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Combined electron microscopy for in-situ direct atomistic observation of surface dynamics

Research Project

Project/Area Number 14350018
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field 表面界面物性
Research InstitutionUniversity of Tsukuba

Principal Investigator

KIZUKA Tokushi  University of Tsukuba, Graduate School of Pure and Applied Sciences, Associate Professor, 大学院・数理物質科学研究科, 助教授 (10234303)

Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥7,300,000 (Direct Cost: ¥7,300,000)
Fiscal Year 2004: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2003: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 2002: ¥4,400,000 (Direct Cost: ¥4,400,000)
Keywordselectron microscopy / scanning tunneling microscopy / atomic force microscopyu / surface / nanomaterials / quantized conductance / point contact / friction / 量子コンダクタンス / バリスティック伝導 / ナノテクノロジー / 微細接触 / 接点 / 材料力学 / 微細加工 / ナノデバイス / 高分解能透過電子顕微鏡 / 走査プローブ顕微鏡 / 量子効果デバイ
Research Abstract

The combined electron microscopy of electron microscopy, scanning tunneling microscopy and atomic force microscopy that we had developed was improved for the application in various types of research fields. In the previous method the operation of samples was performed by a manual operation and the observation temperature was restricted to an ambient temperature. In this study, we cleared the restriction and developed the method in order to apply it in researches in various types of scientific and technological fields. We improved spatial resolution of an atom operation and recording method of the image and spectra of the piezo voltage, electric conductance and force. As a result, students of 4th grade in a bachelor course could operate the combined electron microscopy after the instruction of a few months. We also developed several sample stages and new force measurement system. As examples of the application to advanced materials, silicon nanowires of 2 rim in width and 70 nm in length were synthesized by the method. Carbon nanotubes were also fabricated by this method and their properties were analyzed The examples show a highest potential of functions in this method was completed by this study.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (28 results)

All 2004 2003 2002 Other

All Journal Article (16 results) Publications (12 results)

  • [Journal Article] The dynamic observation of the filed emission site of electrons on a carbon nanotube tip2004

    • Author(s)
      T.Kuzumaki, Y.Horiike, T.Kizuka, et al.
    • Journal Title

      Diamond & Related Materials 13

      Pages: 1907-1913

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Co-doping effects of Pb and La in (Bi, Pb)_2(Sr, La)_2CuOy2004

    • Author(s)
      T.Amano, M.Tagami, M.Yokoshima, T.Kizuka et al.
    • Journal Title

      Physica C 412-414

      Pages: 230-234

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] 原子直視観察を利用したナノメートル構造の機械加工2004

    • Author(s)
      木塚 徳志
    • Journal Title

      機械の研究 56

      Pages: 1245-1251

    • NAID

      40006508227

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] アトムファクトリー法にみるナノデバイス技術展望-原子を観て、測り、操る-2004

    • Author(s)
      木塚 徳志
    • Journal Title

      未来材料 4

      Pages: 50-56

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] ナノホール制限成長法によるシリコンナノワイヤー作製2004

    • Author(s)
      木塚 徳志 他
    • Journal Title

      まてりあ 43

      Pages: 363-363

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Molecular dynamics simulations of platinum nanowires based on first principles2004

    • Author(s)
      J.A.Tones, T.Kizuka
    • Journal Title

      Proc.Joint Meeting of FIMS/ITS-NS/CTC/PLASMA I

      Pages: 71-71

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Co-doping effects of Pb and La in (Bi, Pb)_2(Sr, La)_2CuO_y2004

    • Author(s)
      T.Amano, M.Tagami, M.Yokoshima, T.Kizuka, S.Nishizaki, R.Yoshizaki
    • Journal Title

      Physica C 412-414

      Pages: 230-234

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The dynamic observation of the filed emission site of electrons on a carbon nanotube tip2004

    • Author(s)
      T.Kuzumaki, Y.Horiike, T.Kizuka et al.
    • Journal Title

      Diamond & Related Materials 13

      Pages: 1907-1913

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Co-doping effects of Pb and La in (Bi, Pb)_2(Sr, La)_2CuO_y2004

    • Author(s)
      T.Amano, M Tagami, M.Yokoshima T.Kizuka et al.
    • Journal Title

      Physica C 412-414

      Pages: 230-234

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Molecular dynamics simulations of platinum nanowires based on first principles2004

    • Author(s)
      J.A.Torres, T.Kizuka
    • Journal Title

      Proc.Joint Meeting of FIMS/ITS-NS/CTC/PLASMA I

      Pages: 71-71

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Direct observation of electron migration and induced stress in Cu nanowires2003

    • Author(s)
      Satoru Fujisawa, Tokushi Kizuka
    • Journal Title

      Jpn.J.Appl.Phys. 42

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of lateral displacement of atomic force microscope tip caused by contactscanning by in-situ transmission electron microscopy2003

    • Author(s)
      Satoru Fujisawa, Tokushi Kizuka
    • Journal Title

      Jpn.J.Appl.Phys. 42

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Lateral displacement of an AFM tip observed by in-situ TEM/AFM combined microscopy : The effect of the friction in AFM2003

    • Author(s)
      Satoru Fujisawa, Tokushi Kizuka
    • Journal Title

      Tribology Lett. 15

      Pages: 163-168

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Atomistic deformation mechanics of individual nanometer-sized contacts of noble metals2003

    • Author(s)
      Tokushi Kizuka
    • Journal Title

      Recent Research Developments in Applied Physics (Trans World Network, Trivandrum) Vol.6

      Pages: 829-838

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The atomistic deformation mechanics of nanomaterials2002

    • Author(s)
      Tokushi Kizuka
    • Journal Title

      Defect and Diffusion Forum Vols. 206-207

      Pages: 103-110

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] A experimental method for the atomic scale deformation mechanics of nanomaterials2002

    • Author(s)
      Tokushi Kizuka
    • Journal Title

      Recent Research Developments in Applied Chemistry (Trans World Network, Trivandrum) Vol.1

      Pages: 39-47

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Publications] Satoru Fujisawa, Tokushi Kizuka: "Direct observation of electron migration and induced stress in Cu nanowires"Jpn.J.Appl.Phys.. 42. L1433-L1435 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Satoru Fujisawa, Tokushi Kizuka: "Effect of lateral displacement of atomic force microscope tip caused by contact scanning by in-situ transmission electron microscopy"Jpn.J.Appl.Phys.. 42. L1182-L1184 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Satoru Fujisawa, Tokushi Kizuka: "Lateral displacement of an AFM tip observed by in-situ TEM/AFM combined microscopy : The effect of the friction in AFM"Tribology Lett.. 15. 163-168 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Tokushi Kizuka et al.: "Preparation of self-standing silicon nanowires by nanometer tip contact"Proc. 1st International Symposium on Active Nano-Characterization and Technology. 105 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Tokushi Kizuka et al.: "Mechanical Properties of Nanometer-sized Cu Contacts"Proc.Int.Conf. Solid State Devices and Materials. 600-601 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 木塚徳志: "ピエゾ駆動による粒界すべりの電子顕微鏡観察"超音波. 15. 66-68 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Tokushi Kizuka: "The atomistic deformation mechanics of nanomaterials"Defect and Diffusion Forum. 206-207. 103-110 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] Tokushi Kizuka: "A experimental method for the atomic scale deformation mechanics of nanomaterials"Recent Research Developments in Applied Chemistry. 1. 39-47 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] Tokushi Kizuka et al.: "Quantitative microscopy for atomistic deformation mechanics of nanomaterials"Proc.Int.Congress Electron Microscopy. 527-528 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] Tokushi Kizuka et al.: "Atomistic deformation mechanics of nanostructures on surfaces"Proc.Int.Conf. Solid Films and Surfaces. (in print). (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 木塚徳志: "ナノ構造操作のアトムダイナミックス"応用物理学会誌. 71. 989-995 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 木塚徳志: "金原子1個ずつならぶネックレス"パリティ. 17. 21-25 (2002)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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