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Trial manufacture of dental bonding system to achieve extremely high bond strength

Research Project

Project/Area Number 14370641
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field 補綴理工系歯学
Research InstitutionKagoshima University

Principal Investigator

TANAKA Takuo  Kagoshima University, Graduate School of Medical and Dental Sciences, Professor, 大学院・医歯学総合研究科, 教授 (40113584)

Co-Investigator(Kenkyū-buntansha) ONIZUKA Tadashi  Kagoshima University, Graduate School of Medical and Dental Sciences, Associate Professor, 大学院・医歯学総合研究科, 助教授 (80038877)
KAJIHARA Hirotada  Kagoshima University, University Hospital, Faculty of Medicine and Dentistry, Assistant Professor, 医学部・歯学部附属病院, 講師 (20274855)
KADOKAWA Akihiko  Kagoshima University, Graduate School of Medical and Dental Sciences, Research Associate, 大学院・医歯学総合研究科, 助手 (00169533)
MINAMI Hiroyuki  Kagoshima University, Graduate School of Medical and Dental Sciences, Research Associate, 大学院・医歯学総合研究科, 助手 (50244257)
Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥5,900,000 (Direct Cost: ¥5,900,000)
Fiscal Year 2004: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2003: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2002: ¥4,200,000 (Direct Cost: ¥4,200,000)
KeywordsDental Adhesion System / Adhesive Strength / Acrylic Resin Adhesive / Composite Resin Adhesive / Cohesive Failure / Adhesive Failure / Adhesion Durability / Adhesion Specimen / 圧縮剪断試験 / 凝集強度 / 熱サイクル耐久試験 / 金属接着プライマー / ボンディング材 / 酸化ジルコニウム / 金銀パラジウム合金 / 高強度 / ファインセラミックス / メタルエポキシ樹脂 / フェノールコンパウンド / 接着前処理 / イオンコーティング処理 / シランカップリング処理 / シリカコーティング処理 / 高強度接着 / 高強度接着試験片 / 剪勇断凝集強度 / フェノールコンパウンド樹 / 接着プライマー / ボンディング剤 / Co-Cr合金
Research Abstract

Adhesive resin cement, 4-META/MMA-TBBO resin was developed 25years ago. That is the first product introduced in dental treatment. Then, many types of another adhesives were also induced in clinic. However, their adhesive bonding strength were almost same and concluded in range of 20 to 40MPa. These relatively low bond strengths restrict the treatment method. For example, adhesion fixed partial denture needs metal retainer to retain a pontic on missing tooth position. That is because a distribution occlusal stress on wider adhesion area and to reduce the stress per unit area. If the adhesive bonding strength increased to several times higher value, fixed partial denture with metal free retainer will be realized. To achieve minimum intervention in dental treatment, realization of adhesive bond system, with over 100 MPa bond strength is indispensable. To achieve an extra ordinary high bond strength adhesion system, adhesive material with extra high value of cohesive strength was developed. Composite material of 4-META and polyamides monomer was selected. As an adhered material, cobalt-chromium alloy for dental use which possesses high react ability was chosen. Special constructions method of adhesion specimen was adopted. Higher polymerization temperature of 40〜45℃ used for composite adhesive material. To reduce the void which induces the concentration of stress, 10 atm pressure was added. As a result in this study, 80MPa of adhesive bond strength was attained. However, bonding durability of this system is relatively poor and separation of adhesive occurred at the 300 times of thermo-cycling, at 4℃-60℃.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (23 results)

All 2005 2004 2003 Other

All Journal Article (17 results) Book (1 results) Publications (5 results)

  • [Journal Article] Flexural strengths of denture base resin repaired with auto-polymerizing resin and reinforcements after thermo-cycle stressing2005

    • Author(s)
      Hiroyuki Minami
    • Journal Title

      Journal of Prosthodontics 14

      Pages: 12-18

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The effects of air-abrasion on dentin, enamel, and metal bonding2004

    • Author(s)
      Hirotada Kajihara
    • Journal Title

      American Journal of Dentistry 17

      Pages: 406-411

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In vitro Evaluation of Bond Strength and Surface Roughness of a Resin-paint Material2004

    • Author(s)
      Koichi Muraguchi
    • Journal Title

      Dental Materials Journal 23

      Pages: 406-411

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The Effect of Surface Treatment on the Bonding of an Auto-polymerizing Soft Denture Liner to a Denture Base Resin2004

    • Author(s)
      Hiroyuki Minami
    • Journal Title

      International Journal of Prosthodontics 17

      Pages: 297-301

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In vitro evaluation of the influence of repairing condition of denture base resin on the bonding of auto-polymerizing resins2004

    • Author(s)
      Hiroyuki Minami
    • Journal Title

      Journal of Prosthetic Dentistry 91

      Pages: 164-170

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] The Effects of air-abrasion on dentin, enamel, and metal bonding2004

    • Author(s)
      Hirotada Kajihara
    • Journal Title

      American Journal of Dentistry 17(3)

      Pages: 161-164

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In vitro evaluation of bond strength and surface roughness of a resin-paint material2004

    • Author(s)
      Koichi Muraguchi
    • Journal Title

      Dental Materials Journal 23

      Pages: 406-411

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Bonding strength and durability of alkaline-treated titanium to veneering resin2004

    • Author(s)
      Seiji Ban
    • Journal Title

      Dental Materials Journal 23

      Pages: 424-428

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Bonding strength and durability of alkaline-treated titanium to veneering Resin.2004

    • Author(s)
      Seiji Ban
    • Journal Title

      Dental Materials Journal (Dent Mater J) 23(3)

      Pages: 424-428

    • Related Report
      2004 Annual Research Report
  • [Journal Article] In vitro evaluation of the influence of repairing condition of denture base resin on the bonding of autopolymerizing resins.2004

    • Author(s)
      Hiroyuki Minami
    • Journal Title

      Journal of Proshtetic Dentistry (J Prosthe dent) 91(2)

      Pages: 164-170

    • Related Report
      2004 Annual Research Report
  • [Journal Article] The effect of air-abrasion on dentin, enamel, and metal bonding.2004

    • Author(s)
      Hirotada Kajihara
    • Journal Title

      American Journal of Dentistry (J Amer Dent) 17(3)

      Pages: 161-164

    • Related Report
      2004 Annual Research Report
  • [Journal Article] In vitro evaluation of bond strength and surface roughness of a resin-paint material.2004

    • Author(s)
      Kouichi Muraguchi
    • Journal Title

      Dental Materials Journal (Dent Mater J) 23(3)

      Pages: 406-411

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of surface treatment on the bonding of an autopolymerizing soft denture liner to a denture base resin.2004

    • Author(s)
      Hiroyuki Minami
    • Journal Title

      International journal of prosthodontics 17(3)

      Pages: 297-301

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of Reinforcement Methods on the Retention of Resin-bonded Fixed partial Dentures using a Composite Denture Tooth as a Pontic : In Vitro Evaluation2003

    • Author(s)
      Yoshito Minesaki
    • Journal Title

      The Journal of Adhesive Dentistry 5

      Pages: 225-234

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Bonding abutments to cast metal post/cores : comparison of pre-treatment effects2003

    • Author(s)
      Hirotada Kajihara
    • Journal Title

      Journal of Oral Rehabilitation 30

      Pages: 119-124

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of reinforcement methods on the retention of resin-bonded fixed partial dentures using a composite denture tooth as a pontic : In vitro evaluation.2003

    • Author(s)
      Yoshito Minesaki
    • Journal Title

      The Journal of the Adhesive Dentistry 5(3)

      Pages: 225-235

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In vitro evaluation of toothbrush and generalized wear of luting materials

    • Author(s)
      Shiro Suzuki
    • Journal Title

      American journal of Dentistry (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Book] ステップアップ接着治療(正しい理解と実践)2004

    • Author(s)
      田中卓男
    • Total Pages
      139
    • Publisher
      財団法人 口腔保健協会
    • Related Report
      2004 Annual Research Report
  • [Publications] S.Suzuki, H.Kurashige, T.Tanaka: "In Vitro Simulation of Marginal Degradation of Composite Restrations"International Conference on Composites Engineering. 9. 421-422 (2002)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Kajihara, S.Suzuki, H.Kurashige, Y.Minesaki, T.Tanaka: "In Vitro Simulation of Marginal Degradation of Composite Restrations"International Conference on Composites Engineering. 9. 755-756 (2002)

    • Related Report
      2003 Annual Research Report
  • [Publications] 梶原浩忠, 阿比留史実, 鬼塚 雅, 田中卓男: "ジルコニア系セラミックスのリン酸エステル系レジンセメントに対する接着用表面処理"補綴誌. 47 110回特別号. 153-153 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 阿比留史実, 梶原浩忠, 鬼塚 雅, 田中卓男: "リン酸エステル系レジンセメントに有効なジルコニア系セラミックスの接着用表面処理"補綴誌. 九州支部会抄録集. 18-18 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 鬼塚 雅, 嶺崎良人, 梶原浩忠, 田中卓男: "義歯修理用試作レジンの床用レジンおよびコバルトクロム合金に対する接着性"接着歯学. 21. 167-174 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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