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Production of High Toughness Martensitic Stainless Steel using Partial Solution Treatment

Research Project

Project/Area Number 13650801
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Metal making engineering
Research InstitutionKyushu University

Principal Investigator

TAKAKI Setsuo  Kyushu University, Faculty of Engineering, Professor, 大学院・工学研究院, 教授 (90150490)

Co-Investigator(Kenkyū-buntansha) TOMIMURA Kouki  Nisshin Steel Co.Ltd., ステンレス高合金研究部, 主任研究員
Project Period (FY) 2001 – 2002
Project Status Completed (Fiscal Year 2002)
Budget Amount *help
¥3,300,000 (Direct Cost: ¥3,300,000)
Fiscal Year 2002: ¥1,400,000 (Direct Cost: ¥1,400,000)
Fiscal Year 2001: ¥1,900,000 (Direct Cost: ¥1,900,000)
Keywordspartial solution treatment / martensitic stainless steel / carbide / grain size / toughness / 未固溶炭化物 / オーステナイト粒径
Research Abstract

For the purpose of developing a process for toughening of martensitic stainless steels using Partial Solution treatment, techniques for the carbide dispersion treatment and the nucleation-site control of ferrite by dispersed carbide particles were proposed. Concretely, the Partial Solution treatment (re-solution treatment in dual-phase region of austenite and M23C6 after quench-and-tempering) enabled to disperse the carbide of O.3μm in diameter homogeneously within austenite matrix and to increase the frequency of nucleation markedly in γ-α transformation on cooling. By this effect, equiaxed fine ferritic structure with random crystallographic orientation distribution was obtained and the ductility and formability of conventional steel that "high strength but low ductility" was remarkably improved. The strength-ductility balance was investigated by means of tensile testing at Kyushu University, and then it was clarified that each of uniform elongation, work hardening and necking strain was enlarged significantly. The formability of the developed steel was evaluated in terms of deep drawability at Nisshin Steel co., ltd. And it was found that the developed steel could be easily formed without the problem of cracking during the deep drawing. In addition, it is possible to perform the microstructural control only by the heat treatment without deformation process so that large-sized materials were confirmed to be produced on the practical manufacturing line without any problem. On the other hand, the mechanism of the microstructure development was revealed by using transmission electron microscopy or X ray analysis, and then the heat treatment condition was also optimized with kinetics derived from diffusion theory.

Report

(3 results)
  • 2002 Annual Research Report   Final Research Report Summary
  • 2001 Annual Research Report
  • Research Products

    (17 results)

All Other

All Publications (17 results)

  • [Publications] 三上真人, 土山聡宏, 高木節雄: "12%Cr-0.3%C鋼における恒温変態挙動"鉄と鋼. 87・1. 49-54 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 稲葉智一, 三上真人, 小野嘉則, 土山聡宏, 高木節雄: "部分溶体化処理した12%Cr-0.3%C鋼の恒温変態挙動"鉄と鋼. 87・9. 613-618 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Toshihiro TSUCHIYAMA, Yuji MIYAMOTO, Setsuo TAKAKI: "Recrystallization of Lath Martensite with Bulge Nucleation and Growth Mechanism"ISIJ International. 41・9. 1047-1052 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Toshihiro TSUCHIYAMA, Setsuo TAKAKI: "Recrystallization Mechanism of Lath Martensite in High Chromium Steel"Recrystallization and Grain Growth Volume 2. 803-808 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Masato MIKAMI, Toshihiro TSUCHIYAMA and Setsuo TAKAKI: "Isothermal Transformation Behavior in 12%Cr-0.3%C Steel"Tetsu-to-Hagane. Vol.87. 49-54 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Hirokazu INABA, Masato MIKAMI, Yoshinori ONO, Toshihiro TSUCHIYAMA and Setsuo TAKAKI: "Isothermal Transformation Behavior in 12%Cr-0.3%C Steel with Partial Solution Treatment"Tetsu-to-Hagane. Vol.87. 613-618 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Toshihiro TSUCHIYAMA, Yuji MIYAMOTO and Setsuo TAKAKI: "Recrystallization of Lath Martensite with Bulge Nucleation and Growth Mechanism"ISIJ International. Vol.41. 1047-1052 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] Toshihiro TSUCHIYAMA and Sestuo TAKAKI: "Recrystallization Mechanism of Lath Martensite in High Chromium Steel"Recrystallization and Grain Growth. Volume 2. 803-806 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2002 Final Research Report Summary
  • [Publications] 三上真人, 土山聡宏, 高木節雄: "12%Cr-0.3%C鋼における恒温変態挙動"鉄と鋼. 87・1. 49-54 (2001)

    • Related Report
      2002 Annual Research Report
  • [Publications] 稲葉智一, 三上真人, 小野嘉則, 土山聡宏, 高木節雄: "部分溶体化処理した12%Cr-0.3%C鋼の恒温変態挙動"鉄と鋼. 87・9. 613-618 (2001)

    • Related Report
      2002 Annual Research Report
  • [Publications] Toshihiro TSUCHIYAMA, Yuji MIYAMOTO, Setsuo TAKAKI: "Recrystallization of Lath Martensite with Bulge Nucleation and Growth Mechanism"ISIJ International. 41・9. 1047-1052 (2001)

    • Related Report
      2002 Annual Research Report
  • [Publications] Toshihiro TSUCHIYAMA, Setsuo TAKAKI: "Recrystallization Mechanism of Lath Martensite in High Chromium Steel"Recrystallization and Grain Growth Volume 2. 803-808 (2001)

    • Related Report
      2002 Annual Research Report
  • [Publications] 高野光司, 土山聡宏, 高木節雄: "12%Cr-0.1%C鋼の等温変態により析出する炭化物の分散状態に及ぼす前加工の影響"鉄と鋼. 88・11. 779-785 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 三上真人, 土山聡宏, 高木節雄: "12%Cr-0.3%C鋼における恒温変態挙動"鉄と鋼. 87・1. 49-54 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] 稲葉智一, 三上真人, 小野嘉則, 土山聡宏, 高木節雄: "部分溶体化処理した12%Cr-0.3%C鋼の恒温変態挙動"鉄と鋼. 87・9. 613-618 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Toshihiro TSUCHIYAMA, Yuji MIYAMOTO, Setsuo TAKAKI: "Recrystallization of Lath Martensite with Bulge Nucleation and Growth Mechanism"ISIJ International. 41・9. 1047-1052 (2001)

    • Related Report
      2001 Annual Research Report
  • [Publications] Toshihiro TSUCHIYAMA, Setsuo TAKAKI: "Recrystallization Mechanism of Lath Martensite in High Chromium Steel"Recrystallization and Grain Growth Volume 2. 803-808 (2001)

    • Related Report
      2001 Annual Research Report

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Published: 2001-04-01   Modified: 2016-04-21  

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