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PRODUCTION OF HIGH FRACTURE TOUGHNESS AND HIGH FATIGUE STRENGTH BULK METALLIC GLASSES AND EXAMINATION OF THE MECHANISM

Research Project

Project/Area Number 14350063
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionUbe National College of Technology

Principal Investigator

FUJITA Kazutaka  Ube National College of Technology, Mechanical Eng., Prof., 機械工学科, 教授 (10156862)

Co-Investigator(Kenkyū-buntansha) HATANAKA Kenji  Ube National College of Technology, Principal, 校長 (60026193)
KUBUKI Shiro  Ube National College of Technology, Chemical and Biological Eng., Associate Prof., 物質工学科, 助教授 (90321489)
YAMAZAKI Tohru  University of hyogo, Mater. Sci. and Chemistry, Associate Prof., 工学部, 助教授 (30137252)
YOKOHAMA Yoshihiko  Tohoku Univ., Institute of Materials Research, Associate Prof., 金属材料研究所, 助教授 (00261511)
張 涛  東北大学, 金属材料研究所, 助教授 (70250818)
Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥14,000,000 (Direct Cost: ¥14,000,000)
Fiscal Year 2004: ¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 2003: ¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 2002: ¥10,600,000 (Direct Cost: ¥10,600,000)
KeywordsBulk Metallic Glass / Amorphous / Microcrystal / Nanocrystal / Fracture toughness / Fatigue / Tensile strength / Plastic strain / バルクガラス合金 / 破壊靭性 / フラクトグラフィ / 疲労き裂伝ぱ
Research Abstract

Single phase (SF) bulk glassy alloys (BGAs) and nanocrystalline (NC) EGAs of some Zr-, Cu- and Pd-based systems have been synthesized by some fabrication methods. Where, the NC BGA is the glassy alloy which contain nano-scale crystalline particles embedded homogeneously in glassy matrix. Then fatigue strength and fracture toughness in these BGAs were examined.
The ratio of fatigue limit (σ_w ; half a full stress amplitude) under stress ratio of 0.1 to tensile strength (σ_B) of the Zr-based NC BGA showed a value of 15% (σ_B=1.7 GPa), and it was approximately three times larger compared with the ratio of the SF BGA of the same composition. The ratio of σ_w to σ_B of the Cu-based BGA exhibited a very large value of 24% (σ_B=2.0 GPa). These σ_w s show the enough values for applications. It is thought that the drastic rise in the σ_w of these NC BGAs is derived from the prevention of slip initiation and propagation by the NC particles.
A Zr-based BGA with a high degree of amorphousness exhibited a fracture touness value (Kic) of 53 MPa・m^<1/2>. It was clarified that the Zr-based BGA has a sufficient Kic for practical uses. The Kic s of a Zr-based NC BGA and considerably crystallized Zr-based BGA were small even in the maximum value with 40 and 11 MPa・m^<1/2>, respectively. This is thought to be due to the embrittlement by the crystallization.
The Pd-based SF BGA could not have fatigue cracks, and the value of notched fracture toughness exhibit 36 MPa・m^<1/2> and cracks propagated in three or more directions at the same time. An estimated K/c showed a small value of 12 MPa・m^<1/2>.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (17 results)

All 2005 2003 2002 Other

All Journal Article (13 results) Publications (4 results)

  • [Journal Article] 金属ガラスの機械的性質2005

    • Author(s)
      藤田 和孝
    • Journal Title

      金属 75・1

      Pages: 34-40

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Fracture Toughness in Zr-Based Bulk Metallic Glass2005

    • Author(s)
      Kazutaka Fujita
    • Journal Title

      Journal of Metastable & Nanocrystalline Materials (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Mechanical Properties in Bulk Metallic Glasses2005

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      Materials Science & Technology Vol.75-No.1

      Pages: 34-40

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Fracture Toughness in Zr-Based Bulk Metallic Glass2005

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      J. Metastable & Nanocrystalline Materials (in print.)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Fracture Toughness in Zr-Based Bulk Metallic Glass2005

    • Author(s)
      Kazutaka Fujita
    • Journal Title

      Journal of Metastable & Nanocrystalline Materials (発表予定)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Zr基バルク金属ガラスの疲労寿命特性に及ぼすナノ結晶分散効果2003

    • Author(s)
      藤田 和孝
    • Journal Title

      日本金属学会誌 67・2

      Pages: 79-84

    • NAID

      10011456603

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] 薄膜アモルファス合金およびバルクガラス合金における疲労寿命特性の検討2003

    • Author(s)
      藤田 和孝
    • Journal Title

      宇部工業高等専門学校研究報告 49号

      Pages: 1-4

    • NAID

      110000045973

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Effect of Nanocrystalline Dispersion on Fatigue in a Zr-based Bulk Metallic Glass2003

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      J. Japan Inst. Metals Vol.67-No.2

      Pages: 79-84

    • NAID

      10011456603

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] General Tendency on Fatigue Life Properties of Thin Amorphous Alloys and Bulk Glassy Alloys2003

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      Research Reports of Ube National College of Technology No.49

      Pages: 1-4

    • NAID

      110000045973

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] ガラス合金の機械的性質と破壊挙動2002

    • Author(s)
      藤田 和孝
    • Journal Title

      機能材料 22・6

      Pages: 32-34

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Anelastic Behavior under Tensile and Shearing Stresses in Bulk Metallic Glasses2002

    • Author(s)
      Kazutaka Fujita
    • Journal Title

      Materials Transactions 43・8

      Pages: 1957-1960

    • NAID

      10023890934

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Mechanical Properties and Fracture Behaviors in Bulk Glassy Alloys2002

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      Function & Materials Vol.22-No.6

      Pages: 32-34

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Anelastic Behavior under Tensile and Shearing Stresses in Bulk Metallic Glasses2002

    • Author(s)
      Kazutaka FUJITA
    • Journal Title

      Materials Transactions Vol.43-No.8

      Pages: 1957-1960

    • NAID

      10023890934

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Publications] 藤田 和孝: "Zr基バルク金属ガラスの疲労寿命特性に及ぼすナノ結晶分散効果"日本金属学会誌. 67・2. 79-84 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 藤田 和孝: "薄膜アモルファス合金およびバルクガラス合金における疲労寿命特性の検討"宇部工業高等専門学校研究報告. 49号. 1-4 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 藤田和孝: "Zr基バルク金属ガラスの疲労寿命特性に及ぼすナノ結晶分散効果"日本金属学会誌. 67・2. 79-84 (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] 藤田和孝: "薄膜アモルファス合金およびバルクガラス合金における疲労寿命特性の検討"宇部工業高等専門学校研究報告. 49号. 1-4 (2003)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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