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Synthesis of crystallite-dispersed nano-composites by ion implantation into amorphous alloys

Research Project

Project/Area Number 13650724
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionMusashi Institute of Technology

Principal Investigator

WAKABAYASHI Hidehiko  Musashi Institute of Technology, Faculty of Engineering, Assistant Professor, 工学部, 助教授 (50267340)

Co-Investigator(Kenkyū-buntansha) TORIYAMA Tamotsu  Musashi Institute of Technology, Faculty of Engineering, Professor, 工学部, 教授 (40016176)
Project Period (FY) 2001 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 2002: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 2001: ¥1,300,000 (Direct Cost: ¥1,300,000)
Keywordsion implantation / amorphous alloys / crystalline / nano-composite / implantation temperature / synthesis process / 結晶化 / 微粒子
Research Abstract

The applicability of ion-implantation induced local crystallization of amorphous alloys to the synthesis of crystal/amorphous nano-composites was studied. Helium ions were used as implant species since they are chemically most inactive. For target materials, Fe-B and Fe-Si-B alloys were used as representatives of metal- metalloid type amorphous alloys, whereas Fe-Zr alloy was selected as typical metal-metal type amorphous alloy. After installing a unit for precision control of implantation temperature, implantations were conducted on Fe-B alloy samples. However, systematic preparation of implanted samples was not possible due to the malfunction of the ion implanter. Thus the following were concluded from the results only on Fe-B alloys: 1) the amount of induced crystalline phase increases with increasing dose and saturates at high doses; the dose dependence becomes moderated by lowering implantation temperature so that the amount becomes well controllable, 2) no significant change is observed in local structure and in thermal stability after implantation if doses are below the critical dose for crystallization, 3) when the amount of induced crystalline phase is small, crystalline fine particles are magnetically isolated from the residual amorphous phase(s), 4) crystalline fine particles seems to grow by integrating neighboring parlicles, which are unfavorable for the present purpose because amount and size of crystalline particles cannot be controlled independently. The comparison with the results for Fe-Si-B and Fe-Zr will be reported as soon as possible.

Report

(3 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • Research Products

    (3 results)

All Other

All Publications (3 results)

  • [Publications] Hidehiko Wakabayashi: "The Effect of Temperature during Helium Ion Implantation-Induced Crystallization of Iron-Based Amorphous Alloys"Proc.14th Int.Conf.Ion Implantation Technology. (to be published by IEEE). (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Hidehiko Wakabayashi: "The Effect of Temperature during Helium Ion Implantation-Induced Crystallization of Iron-Based Amorphous Alloys"Proc. 14th Int. Conf. Ion Implant. Tech.. (to be published by IEEE). (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Hidehiko Wakabayashi: "The Effect of Temperature during Helium Ion Implantation-Induced Crystallization of Iron-Based Amorphous Alloys"Proc. 14th Int. Conf. Ion Implantation Technology (to be published, accepted on Dec. 24^<th>24, 2002). (受理).

    • Related Report
      2002 Annual Research Report

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Published: 2001-04-01   Modified: 2016-04-21  

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