A New Method for Dental Identification by Component Analysis of Dental Porcelain Using Energy Dispersion X-ray Fluorescence Spectrometer
| Project/Area Number |
14370702
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| Research Category |
Grant-in-Aid for Scientific Research (B)
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| Allocation Type | Single-year Grants |
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| Section | 一般 |
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| Research Field |
矯正・小児・社会系歯学
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| Research Institution | Nihon University |
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Principal Investigator |
ABOSHI Hirofumi Nihon University, School of Dentistry, Assistant Professor, 歯学部, 講師 (60212560)
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| Co-Investigator(Kenkyū-buntansha) |
KOMURO Toshinobu Nihon University, School of Dentistry, Professor, 歯学部, 教授 (50139200)
TAKAHASHI Toyoko Nihon University, School of Dentistry, Instructor, 歯学部, 助手 (50120499)
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| Project Period (FY) |
2002 – 2003
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| Project Status |
Completed (Fiscal Year 2003)
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| Budget Amount *help |
¥11,900,000 (Direct Cost: ¥11,900,000)
Fiscal Year 2003: ¥1,400,000 (Direct Cost: ¥1,400,000)
Fiscal Year 2002: ¥10,500,000 (Direct Cost: ¥10,500,000)
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| Keywords | identification / foresic odontology / dental porcelain / fluorescent X ray analysis / component analysis / 物体検査 / 異同識別 |
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| Research Abstract |
The aim of this study was to develop a method of component analysis of dental porcelain by energy dispersion x-ray fluorescence spectrometer, for application in dental identification. As the spectrometer can gather data by scanning the porcelain surface only, this technique is non-destructive, which is of great benefit in forensic situations.
Initially, 14 porcelain samples, designed for crown surface reproduction on porcelain fused metal crown, were processed as a trial to establish a routine for analysis. Eleven (11) products from 6 manufacturers, 76 samples in total, were used as the control samples. The technicians from each company were requested to construct porcelain fused to metal crowns, using 6 kinds of porcelain products only, in shade A3. These acted as the experimental samples.
By simple qualitative analysis, 20 elements were detected in the control porcelain samples and the ratios of elements used were different among the manufacturers. Quantitative analysis by calibration curve indicated that the surface porcelains were composed predominantly of Silicon (Si), Aluminium (Al), and Potassium (K), with weight compositions ranging between 55-70% Si, 10-17% Al, and 7-12% K. A difference in weight composition among the 11 products was detected, particularly in the levels of Silicon and Zirconium.
The names of all 6 manufacturers were correctly identified from the combined qualitative and quantitative analysis results. It was only possible to correctly identify individual samples from each manufacturer in 4 of the 11 samples. The composition of elements and peaks of energy detected from the surfaces of the porcelain fused to metal crowns corresponded accurately to each of the porcelains used in the construction.
Component analysis of dental porcelain will be an effective means of assisting dental identification.
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Report
(3 results)
Research Products
(1 results)
