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Microstructure control of ferrous martensite by defects inherited from austenite

Research Project

Project/Area Number 14205104
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionKyoto University

Principal Investigator

MAKI Tadashi  Kyoto University, Department of Materials Science and Engineering, Professor, 工学研究科, 教授 (10026247)

Co-Investigator(Kenkyū-buntansha) FURUHARA Tadashi  Kyoto University, Department of Materials Science and Engineering, Associate Professor, 工学研究科, 助教授 (50221560)
MORITO Shigekazu  Kyoto University, Department of Materials Science and Engineering, Research Associate, 工学研究科, 助手 (00301242)
Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥32,370,000 (Direct Cost: ¥24,900,000、Indirect Cost: ¥7,470,000)
Fiscal Year 2004: ¥3,250,000 (Direct Cost: ¥2,500,000、Indirect Cost: ¥750,000)
Fiscal Year 2003: ¥13,260,000 (Direct Cost: ¥10,200,000、Indirect Cost: ¥3,060,000)
Fiscal Year 2002: ¥15,860,000 (Direct Cost: ¥12,200,000、Indirect Cost: ¥3,660,000)
Keywordssteel / phase transformation / martensite / dislocation / precipitation / strength / shape memory alloy / thermomechanical processing
Research Abstract

(1)Inheritance of matrix dislocation and precipitate into martensite
In ausformed lath martensite in Fe-20%Ni-5.5%Mn, dislocations introduced in the austenite are inherited into martensite with the Bain correspondence. γ'-Ni3Al precipitated in the austenite of Fe-31%Ni-10Co-3Ti is inherited into thin-plate martensite. When γ', which has a finer size due to a short aging, changes its structure by transformation shear, thermally elastic martensite is formed in the cooling. When the γ' size gets larger by prolonged aging, no structure change occurs for γ' and athermal martensite is formed in the cooling.
(2)Refinement of lath martensite by precipitation
Lath martensite packets/blocks are refined by decreasing austenite grain size in Fe-(1.5,2)Mn-0.2C alloys. In the austenite of which grain size is about 2μm with pinning by alloy carbide, a block size of 1μm was obtained. The strength of the as-quenched martensite increases by following a Hall-Petch type relation against the block size. Finely dispersed V(C,N) particles are capable of refining the lath martensite structure.
(3)The change of martensite/bainite substructure with inherited dislocations
In lenticular martensite, substructure changes from twinning to dislocations. Near the martensite/austenite interface, the austenite contains tangled dislocations due to plastic accommodation of transformation strain. Similar tangled dislocations are also observed in the martensite, resulting in local lattice orientation near the interface. It is concluded that those dislocations are inherited from the surrounding austenite. It is observed that the deformation of austenite prior to transformation (ausforming) refines lath martensite structures but results in the coarsening of upper bainite structures in Fe-Ni alloys.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (28 results)

All 2005 2004 2003 2002 Other

All Journal Article (20 results) Publications (8 results)

  • [Journal Article] Effect of austenite grain size on the morphology and crystallography of lath martensite in low carbon steels2005

    • Author(s)
      S.Morito, H.Saito, T, Ogawa, T.Furuhara, T.Maki
    • Journal Title

      ISIJ International Vol.45

      Pages: 91-94

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Local orientation change inside lenticular martensite in Fe-33Ni alloy2005

    • Author(s)
      A.Shibata, S.Morito, T.Furuhara, T.Maki
    • Journal Title

      Scripta Materialia (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of austenite grain size on the morphology and crystallography of lath martensite in low carbon steels2005

    • Author(s)
      S.Morito, H.Saito, T.Ogawa, T.Furuhara, T.Maki
    • Journal Title

      ISIJ International Vol.45, No.1

      Pages: 91-94

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Local orientation change inside lenticular martensite in Fe-33Ni alloy2005

    • Author(s)
      A Shibata, S.Morito, T.Furuhara, T.Maki
    • Journal Title

      Scripta Materialia (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of austenite grain size on the morphology and crystallography of lath martensite in low carbon steels2005

    • Author(s)
      S.Morito, H.Saito, T.Ogawa, T.Furuhara, T.Maki
    • Journal Title

      ISIJ International Vol.45 No.1

      Pages: 91-94

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Enhanced Structural Evolution by Martensitic Transformation and Deformation of IF Steels2004

    • Author(s)
      S.Morito, X.Huang, T.Furuhara, T.Maki, N.Hansen
    • Journal Title

      Proc.of the 25^<st> Ris0 International Symposium on Materials Science

      Pages: 453-458

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Control of Cementite Precipitation in Lath Martensite by Rapid-heating Tempering2004

    • Author(s)
      T.Furuhara, K.Kobayashi, T.Maki
    • Journal Title

      ISIJ International Vol.44

      Pages: 1937-1944

    • NAID

      10013963732

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Enhanced Structural Evolution by Martensitic Transformation and Deformation of IF Steels2004

    • Author(s)
      S.Morito, X.Huang, T.Furuhara, T.Maki, N.Hansen
    • Journal Title

      Proc.of the 25^<st> Risφ International Symposium on Materials Science

      Pages: 453-458

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Control of Cementite Precipitation in Lath Martensite by Rapid-heating Tempering2004

    • Author(s)
      T.Furuhara, K.Kobayashi, T.Maki
    • Journal Title

      ISIJ International Vol.44, No.11

      Pages: 1937-1944

    • NAID

      10013963732

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Control of Cementite Precipitation in Lath Martensite by Rapid-heating Tempering2004

    • Author(s)
      T.Furuhara, K.Kobayashi, T.Maki
    • Journal Title

      ISIJ International Vol.45 No.1

      Pages: 1937-1944

    • NAID

      10013963732

    • Related Report
      2004 Annual Research Report
  • [Journal Article] The Morphology and Crystallography of Lath Martensite in Fe-C Alloys2003

    • Author(s)
      S.Morito, H.Tanaka, R.Konishi, T.Furuhara, T.Maki
    • Journal Title

      Acta Materialia Vol.51

      Pages: 1789-1799

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Morphology, substructure and crystallography of lath martensite in Fe-C alloys2003

    • Author(s)
      T.Furuhara, S.Morito, T.Maki
    • Journal Title

      Journal de Physique IV France Vol.112

      Pages: 255-258

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Interphase boundary structures of lath martensite and bainite in steel2003

    • Author(s)
      T.Furuhara, N.Miyajima, T.Moritani, T.Mak
    • Journal Title

      Journal de Physique IV France Vol.112

      Pages: 319-322

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Microstructure of ausformed lath martensite in 18%Ni maraging steel2003

    • Author(s)
      S.Morito, I.Kishida, T.Maki
    • Journal Title

      Journal de Physique IV France Vol.112

      Pages: 453-456

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Dislocation density in lath martensite in Fe-C and Fe-Ni alloys2003

    • Author(s)
      S.Morito, J.Nishikawa, T.Maki
    • Journal Title

      ISIJ International Vol.43

      Pages: 1475-1477

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The Morphology and Crystallography of Lath Martensite in Fe-C Alloys2003

    • Author(s)
      S.Morito, H.Tanaka, R.Konishi, T.Furuhara, T.Maki
    • Journal Title

      Acta Materialia Vol.51, No.6

      Pages: 1789-1799

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Interphase boundary structures of lath martensite and bainite in steel2003

    • Author(s)
      T.Furuhara, N.Miyajima, T.Moritani, T.Maki
    • Journal Title

      Journal de Physique IV France Vol.112

      Pages: 319-322

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Dislocation density in lath martensite in Fe-C and Fe-Ni alloys2003

    • Author(s)
      S.Morito, J.Nishikawa, T.Maki
    • Journal Title

      ISIJ International Vol.43, No.9

      Pages: 1475-1477

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Comparison of interphase boundary structure between bainite and martensite in steel2002

    • Author(s)
      T.Moritani, N.Miyajima, T.Furuhara, T.Maki
    • Journal Title

      Scripta Materialia Vol.47

      Pages: 193-199

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Comparison of interphase boundary structure between bainite and martensite in steel2002

    • Author(s)
      T.Moritani, N.Miyajima, T.Furuhara, T.Maki
    • Journal Title

      Scripta Materialia Vol.47, No.3

      Pages: 193-199

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Publications] S.Morito, H.Tanaka, R.Konishi, T.Furuhara, T.Maki: "The Morphology and Crystallography of Lath Martensite in Fe-C Alloys"Acta Materialia. 51・6. 1789-1799 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Moritani, N.Miyajima, T.Furuhara, T.Maki: "Comparison of interphase boundary structure between bainite and martensite in steel"Scripta Materialia. 47・3. 193-199 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Furuhara, S.Morito, T.Maki: "Morphology, substructure and crystallography of lath martensite in Fe-C alloys"Journal de Physique IV France. 112. 255-258 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Furuhara, N.Miyajima, T.Moritani, T.Maki: "Interphase boundary structures of lath martensite and bainite in steel"Journal de Physique IV France. 112. 319-322 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] S.Morito, J.Nishikawa, T.Maki: "Dislocation density in lath martensite in Fe-C and Fe-Ni alloys"ISIJ International. 43・9. 1475-1477 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] S.Morito, T.Furuhara, T.Maki: "Morphology, substructure and crystallography of lath martensite in Fe-C alloys"Proc.Inter.Conf.Martensitic Transformations (ICOMAT'02). (印刷中). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] T.Furuhara, N.Miyajima, T.Moritani, T.Maki: "Interphase boundary structures of lath martensite and bainite in steel"Proc.Inter.Conf.Martensitic Transformations (ICOMAT'02). (印刷中). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] S.Morito, H.Tanaka, R.Konishi, T.Furuhara, T.Maki: "The morphology and crystallography of lath martensite in Fe-C alloys"Acta Materialia. Vol.51,No.6. 1789-1799 (2003)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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