuo  Nagoya University, CIRSE, Professor, 理工科学総合研究センター, 教授 (40126876)

Co-Investigator(Kenkyū-buntansha) YAMASAKI Jun  Nagoya University, CIRSE, Assistant, 理工科学総合研究センター, 助手 (40335071)
WATANABE Hiroki  Denso Co, Basic Laboratory, researcher, 基礎研究所, 研究員
MUROOKA Yoshie  Nagoya University, Department of Electrical Engineering, Assistant, 工学研究科, 助手 (40273263)
Project Period (FY) 2001 – 2003
Project Status Completed (Fiscal Year 2003)
Budget Amount *help
¥13,500,000 (Direct Cost: ¥13,500,000)
Fiscal Year 2003: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2002: ¥2,700,000 (Direct Cost: ¥2,700,000)
Fiscal Year 2001: ¥10,100,000 (Direct Cost: ¥10,100,000)
KeywordsTime-resolved / TEM / Hydrogen-absorption / Milli-second / Atomistic observation / 時間分解TEM / 水素放出 / パラジウム / ランタンニッケル
Research Abstract

The objectives of the present study are (1) to develop a TEM instrument for observation of hydrogen -related reactions when hydrogen gas is introduced into the TEM column, and (2) to clarify the basic physical properties of the hydrogen-absorption materials.
In 2001-2002 we have constructed the instrument for the observation and made experiments on palladium clusters and LaNi_5 small crystals, whose results were published in the proceedings of PRICM-4. In 2002-2003, the image-analysis on the video tapes was carried out and the data were published in a journal "KNZOKU"(Japanese). Also another study related to decomposition of hydro-carbon by using the in-situ observation apparatus and the results were published in Applied Physics Letters.

Report

(4 results)
  • 2003 Annual Research Report   Final Research Report Summary
  • 2002 Annual Research Report
  • 2001 Annual Research Report
  • Research Products

    (14 results)

All Other

All Publications (14 results)

  • [Publications] K.Yoshida, J.Yamasaki, N.Tanaka: "In-situ HRTEM observation of photo-decomposition process of poly-hydrocarbon catalytic TiO_2 films"Applied Physics Letters. 84. 2542-2544 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] N.Tanaka, T.Kubota, K.Tanaka: "In-situ HRTEM observation of hydrogen-absorption material exposed to H_2"Adv.Mater.Processing. 1. 417-420 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] N.Tanaka, T.Kubota: "High-resolution and in-situ electron microscope observation of hydrogen-related reactions on nano-crystals"KINZOKU(Japanese). 72. 632-636 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 田中信夫(分担執筆): "ナノテクノロジーハンドブック 電子回折の項目"オーム社. 121-125 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Yoshida, J.Yamasaki, N.Tanaka: "In-situ HRTEM observation of photo-decomposition process of poly-hydrocarbon catalytic TiO_2 films"Applied Physics Letters. 84. 2542-2544 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] N.Tanaka, T.Kubota, K.Tanaka: "In-situ HRTEM observation of hydrogen-absorption material exposed to H_2"Adv.Mater.Processing. 1. 417-420 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] N.Tanaka, T.Kubota: "High-resolution and in-situ electron microscope observation of hydrogen-related reactions on nano-crystals"KINZOKU(Japanese). 72. 632-636 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] K.Yoshida, J.Yamasaki, N.Tanaka: "In-situ HRTEM observation of photo-decomposition process of poly-hydrocarbon on catalytic TiO_2 films"Applied Physics Letters. (in print). 1 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 田中信夫(分担執筆): "ナノテクノロジーハンドブック 電子回打の項目"オーム社. 934 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 田中信夫: "ナノ結晶の水素化反応の高分解能その場電子顕微鏡観察"金属. 72・7. 632-636 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Tanaka, M.Sowa, Y.Kita, T.Kubota, N.Tanaka: "Hydrogen storage properties of amorphous at nano crystalline Zr-Ni-V alloys"J. Alloys at Compounds. 330・8. 732-737 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] J.Yin, K.Tanaka, N.Tanaka: "Hydrogen-storage properties at structure characterization of melt-spun and annealed Mg-Ni-Nd alloy"Mater. Trans JIM. 43・3. 417-420 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 平山司, 幾原雄一, 田中信夫: "透過電子顕微鏡によるその場計測技術と超高分解能観察"まてりあ. 41・9. 598-603 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] K.Tanaka, M.Sowa, Y.Kita, T.Kubota, N.Tanaka: "Hydrogen Storage Properties of Amorphous at Nanocrystalliue Zr-Ni-V Alleys"J.Alloys and Compounds. 330/332. 732-737 (2002)

    • Related Report
      2001 Annual Research Report

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Published: 2001-04-01   Modified: 2016-04-21  

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