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Nanostructure fabrication by using photoreactive nanoparticles and characterization of those

Research Project

Project/Area Number 14550802
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field 無機工業化学
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

NIIDOME Yasuro  Kyushu University, Department of Applied Chemistry, Research Associate, 大学院・工学研究院, 助手 (50264081)

Co-Investigator(Kenkyū-buntansha) AKIYAMA Tsuyoshi  Kyushu University, Department of Applied Chemistry, Research Associate, 大学院・工学研究院, 助手 (20304751)
Project Period (FY) 2002 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 2004: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 2003: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2002: ¥1,700,000 (Direct Cost: ¥1,700,000)
KeywordsLaser Deposition / Gold Nanopartilce / Gold Nanorod / Surface Enhanced Raman Scattering / Refractive Index Sensor / 光組織化 / 酸化チタン
Research Abstract

On irradiation with pulsed 532-nm laser light, dodecanethiol(DT)-capped gold nanoparticles (DT-Au) aggregate and fuse in organic solvents. As a result of particle destabilization, the particles are deposited onto a glass substrate immersed in a colloidal cyclohexane solution. Generally, the properties of gold nanoparticles depend strongly on the surface conditions of the particles. In this report, small amounts of immobilized DT molecules were replaced with 1,6-hexanedithiol (HD) molecules, giving gold nanoparticles capped with DT and HD, denoted as (DT+HD)-Au. The amount of HD in (DT+HD)-Au was determined to be 〜6% by elemental analysis. Interestingly, the absorption spectra of DT-Au and (DT+HD)-Au indicated that both particles have similar stabilities in colloidal solution. Despite this, the activities of these gold nanoparticles after laser irradiation differed dramatically. When (DT+HD)-Au was used instead of DT-Au, the degree of growth and deposition of gold nanoparticles was accelerated, and the deposited particles were huge, reaching sizes of several hundreds of nanometers.

Report

(4 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • 2002 Annual Research Report
  • Research Products

    (46 results)

All 2005 2004 2003 Other

All Journal Article (29 results) Patent(Industrial Property Rights) (9 results) Publications (8 results)

  • [Journal Article] Facile Fabrication of Morphology-Controlled Gold Nanoparticle Architectures by Electrolyte-induced Agglomeration and Their Photoelectrochemical Applications2005

    • Author(s)
      T.Akiyama, K.Inoue, Y.Kuwahara, Y.Niidome, N.Terasaki, S.Nitahara, S.Yamada
    • Journal Title

      Langmuir 21・2

      Pages: 793-796

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effects of Ammonium Salts and Anionic Amphiphiles on Photochemical Formation of Gold Nanorods2005

    • Author(s)
      Yasuro Niidome, Koji Nishioka, Hideya Kawasaki, Sunao Yamada
    • Journal Title

      Colloid and Surfaces A Vol.257-258

      Pages: 161-164

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Controlled Release of Plasmid DNA from Gold Nanorods Induced by Pulsed Near-Infrared Light2005

    • Author(s)
      Hironobu Takahashi, Yasuro Niidome, Sunao Yamada
    • Journal Title

      Chemical Communications No.17

      Pages: 2247-2249

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Facile Fabrication of Morphology-Controlled Gold Nanoparticle Architectures by Electrolyte-induced Agglomeration and Their Photoelectrochemical Applications2005

    • Author(s)
      Tsuyoshi Akiyama, Kazuma Inoue, Yutaka Kuwahara, Yasuro Niidome, Nao Terasaki, Satoshi Nitahara, Sunao Yamada
    • Journal Title

      Langmuir Vol.21、No.2

      Pages: 793-796

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Facile Fabrication of Morphology- Controlled Gold Nanoparticle Architectures by Electrolyte-induced Agglomeration and Their Photoelectrochemical Applications2005

    • Author(s)
      T.Akiyama, K.Inoue, Y.Kuwahara, Y.Niidome, N.Terasaki, S.Nitahara, S.Yamada
    • Journal Title

      Langmuir 21・2

      Pages: 793-796

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering of Rhodamine 6G Molecules Adsorbed on Gold Nanorod Films2004

    • Author(s)
      M.Suzuki, Y.Niidome, S.Urakawa, M.Kawahara, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 2 43・4B

    • NAID

      10012904170

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Preparation of Primary Amine-modified Gold Nanoparticles and Their Transfection Ability into Cultivated Cells2004

    • Author(s)
      T.Niidome, K.Nakashima, Hironobu Takahashi, Yasuro Niidome
    • Journal Title

      Chemical Communications --・17

      Pages: 1978-1979

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering from Size- and Morphology-Controlled Gold Nanoparticle Films2004

    • Author(s)
      M.Suzuki, Y.Niidome, Y.Kuwahara, N.Terasaki, K.Inoue, S.Yamada
    • Journal Title

      Journal of Physical Chemistry B 108・10

      Pages: 11660-11665

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effects of Capping Thiols on the Laser-Induced Fusion of Gold Nanoparticles and Deposition onto Glass Substrates in Cyclohexane2004

    • Author(s)
      H.Takahashi, Y.Niidome, T.Sato, S.Yamada
    • Journal Title

      Colloid and Surfaces A 247・1-3

      Pages: 105-113

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Immobilization of Gold Nanorods on the Glass Substrate by the Electrostatic Interactions for Localized Plasmon Sensing2004

    • Author(s)
      Y.Niidome, H.Takahashi, S.Urakawa, K.Nishioka, S.Yamada
    • Journal Title

      Chemistry Letters 33・4

      Pages: 454-455

    • NAID

      10012847382

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Effects of Capping Thiols on the Laser-Induced Fusion of Gold Nanoparticles and Deposition onto Glass Substrates in Cyclohexane2004

    • Author(s)
      Hironobu Takahashi, Yasuro Niidome, Takuro Sato, Sunao Yamada
    • Journal Title

      Colloid and Surfaces A Vol.247、Nos.1-3

      Pages: 105-113

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Preparation of Primary Amine-modified Gold Nanoparticles and Their Transfection Ability into Cultivated Cells2004

    • Author(s)
      Takuro Niidome, Kanako Nakashima, Hironobu Takahashi, Yasuro Niidome
    • Journal Title

      Chemical Communication No.17

      Pages: 1978-1979

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering from Size-and Morphology-Controlled Gold Nanoparticle Films2004

    • Author(s)
      Mototsugu Suzuki, Yasuro Niidome, Yutaka Kuwahara, Nao Terasaki, Kazuma Inoue, Sunao Yamada
    • Journal Title

      Journal of Physical Chemistry B Vol.108

      Pages: 11660-11665

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Immobilization of Gold Nanorods on the Glass Substrate by the Electrostatic Interactions for Localized Plasmon Sensing2004

    • Author(s)
      Yasuro Niidome, Hironobu Takahashi, Shinji Urakawa, Koji Nishioka, Sunao Yamada
    • Journal Title

      Chemistry Letters Vol.33、 No.4

      Pages: 454-455

    • NAID

      10012847382

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering of Rhodamine 6G Molecules Adsorbed on Gold Nanorod Films2004

    • Author(s)
      Mototsugu Suzuki, Yasuro Niidome, Nao Terasaki, Yutaka Kuwahara, Kazuma, Inoue, Sunao Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 2 Vol.43、 No.4B

    • NAID

      10012904170

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering of Rhodamine 6G Molecules Adsorbed on Gold Nanorod Films2004

    • Author(s)
      M.Suzuki, Y.Niiodome, S.Urakawa, M.Kawahara, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 2 43・4B

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Surface-Enhanced Non-Resonance Raman Scattering from Size- and Morphology-Controlled Gold Nanoparticle Films2004

    • Author(s)
      T.Suzuki, Y.Niidome, Y.Kuwahara, N.Terasaki, K.Inoue, S.Yamada
    • Journal Title

      Journal of Physical Chemistry B 108・10

      Pages: 11660-11665

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effects of Capping Thiols on the Laser-Induced Fusion of Gold Nanoparticles and Deposition onto Glass Substrates in Cyclohexane2004

    • Author(s)
      H.Takahashi, Y.Niiodme, T.Sato, S.Yamada
    • Journal Title

      Colloid and Surfaces A 247・1-3

      Pages: 105-113

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Dicroism of Poly(vinylalcohol) Films Containing Gold Nanorods Induced by Polarized Pulsed-Laser Light2003

    • Author(s)
      Y.Niidome, S.Urakawa, M.Kawahara, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 42・4A

      Pages: 1749-1750

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Rapid Synthesis of Gold Nanorods by the Combination of Chemical Reduction and Photoirradiation Processes2003

    • Author(s)
      Y.Niidome, K.Nishioka, H.Kawasaki, S.Yamada
    • Journal Title

      Chemical Communications No.16

      Pages: 2376-2377

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Novel Method for Spatioselective Electroless Plating Catalyzed by Laser-Deposited Gold Nanoparticles2003

    • Author(s)
      Y.Niidome, H.Takahashi, T.Kawasawa, A.Hori, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 42・12

      Pages: 7640-7641

    • NAID

      10011841372

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Particle-size Effects on the Photochurrent Efficiency of Nanostrured Assemblies of Gold Nanoparticles and a Ruthenium Complex-viologen Linked Thiol2003

    • Author(s)
      T.Akiyama, K.Inoue, Y.Kuwahara, N.Terasaki, Y.Niidome, S.Yamada
    • Journal Title

      Journal of Electroanalytical Chemstry 550/551

      Pages: 303-307

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] 光固定した金ナノ粒子を用いたL-システインの表面増強赤外吸収分光分析2003

    • Author(s)
      久鍋秀幸, 新留康郎, 高橋宏信, 山田淳
    • Journal Title

      分析化学 53・9

      Pages: 661-664

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Novel Method for Spatioselective Electroless Plating Catalyzed by Laser-Deposited Gold Nanoparticles2003

    • Author(s)
      Yasuro Niidome, Hironobu Takahashi, Takahiro Kawasawa, Ayako Hori, Sunao Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 Vol.42、No.12

      Pages: 7640-7641

    • NAID

      10011841372

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Rapid Synthesis of Gold Nanorods by the Combination of Chemical Reduction and Photoirradiation Processes2003

    • Author(s)
      Yasuro Niidome, Koji Nishioka, Hideya Kawasaki, Sunao Yamada
    • Journal Title

      Chemical Communications No.16

      Pages: 2376-2377

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Particle-size Effects on the Photochurrent Efficiency of Nanostructured Assemblies of Gold Nanoparticles and a Ruthenium Complex-viologen Linked Thiol.2003

    • Author(s)
      Tsuyoshi Akiyama, Kazuma Inoue, Yutaka Kuwahara, Nao Terasaki, Yasuro Niidome, Sunao Yamada
    • Journal Title

      Journal of Electroanalytical Chemstry Vol.550-551

      Pages: 303-307

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Dichroism of Poly(vinylalcohol) Films Containing Gold Nanorods Induced by Polarized Pulsed-Laser Irradiation.2003

    • Author(s)
      Yasuro Niidome, Shinji Urakawa, Miyuki Kawahara, Sunao Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 Vol.42、No.4A

      Pages: 1749-1750

    • NAID

      10010800213

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Dicroism of Poly(vinylalcohol) Films Containing Gold Nanorods Induced by Polarized Pulsed-Laser Light2003

    • Author(s)
      Y.Niiodome, S.Urakawa, M.Kawahara, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 42・4A

      Pages: 1749-1750

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Novel Method for Spatioselective Electroless Plating Catalyzed by Laser-Deposited Gold Nanoparticles2003

    • Author(s)
      Y.Niidome, H.Takahashi, T.Kawasawa, A.Hori, S.Yamada
    • Journal Title

      Japanese Journal of Applied Physics Part 1 23・12

      Pages: 7640-7641

    • NAID

      10011841372

    • Related Report
      2004 Annual Research Report
  • [Patent(Industrial Property Rights)] ナノ粒子配向薄膜の製造方法2005

    • Inventor(s)
      新留 康郎他4名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Industrial Property Number
      2005-001448
    • Filing Date
      2005-01-17
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 金ナノロッドの製造方法と用途2004

    • Inventor(s)
      新留 康郎他10名
    • Industrial Property Rights Holder
      新留康郎, 三菱マテリアル, 大日本塗料
    • Industrial Property Number
      2004-024006
    • Filing Date
      2004-01-30
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 金属微粒子、それを含む組成物、および金属微粒子の製造方法2004

    • Inventor(s)
      新留 康郎他10名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Filing Date
      2004-09-02
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 金属ナノロッドの製造方法およびその用途2004

    • Inventor(s)
      新留 康郎他11名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Filing Date
      2004-05-13
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] レーザー光照射による酸化物半導体の作製法2004

    • Inventor(s)
      新留 康郎他2名
    • Industrial Property Rights Holder
      科学技術振興機構
    • Industrial Property Number
      2004-083809
    • Filing Date
      2004-03-23
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 金属微粒子、それを含む組成物、および金属微粒子の製造方法2004

    • Inventor(s)
      新留 康郎他10名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Filing Date
      2004-09-02
    • Related Report
      2004 Annual Research Report
  • [Patent(Industrial Property Rights)] 金属ナノロッドの製造方法およびその用途2004

    • Inventor(s)
      新留 康郎他11名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Filing Date
      2004-05-13
    • Related Report
      2004 Annual Research Report
  • [Patent(Industrial Property Rights)] 金ナノロッドの調製法2003

    • Inventor(s)
      新留 康郎他3名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Industrial Property Number
      2003-314203
    • Filing Date
      2003-09-05
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 金ナノロッドの調製法2003

    • Inventor(s)
      新留 康郎他3名
    • Industrial Property Rights Holder
      新留 康郎, 三菱マテリアル, 大日本塗料
    • Industrial Property Number
      2003-135062
    • Filing Date
      2003-05-13
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Publications] Y.Niiodome, S.Urakawa, M.Kawahara, S.Yamada: "Dicroism of Poly(vinylalcohol) Films Containing Gold Nanorods Induced by Polarized Pulsed-Laser Light"Japanese Journal of Applied Physics Part 1. 42・4A. 1749-1750 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Niidome, K.Nishioka, H.Kawasaki, S.Yamada: "Repid Synthesis of Gold Nanorods by the Combination of Chemical Reduction and Photoirradiation Processes"Chemical Communications. No. 16. 2376-2377 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Niidome, H.Takahashi, T.Kawasawa, A.Hori, S.Yamada: "Novel Method for Spatioselective Electroless Plating Catalyzed by Laser-Deposited Gold Nanoparticles"Japanese Journal of Applied Physics Part 1. 42・12. 7640-7641 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Akiyama, K.Inoue, Y.Kuwahara, N.Terasaki, Y.Niidome, S.Yamada: "Particle-size Effects on the Photochurrent Efficiency of Nanostrured Assemblie of Gold Nanoparticles and a Ruthenium Complex-viologen Linked Thiol"Journal of Electroanalytical Chemstry. 550/551. 303-307 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 久鍋秀幸, 新留康郎, 高橋宏信, 山田淳: "光固定した金ナノ粒子を用いたL-システインの表面増強赤外吸収分光分析"分析化学. 53・9. 661-664 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Niidome, H.Takahashi.S.Urakawa, K.Nishioka, S.Yamada: "Immobilization of Gold Nanorods on the Glass Substrate by the Electrostatic Interactions for Localized Plasmon Sensing"Chemistry Letters. (In press). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.Suzuki, Y.Niiodome, S.Urakawa, M.Kawahara, S.Yamada: "Surface-Enhanced Non-Resonance Raman Scattering of Rhodamine 6G Molecules Adsorbed on Gold Nanorod Films"Japanese Journal of Applied Physics Part 2. (In press). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Niiodome, S.Urakawa, M.Kawahara, S.Yamada: "Dicroism of Poly(vinylalcohol) Films Containing Gold Nanorods Induced by Polarized Pulsed-Laser Light"Japanese Journal of Applied Pysics. 42・4A. 1-2 (2003)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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