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Observation of lattice defects, deformation behavior in duplex alloys and evaluation of their lifetime using magnetic properties.

Research Project

Project/Area Number 14205105
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionOsaka University

Principal Investigator

UMAKOSHI Yukichi  Osaka University, Graduate School of Engineering, Professor, 大学院・工学研究科, 教授 (00029216)

Co-Investigator(Kenkyū-buntansha) NAKANO Takayoshi  Osaka University, Graduate School of Engineering, Associate Professor, 大学院・工学研究科, 助教授 (30243182)
YASUDA Hiroyuki  Osaka University, Center of Ultra high Voltage Electronmicroscope, Associate Professor, 超高圧電子顕微鏡センター, 助教授 (60294021)
Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥54,730,000 (Direct Cost: ¥42,100,000、Indirect Cost: ¥12,630,000)
Fiscal Year 2004: ¥8,580,000 (Direct Cost: ¥6,600,000、Indirect Cost: ¥1,980,000)
Fiscal Year 2003: ¥17,290,000 (Direct Cost: ¥13,300,000、Indirect Cost: ¥3,990,000)
Fiscal Year 2002: ¥28,860,000 (Direct Cost: ¥22,200,000、Indirect Cost: ¥6,660,000)
KeywordsSpontaneous magnetization / coercive force / paramagnetism / fatigue / deformation / superparamagnetism / material reliability / superalloy / 超常磁性 / 格子欠陥 / 転位 / 磁気特性 / 破壊 / 信頼性 / 面欠陥 / 磁性 / 硬化 / 疲労軟化
Research Abstract

Numerous dislocations and planar faults in metallic materials are introduced during fatigue deformation. Stress concentration near high density of lattice defects initiates a microcrack and finally fracture occurs. To understand the deformation mechanism and evaluate the reliability observation of lattice defects such as dislocations is necessary.. In general, the observation of lattice defects is performed using electron microscope. However, it is very difficult to obtain exact information about nature of dislocations due to high residual stress near the dislocations. It is known that magnetic properties are very sensitive to lattice defects in ferromagnetic materials. The lattice defects have been observed by magnetic technique. In this work, deformation behavior of FeAl, Fe_3Al and Ni_3(Al,Ti) containing small γ precipitates single crystals were prepared and their fatigue behavior was examined by magnetic technique. High-field susceptibility and spontaneous magnetization in FeAl and Fe_3Al were influenced by deformation. Type of dislocation and planar faults were determined by anisotropy of high field susceptibility. Lifetime of FeAl can be estimated by monitoring spontaneous magnetization because the spontaneos magnetization rapidly increases just before fracture during fatigue.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (38 results)

All 2005 2004 2003 2002 Other

All Journal Article (28 results) Book (1 results) Publications (9 results)

  • [Journal Article] Nondestructive damage evaluation of γ'-Ni_3(Al,Ti) single crystals containing disordered γ precipitates.2005

    • Author(s)
      H.Y.Yasuda, T.Yanai, Y.Umakoshi
    • Journal Title

      Journal of Applied Physics (in press)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Quantitative analysi of γ precipitates in cyclically deformed Ni_3(Al,Ti) single crystals using magnetic technique.2005

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda, Y.Yanai
    • Journal Title

      Mat.Res.Soc.Symp.Proc. (in press)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestructive damage evaluation for γ'-Ni_3(Al, Ti) single crystals containing disordered γ precipitates2005

    • Author(s)
      H.Y.Yasuda, T.Hatta, Y.Umakoshi
    • Journal Title

      J.Appl.Phys. (in press)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Quantitative analysis of y precipitates in cyclically deformed Ni_3(Al, Ti) single crystals using magnetic technique2005

    • Author(s)
      Y.Umakoshi, H.Yasuda, T.Yanai
    • Journal Title

      Mat.Res.Soc.Symp. (in press)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Magnetic observation of deformation substructure in cyclically deformed Fe3Al single crystals2004

    • Author(s)
      H.Y.Yasuda, T.Hatta, Y.Umakoshi
    • Journal Title

      Science and Technology of Advanced Materials 5

      Pages: 3-9

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestruction lifetime prediction by magnetic measurements2004

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Encyclopedia of Materials, Science and Technology

      Pages: 1-9

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestructive devaluation of lifetime of intermetallics using magnetic properties2004

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Kensa-Gijyutsu 11

      Pages: 13-18

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Magnetic observation of deformation substructure in cyclically deformed Fe_3Al Single crystals.2004

    • Author(s)
      H.Y.Yasuda, T.Hatta, Y.Umakoshi
    • Journal Title

      Science and Technology of Advanced Materials 5

      Pages: 3-9

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestruction lifetime Prediction by magnetic measurements.2004

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Encyclopedia of Materials, Science and Technology

      Pages: 1-9

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestructive evaluation of lifetime of intermetallics using magnetic properties.2004

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Kensa-Gijyutsu 11

      Pages: 13-18

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Magnetic observation of deformation substructure in cyclically deformed Fe3Al single crystals2004

    • Author(s)
      H.Y.Yasuda, T.Hatta, Y.Umakoshi
    • Journal Title

      Sci.Tech.Adv.Mater. 5巻・1号

      Pages: 3-9

    • Related Report
      2004 Annual Research Report
  • [Journal Article] 磁気特性を利用した金属間化合物の非破壊検査2004

    • Author(s)
      馬越佑吉, 安田弘行
    • Journal Title

      検査技術 9巻・11号

      Pages: 13-18

    • NAID

      40006468132

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Nondestructive evaluation of dislocation structure in cyclically deformed Ni3Fe single crystals using magnetic technique.2003

    • Author(s)
      H.Y.Yasuda, A.Sasaki, Y.Umakoshi
    • Journal Title

      Journal of Applied Physics 93

      Pages: 1472-1476

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of interphase boundary character on mechanical properties in NiAl(β) bicrystals with Ni3Al(γ') precipitates along grain boundary.2003

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Mat.Res.Soc.Symp.Proc. 753

      Pages: 297-302

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Observation of deformation substructure in fatigued intermatallic alloys using magnetic properties.2003

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Mta.Res.Soc.Symp.Proc. 753

      Pages: 297-272

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of interphase boundary character on mkechanical properties in NiAl(β) bicrystals with Ni3Al(γ') precipitates along grain boundary.2003

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Mat.Res.Soc.Symp.Proc. 753

      Pages: 297-302

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Observation of deformation substructure in fatigued intermeallic alloys using magnetic properties.2003

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Journal Title

      Mat.Res.Soc.Symp.Proc. 753

      Pages: 267-272

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Formation of deformation bands and precipitation of Ni_3Al(γ') phase in NiAl(β)-based single crystals by thermomechanical processing.2002

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Intermatalics 10

      Pages: 139-149

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Cyclic deformation behavior of γ'-Ni_3(Al,Ti) single crystals containing disordered γ precipitates2002

    • Author(s)
      H.Y.Yasuda, R.Jimba, Y.Umakoshi
    • Journal Title

      Acta Materialia 50

      Pages: 161-169

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Concurrent design for NiAl-based (β/γ') Two phase alloys by controlling microstructure and texture.2002

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Science and Technology of Advanced Materials 3

      Pages: 165-169

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Fatigue mechanism in Ni3Fe single crystals with L1_2 structure.2002

    • Author(s)
      H.Y.Yasuda, D.Furuta, A.Sasaki, A.Izaki, Y.Umakoshi
    • Journal Title

      Acta Materialia 50

      Pages: 2715-2724

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Formation of deformation Bands and precipitation of Ni_3Al(γ') phase in NiAl(β)-based single crystals by thermomechanical processing.2002

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Intermetallics 10

      Pages: 139-147

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Cyclic deformation behavior of γ'-Ni_3(Al,Ti) single crystal containing disordered γ precipitates.2002

    • Author(s)
      H.Y.Yasuda, R.Jimba, Y.Umakoshi
    • Journal Title

      Acta Materialia 50

      Pages: 161-169

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Concurrent design for NiAl-based(β/γ') two-phase alloys by controlling microstructure and texture.2002

    • Author(s)
      T.Sakata, H.Y.Yasuda, Y.Umakoshi
    • Journal Title

      Science and Technology of Advanced Materials 3

      Pages: 161-169

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] fatigue mechanism in Ni_3Fe single crystals with L1_2 superlattice structure.2002

    • Author(s)
      H.Y.Yasuda, D.Furuta, A.Sasaki, A.Izaki, Y.Umakoshi
    • Journal Title

      Acta Materialia 50

      Pages: 2715-2724

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestructive Evaluation of dislocation substructure in cyclically deformed Ni_3Fe single crystals using magnetic technique.

    • Author(s)
      H.Y.Yasuda, A.Sasaki, Y.Umakoshi
    • Journal Title

      Journal of Applied Physics 93

      Pages: 1472-1476

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nondestructive Damage evaluation of γ'-Ni_3(Al,Ti) single crystals Containing disordered γ precipitates.

    • Author(s)
      H.Y.Yasuda, T.Yanai, Y.Umakoshi
    • Journal Title

      Journal of Applied Physics (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Quantitative Analysis of γ precipitates in cyclically deformed Ni_3(Al,Ti) single crystals using magnetic technique.

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda, T.Yanai
    • Journal Title

      Mat.Res.Soc.Symp.Proc. (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Book] Nondestructive lifetime prediction by magnetic measurements, Encyclopedia of Materials2004

    • Author(s)
      Y.Umakoshi, H.Y.Yasuda
    • Publisher
      Elsevier Science
    • Related Report
      2004 Annual Research Report
  • [Publications] H.Y.Yasuda, A.Sasaki, Y.Umakoshi: "Nondestructive evaluation of dislocation structure in cyclically deformed Ni_3Fe single crystals using magnetic techniques"Journal of Applied Physics. 93(3). 1472-1476 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Y.yasuda, R.Jimba, Y.Umakoshi: "Quantitative analysis of anti-phase boundary tubes in cyclically deformed Fe-40at.%Al single crystals by means o magnetic technique"Scripta Materialia. 48. 589-592 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Y.Yasuda, T.Hatta, Y.Umakoshi: "Magnetic observation of deformation substructure in cyclically deformed Fe_3Al single crystals"Science and Technology of Advanced Materials. (In press).

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Umakoshi, H.Y.Ysuda: "Nondestructive lifetime prediction by magnetic measurements"Enyclopedia of Materials : Science and Technology. (In press).

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Sakata, H.Y.Yasuda, Y.Umakoshi: "Formation of defomation bonds and precipitation of Ni_3Al(γ') phase in NiAl(β)-based single unygtol by theimoned and calproces"Intermetallics. 10. 139-147 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] H.Y.Yasuda, R.Jimba, Y.Umakoshi: "Cydic deformation befaviore of γ'-Ni_3(Al, Ti)single cnystal containing dissideed γ precipitates"Acta Materialia. 50. 161-169 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] H.Y.Yasuda, D.Furata, A.Sasaki, Y.Umakoshi: "Fatique mechanism in Ni_3Fe single crystals with W_2 super lattice structure"Acta Materialia. 50. 1715-2724 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] H.Y.Yasuda, R.Jimba, Y.Umakoshi: "Quantitative analysis of anti-phase bocendany tubes in cyclically deformed Fe-40at% Hognesue of magnetic properties"Scripta Materialia. 48. 589-592 (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] X.W.Hi, Y.Umakoshi: "Cyclic deformation behavior of a single-self oriented Fe-35wet%Cr alloy containg fire Curichi precipitate"Scripta Materialia. 48. 545-550 (2003)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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