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SCANNING PROBE MICROSCOPIC OBSERVATION AND DIELECTRIC MEASUREMENTS ON FERROELECTRIC POLYCRYSTALLINE MATERIALS

Research Project

Project/Area Number 13640336
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 固体物性Ⅰ(光物性・半導体・誘電体)
Research InstitutionIWAKI MEISEI UNIVERSITY

Principal Investigator

TAKASHIGE M.  IWAKI MEISEI UNIVERSITY, FACULTY OF SCIENCE AND ENGINEERING, DEPARTMENT OF ELECTRONICS AND COMPUTER SCIENCE, PROFESSOR, 理工学部, 教授 (70114527)

Co-Investigator(Kenkyū-buntansha) HAMAZAKI S.i.  FUKUSHIMA NATIONAL COLLEGE OF TECHNOLOGY, ASSOCIATE PROFESSOR, 助教授 (20306096)
SHIMIZU F.  IWAKI MEISEI UNIVERSITY, FACULTY OF SCIENCE AND ENGINEERING, ASSOCIATE PROFESSOR, 理工学部, 助教授 (20206212)
Project Period (FY) 2001 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2002: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2001: ¥3,000,000 (Direct Cost: ¥3,000,000)
Keywordsdomain / ferroelectric / amorphous / SPM / rochelle salt / barium titanate / bismuth titanate / lithium niobate / 結晶化 / ロッシエル塩
Research Abstract

Main purpose of this project is to visualize surface structure by scanning probe microscopic (SPM) and to measure dielectric properties for the following four materials, crystalline NaKC_4H_4O_64H_2O (rochelle salt) and BaTiO_3, and amorphous Bi_4Ti_3O_<12> and LiNbO_3.
For crystalline samples of NaKC_4H_4O_64H_2O, topographic images in the creation and disappearance process of monoclinic domains were taken with variation of temperature. Also for BaTiO_3, the surface morphology at the crossing of two kinds of 90° domain boundaries was visualized. For amorphous samples of Bi_4Ti_3O_<12> and LiNbO_3 prepared by rapid quenching, the crystallization process from the amorphous state was investigated on heating. SPM images of the samples by annealing at several different temperatures were taken. The sensitive change in hardness distribution images due to the glass transition and the development of the crystal grain growth due to crystallization were realized.
Other than surface imagings and dielectric measurements, material syntheses of halide ferroelectrics having formula A_2BX_4 type were also made.

Report

(3 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • Research Products

    (19 results)

All Other

All Publications (19 results)

  • [Publications] S.Kojima 他6名: "Crystallization of Amorphous Bismuth Titanate"J.Non-Crystalline Solids. 293-295. 250-254 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige 他6名: "Dielectric Properties of Crystallization Process from Amorphous Bi_4Ti_3O_<12>"Japanese Journal of Applied Physics. 40. 5816-5818 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige, S.I.Hamazaki: "An Attempt to Observe Surface Morphology of NaKC_4H_4O_6・4H_2O by Atomic Force Microscope"Ferroelectrics. 266. 125-130 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige 他5名: "Dielectric Properties and Crystallization in Amorphous Bi_4Ti_3O_<12>"Japanese Journal of Applied Physics. 41. 7211-7213 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] F.Shimizu 他3名: "Search for New Ferroelectrics in Tl_2ZnI_4 Group"Ferroelectrics. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] F.Shimizu, M.Takashige: "Dielectric Properties of the Mixed System of (Cs_<1-x>Rb_x)_2HgI_4"Journal of Korean Physical Society. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] S.Kojima et al: "Crystallization of Amorphous Bismuth Titanat"J.Non-Crystalline Solids. 293-295. 250-254 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige et al: "Dielectric Properties of Crystallization Process from Amorphous Bi_4Ti_3O_<12>"Jpn.J.Appl.Phys.. 40. 5816-5818 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige and S.Hamazaki: "An Attempt to Observe Surface Morphology of NaKC_4H_4O_6・4H_2O by Atomic Force Microscope"Ferroelectrics. 266. 125-130 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige et al: "Dielectric Properties and Crystallization in Amorphous Bi_4Ti_3O_<12>"Jpn.J.Appl.Phys.. 41. 7211-7213 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] F.Shimizu et al: "Search for New Ferroelectrics in Tl_2ZnI_4 Group"Ferroelectrics. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] F.Shimizu and M.Takashige: "Dielectric Properties of the Mixed System of(Cs_<1-x>Rb_x)_2HgI_4"J.Kor.Phys.Soc.. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] M.Takashige, S.Hamazaki: "An Attempt to Observe Surface Morphology of NaKC_4H_4O_6・4H_2O by Atomic Force Microscope"Ferroelectrics. 266. 125-130 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] M.Takashige他5名: "Dielectric Properties and Crystallization in Amorphous Bi_4Ti_3O_<12>"Japanese Journal of Applied Physics. 41. 7211-7213 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] F.Shimizu他3名: "Search for New Ferroelectrics in Tl_2ZnI_4 Group"Ferroelectrics. (印刷中).

    • Related Report
      2002 Annual Research Report
  • [Publications] F.shimizu, M.Takashige: "Dielectric Properties of the Mixed System of (Cs_<1-x>Rb_x)_2HgI_4"Journal of Korean Physical Society. (印刷中).

    • Related Report
      2002 Annual Research Report
  • [Publications] M.Takashige他6名: "Dielectric Properties of Crystallization Process from Amorphous Bi_4Ti_3O_<12>"Japanese Journal of Applied Physics. 40. 5816-5818 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] S.Kojima他6名: "I Crystallization of Amorphous Bismuth Titanate"Journal of Non-Crystalline Solids. 293-295. 250-254 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] M.Takashige他1名: "An Attempt to Observe Surface Morphology of NaKC_4H_4O_6・4H_2O by Atomic Force Microscope"Ferroelectrics. (印刷中). (2002)

    • Related Report
      2001 Annual Research Report

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Published: 2001-04-01   Modified: 2020-05-15  

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