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Development of Portable Experimental Apparatus on Education of Polymer Physics

Research Project

Project/Area Number 14580182
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Science education
Research InstitutionTokyo University of Agriculture And Technology

Principal Investigator

MIYATA Seizo  Tokyo University of Agriculture And Technology, Pregident, 本部, 学長 (90015066)

Co-Investigator(Kenkyū-buntansha) SAITO Hiromu  Tokyo University of Agriculture And Technology, Faculty of Technology, Associate Professor, 工学部, 助教授 (90196006)
MURASE Shigemitsu  Tokyo University of Agriculture And Technology, Faculty of Technology, Professor, 工学部, 教授 (10323750)
ICHIHARA Shoji  Tokyo University of Agriculture And Technology, Faculty of Technology, Professor, 工学部, 教授 (60323747)
Project Period (FY) 2002 – 2003
Project Status Completed (Fiscal Year 2003)
Budget Amount *help
¥2,900,000 (Direct Cost: ¥2,900,000)
Fiscal Year 2003: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 2002: ¥1,900,000 (Direct Cost: ¥1,900,000)
Keywordspolymer physics / portable apparatus / thermal property / crystallization / polymer blend / mechanical property / internet camera / 力学
Research Abstract

We developed a desk-size experimental apparatus of polymer physics in which one can carry and perform various experiments in lecture for a short time. The apparatus consist of heating block and constant-temperature oven controlled from room temperature to 200℃. We can investigate thermal property of various polymers, or observe phase separation behavior of polymer blends and crystallization behavior of crystalline polymers by observing digital microscope equipped above the heating block; e.g., crystals are melted by heating above the melting temperature while crystallization occurs by cooling below the melting temperature. Mechanical property and optical property can be estimated by the specially designed compact drawing machine equipped in the constant-temperature oven ; e.g., stress relaxation behavior can be investigated by stretching the specimen quickly and the strain remains constant while creep behavior is investigated by applying constant stress. The change of the birefringence during the stress relaxation or creep is also observed by observing the interference colors under two polarizers. In order to perform the above experiments in lecture, we prepare a textbook "Training of Experiment on Polymer Physics" which is instrumental for undergraduate students and corporate researchers. The remote learning system is also constructed by using an internet camera and local area network to perform the experiments in lecture efficiently.

Report

(3 results)
  • 2003 Annual Research Report   Final Research Report Summary
  • 2002 Annual Research Report
  • Research Products

    (60 results)

All Other

All Publications (60 results)

  • [Publications] M.Tsuburaya, H.Saito: "Crystallization of polycarbonate induced by spinodal decomposition in polymer blends"Polymer. 45. 1027-1032 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] S.Takahashi, H.Saito: "Conformational Change of Phenyl Ring Side Group during Stress Relaxation in Glassy Poly(styrene-co-acrylonitrile)"Macromolecules. 37. 1062-1066 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Oda, H.Saito: "Exclusion Effect of Carbon Dioxide on the Crystallization of Polypropylene"J.Polym.Sci., Pt.B, Polym.Phys.. 42. 1565-1572 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 斎藤拓, 薮原哲哉: "超臨界流体を利用した高分子の高次構造制御-分子形態・結晶化・ポリマーブレンド-"成形加工. 15・6. 382-385 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 斎藤拓: "超臨界法を利用した液液相分離による3次元構造制御"機能材料. 23・7. 19-25 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 西原舞, 村瀬繁満: "ポリ乳酸繊維の加水分解速度"繊維学会誌. 59・9. 371-374 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 大滝学, 村瀬繁満: "ポリトリメチレンテレフタレート繊維のアニーリングによる構造変化"高分子論文集. 60・11. 616-621 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "天然繊維を学ぶ"機能材料. 23・10. 63-69 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "高感性繊維"機能材料. 23・11. 59-65 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "高機能性繊維"機能材料. 23・12. 57-63 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "産業資材用高機能性繊維"機能材料. 24・2. 50-56 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "最近話題の繊維"機能材料. 24・3. 65-72 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] S.Murase, A.Inoue, Y.Miyashita, N.Kimura, Y.Nishio: "Structural Characteristics and Moisture Sorption Behavior of Nylon-6/Clay Hybrid Films"J.Polym.Sci., Part B. 40. 479-487 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yoshida, M.Sone, A.Mizushima, K.Abe, X.T.Tao, S.Ichihara, S.Miyata: "Electroplating of nano structured nickel in emulsion of supercritical carbon dioxide and electrolyte solution"Chem.Lett.. 11. 1086 (2002)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yoshida, M.Sone, A.Mizushima, H.Yan, H.vWakabayashi, K.Abe, X.T.Tao, S.Ichihara, S.Miyata: "Application of Emulsion of Dense Carbon Dioxide in Electroplating Solution with Nonionic Surfactants for Nickel Electroplating"Surf.Coat.Tech.. 173. 285 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yan, M.Sone, N.Sato, S.Ichihara, S.Miyata: "The Effects of Dense Carbon Dioxide on Nickel Plating using Emulsion of Carbon Dioxide in Electroplating Solution"Surf.Coat.Tech.. 182. 335 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Wakabayashi, M.Sone, N.Sato, Y.Takada, H.Yan, K.Abe, S.Ichihara, S.Miyata: Surface & Coating Tech.. (in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Mizushima, M.Sone, H.Yan, Ta.Nagai, K.Shigehara, S.Ichihara, S.Miyata: "Nano Grain Deposition via an Electroplating Reaction in an Emulsion of Dense Carbon Dioxide in a Nickel Electroplating Solution Using Nonionic Fluorinated Surfactant"Surface & Coating Tech.. (in press). (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Yamazaki, M.Teduka, K.Ikeda, S.Ichihara: "Preparation of carbon materials with coral-like continuous pores using miscible polymer blends"J.Mater.Chem. 13. 975-977 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Saito, T.Inoue: "Polymer Characterization Techniques and Their Applications to Blends(分担);Chap II : Light and X-ray Scatterings"Oxford University Press. 516 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 斎藤拓: "超臨界流体の最新応用技術(分担);超臨界流体による高分子の精密高次構造制御"エヌティーエス. 324 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 斎藤拓: "ディスプレイ用光学フィルム(分担);高分子フィルムの光学特性と評価"CMC. 217 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 村瀬繁満: "ナノファイバーテクノロジーを用いた高度産業発掘戦略(分担);ナノ粒子とナノコンポジット"CMC. 457 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Tsuburaya, H.Saito: "Crystallization of polycarbonate induced by spinodal decomposition in polymer blends"Polymer. 45. 1027-1032 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] S.Takahashi, H.Saito: "Conformational Change of Phenyl Ring Side Group during Stress Relaxation in Glassy Poly(styrene-co-acrylonitrile)"Macromolecules. 37. 1062-1066 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Oda, H.Saito: "Exclusion Effect of Carbon Dioxide on the Crystallization of Polypropylene"J. Polym. Sci., Pt. B, Polym. Phys.. 42. 1565-1572 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] J.Polym.Sci., Pt.B, Polym.Phys.: "Morphology Control of Polypropyrene by Crystallization under Carbon Dioxide"J. Polym. Sci., Pt. B, Polym. Phys.. 42(in press). (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] S.Murase, A.Inoue, Y.Miyashita, N.Kimura, Y.Nishio: "Structural Characteristics and Moisture Sorption Behavior of Nylon-6/Clay Hybrid Films"J. Polym. Sci., Part B. 40. 479-487 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yoshida, M.Sone, A.Mizushima, K.Abe, X.T.Tao, S Ichihara, S.Miyata: "Electroplating of nano structured nickel in emulsion of supercritical carbon dioxide and electrolyte solution"Chem. Lett.. 11. 1086 (2002)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yoshida, M.Sone, A.Mizushima, H.Yan, H.vWakabayashi, K.Abe, X.T.Tao, S.Ichihara, S.Miyata: "Application of Emulsion of Dense Carbon Dioxide in Electroplating Solution with Nonionic Surfactants for Nickel Electroplating"Surf. Coat. Tech.. 173. 285 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yan, M.Sone, N.Sato, S.Ichihara, S.Miyata: "The Effects of Dense Carbon Dioxide on Nickel Plating using Emulsion of Carbon Dioxide in Electroplating Solution"Surf. Coat. Tech.. 182. 335 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yoshida, M.Sone, H.Wakabayashi, H.Yan, K.Abe, X.T.Tao, A.Mizushima, S.Ichihara, S.Miyata: "New Electroplating Method of Nickel in emulsion of supercritical carbon dioxide and electrolyte solution to enhance Uniformity and Hardness of Plated Film"Thin Solid Films. 446. 194 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Yan, M.Sone, A.Mizushima, T.Nagai, K.Abe, S.Ichihara, S.Miyata: "Electroplating in CO_2-in -Water and Water-in-CO_2 Emulsion using Nickel Electroplating Solution with Anionic Fluorinated Surfactant"Surf. Coat. Tech. 2004. (in press). (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] H.Wakabayashi, M.Sone, N.Sato, Y.Takada, H.Yan, K.Abe, S.Ichihara, S.Miyata: "Nano-Grain Structure of Nickel Films Prepared by Emulsion Plating with Dense Carbon Dioxide"Surface & Coating Tech.. (in press). (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Mizushima, M.Sone, H.Yan, Ta.Nagai, K.Shigehara S.Ichihara, S.Miyata: "Nano Grain Deposition via an Electroplating Reaction in an Emulsion of Dense Carbon Dioxide in a Nickel Electroplating Solution Using Nonionic Fluorinated Surfactant"Surface & Coating Tech.. (in press). (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Yamazaki, M.Teduka.K.Ikeda, S.Ichihara: "Preparation of carbon materials with coral-like continuous pores using miscible polymer blends"J.Mater.Chem.. 13. 975-977 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] M.Tsuburaya, H.Saito: "Crystallization of polycarbonate induced by spinodal decomposition in polymer blends"Polymer. 45. 1027-1032 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] S.Takahashi, H.Saito: "Conformational Change of Phenyl Ring Side Group during Stress Relaxation in Glassy Poly(styrene-co-acrylonitrile)"Macromolecules. 37. 1062-1066 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Oda, H.Saito: "Exclusion Effect of Carbon Dioxide on the Crystallization of Polypropylene"J.Polym.Sci., Pt.B, Polym.Phys.. 42. 1565-1572 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 斎藤拓, 薮原哲哉: "超臨界流体を利用した高分子の高次構造制御-分子形態・結晶化・ポリマーブレンド-"成形加工. 15・6. 382-385 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 斎藤拓: "超臨界法を利用した液液相分離による3次元構造制御"機能材料. 23・7. 19-25 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 西原舞, 村瀬繁満: "ポリ乳酸繊維の加水分解速度"繊維学会誌. 59・9. 371-374 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 大滝学, 村瀬繁満: "ポリトリメチレンテレフタレート繊維のアニーリングによる構造変化"高分子論文集. 60・11. 616-621 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "天然繊維を学ぶ"機能材料. 23・10. 63-69 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "高感受性繊維"機能材料. 23・11. 59-65 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "高機能性繊維"機能材料. 23・12. 57-63 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "産業資材用高機能性繊維"機能材料. 24・2. 50-56 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "最近話題の繊維"機能材料. 24・3. 65-72 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Saito, T.Inoue: "Polymer Characterization Techniques and Their Applications to Blends (分担); Chap 11 : Light and X-ray Scatterings"Oxford University Press. 516 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 斎藤拓: "超臨界流体の最新応用技術(分担);超臨界流体による高分子の精密高次構造制御"エヌティーエス. 324 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 斎藤拓: "ディスプレイ用光学フィルム(分担);高分子フィルムの光学特性と評価"CMC. 217 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 村瀬繁満: "ナノファイバーテクノロジーを用いた高度産業発掘戦略(分担);ナノ粒子とナノコンポジット"CMC. 457 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 三浦慶子, 斎藤 拓: "超臨界法による高分子の高次構造制御とセルロースへの応用の可能性"セルロース学会誌. 9巻3号. 155-159 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 宇野泰光, 宮田清蔵, 村瀬繁満: "フッ素樹脂の溶融紡糸"繊維学会誌. 58巻4号. 143-148 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] S.Murase, N.Kimura, A.Inoue, Y.Miyashita, Y.Nishio: "Structural Characteristics and Moisture Absorption Behavior of Nylon-6/Clay"Journal of Polymer Science, Part B. 40巻6号. 479-487 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] M.Yamazaki, M.Teduka, K.Ikeda, S.Ichihara: "Preparation of Carbon Materials with coral-like Continuous pores Using Miscible Polymer Blends"Journal of Materials Chemistry. (未定). (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] H.Yoshida, M.Sone, A.Mizushima, Abe, X.T.Tao, S.Ichihara, S.Miyata: "Electroplating of Nanostructured Nickel in Emulsion of Supercritical Carbon Dioxide in Electrolyte Solution"Chemistry Letters. 2002. 1086-1087 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 村瀬繁満, 斎藤拓 (分担): "繊維の百科事典"丸善. 1102 (2002)

    • Related Report
      2002 Annual Research Report
  • [Publications] 市原祥次, 村瀬繁満 (分担): "化学便覧(第6版)"丸善. 1709 (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] 市原祥次 (分担): "高分子の寿命予測と長寿命化技術"エヌ・ティー・エス. 1085 (2002)

    • Related Report
      2002 Annual Research Report

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Published: 2002-04-01   Modified: 2016-04-21  

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