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酸化物分散強化鋼の高温照射環境下における強度劣化とその機構の解明

Research Project

Project/Area Number 14F04903
Research Category

Grant-in-Aid for JSPS Fellows

Allocation TypeSingle-year Grants
Section外国
Research Field Nuclear fusion studies
Research InstitutionTohoku University

Principal Investigator

佐藤 裕樹 (2016)  東北大学, 金属材料研究所, 准教授 (20211948)

阿部 弘亨 (2014-2015)  東北大学 (40343925)

Co-Investigator(Kenkyū-buntansha) LI YANFEN  東北大学, 金属材料研究所, 外国人特別研究員
LI Yanfen  東北大学, 金属材料研究所, 外国人特別研究員
Project Period (FY) 2014-04-25 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 2015: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2014: ¥1,200,000 (Direct Cost: ¥1,200,000)
Keywords原子力材料 / 酸化物分散強化鋼 / クリープ強度 / 微細組織変化 / ヘリウム注入 / 高温熱処理 / ナノ粒子 / nuclear materials / oxide dispersion / creep properties / irradiation effect / thermal stability / microstructure / nano-scale particles / ODS steels
Outline of Annual Research Achievements

We studied microstructural evolution and mechanical properties change of an oxide dispersion strengthened steel (12Cr-ODS) for nuclear application.
The effect of high-temperature annealing at 1473-1673 K on the coarsening kinetics of nanoparticles and microstructural evolution was systematically investigated. The nanoparticles were extremely stable and continued precipitating during annealing at 1473 K, whereas, significant coarsening took place during exposure at 1673 K. Furthermore, heterogeneously distributed voids were developed, sizes of which increased distinctly at 1573 and 1673 K for longer holding time. This is probably due to the growth and/or aggregation of Ar-entrapped and pre-existed voids in the as-fabricated condition. Additionally, no obvious changes were observed in texture at 1473 K, except that its intensity reduced. The hardness slightly decreased at 1473 K up to 24 h, however, obvious reduction was observed after annealing at 1573 and 1673 K for more than 6 h.
The helium implantation experiments were carried out in cyclotron accelerator in Tohoku University. The implanted helium reached 390 μm from the surface, and concentration was 35 and 70 appm. The creep properties were tested at 873 and 973 K with different stresses. The helium leaded to slight reduction in creep time-to-rupture and strain-to-rupture at 973 K. While it shows almost no effects at 873 k. It indicates that 12Cr-ODS steel has the good resistance to helium irradiation, which was derived from the high number density and dispersed nano-particles.

Research Progress Status

28年度が最終年度であるため、記入しない。

Strategy for Future Research Activity

28年度が最終年度であるため、記入しない。

Report

(2 results)
  • 2016 Annual Research Report
  • 2014 Annual Research Report
  • Research Products

    (25 results)

All 2017 2016 2015 2014 Other

All Journal Article (15 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 15 results,  Open Access: 1 results,  Acknowledgement Compliant: 1 results) Presentation (9 results) (of which Int'l Joint Research: 1 results) Remarks (1 results)

  • [Journal Article] Microstructural stability of an as-fabricated 12Cr-ODS steel under elevated-temperature annealing2017

    • Author(s)
      J.J. Shen, H.L. Yang, Y.F. Li, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 695 Pages: 1946-1955

    • DOI

      10.1016/j.jallcom.2016.11.029

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Crystallographic analysis on atomic-plane parallelisms between bcc precipitates and hcp matrix in recrystallized Zr-2.5Nb alloys2017

    • Author(s)
      Y. Matsukawa, I. Okuma, H. Muta, Y. Shinohara, R. Suzue, H.L. Yang, T. Maruyama, T. Toyama, J.J. Shen, Y.F. Li, Y. Satoh, S. Yamanaka, H. Abe
    • Journal Title

      Acta Materialia

      Volume: 126 Pages: 86-101

    • DOI

      10.1016/j.actamat.2016.12.053

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Reassessment of oxidation-induced amorphization and dissolution of Nb precipitates in Zr-Nb nuclear fuel cladding tubes.2017

    • Author(s)
      Y. Matsukawa, S. Kitayama, K. Murakami, Y. Shinohara, K. Yoshida, H. Maeno, H.L. Yang, T. Toyama, K. Yasuda, H. Watanabe, A. Kimura, H. Muta, S. Yamanaka, Y.F. Li, Y. Satoh, S. Kano
    • Journal Title

      Acta Materialia

      Volume: 127 Pages: 153-164

    • DOI

      10.1016/j.actamat.2017.01.032

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of fabrication processing on the microstructure and mechanical properties of oxide dispersion strengthening steels2016

    • Author(s)
      YF. Li, JJ. Shen, F. Li, HL. Yang, S. Kano, Y. Matsukawa, Y. Satoh, HY. Fu, H. Abe, T. Muroga
    • Journal Title

      MATERIALS SCIENCE AND ENGINEERING A

      Volume: 654 Pages: 203-212

    • DOI

      10.1016/j.msea.2015.12.032

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microstructural characterization and strengthening mechanisms of a 12Cr-ODS steel2016

    • Author(s)
      J.J. Shen, Y.F. Li, F. Li, H.L. Yang, Z.S. Zhao, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe
    • Journal Title

      Materials Science and Engineering: A

      Volume: 673 Pages: 624-632

    • DOI

      10.1016/j.msea.2016.07.030

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Study on recrystallization and correlated mechanical properties in Mo-modified Zr-Nb alloys2016

    • Author(s)
      H.L. Yang, S. Kano, Y. Matsukawa, Y.F. Li, J.J. Shen, Z.S. Zhao, F. Li, Y. Satoh, H. Abe
    • Journal Title

      Materials Science and Engineering: A

      Volume: 661 Pages: 9-18

    • DOI

      10.1016/j.msea.2016.03.014

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of molybdenum on microstructures in Zr-1.2Nb alloys after β-quenching and subsequently 873 K annealing2016

    • Author(s)
      H.L. Yang, S. Kano, Y. Matsukawa, Y.F. Li, J.J. Shen, F. Li, Z.S. Zhao, Y. Satoh, H. Abe
    • Journal Title

      Materials & Design

      Volume: 104 Pages: 355-364

    • DOI

      10.1016/j.matdes.2016.05.047

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] The effect of crystallographic mismatch on the obstacle strength of second phase precipitate particles in dispersion strengthening: bcc Nb particles and nanometric Nb clusters embedded in hcp Zr2016

    • Author(s)
      Y. Matsukawa, HL. Yang, K. Saito, Y. Murakami, T. Maruyama, T. Iwai, K. Murakami, Y. Shinohara, T. Kido, T. Toyama, Z. Zhao, YF. Li, S. Kano, Y. Satoh, Y. Nagai, H. Abe
    • Journal Title

      ACTA MATERIALIA

      Volume: 102 Pages: 323-332

    • DOI

      10.1016/j.actamat.2015.09.038

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microstructure and mechanical behavior of metallic glass fiberreinforced Al alloy matrix composites2016

    • Author(s)
      Z. Wang, K. Georgarakis, K. S. Nakayama, Y. Li, A. A. Tsarkov, G. Xie, D. Dudina, D. V. Louzguine-Luzgin, A. R. Yavari
    • Journal Title

      Scientific Reports

      Volume: 6 Pages: 24384-24384

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] In-Situ High-Resolution Transmission Electron Microscopy Investigation of Overheating of Cu Nanoparticles2016

    • Author(s)
      C. Chen, Z. Hu, Y. F. Li, L. Liu, H. Mori, Z. Wang
    • Journal Title

      Scientific Reports

      Volume: 6 Pages: 19545-19545

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effects of alloying elements (Sn, Nb, Cr, and Mo) on the microstructure and mechanical properties of zirconium alloys2015

    • Author(s)
      Huilong Yang, Jingjie Shen, Yoshitaka Matsukawa, Yuhki Satoh, Sho Kano, Zishou Zhao, Yanfen Li, et al.,
    • Journal Title

      Journal of Nuclear Science and Technology

      Volume: in press

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Grain structural characterization of 9Cr-ODS steel aged at 973 K up to 10,000 h by electron backscatter diffraction2014

    • Author(s)
      Yanfen Li, H. Abe, et al.,
    • Journal Title

      Journal of Nuclear Materials

      Volume: 45 Pages: 568-572

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Fabrication andcharacterization of reference 9Cr and 12Cr-ODS low ctivation ferriticmartensitic steels2014

    • Author(s)
      T. Muroga, T. Nagasaka, Y. Li, et al.,
    • Journal Title

      Fusion Engineering and Design

      Volume: 89 Pages: 1717-1722

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Stability of Oxide Particles under Electron Irradiation in a 9Cr ODS Steel at 400°C2014

    • Author(s)
      Feng Li, Hiroaki Abe, Takahiro Ishizaki, Yanfen Li, et al.,
    • Journal Title

      Journal of Nuclear Materials

      Volume: 45 Pages: 724-727

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] New Approach to In Situ Observation Experiments under Irradiation in High Voltage Electron Microscopes2014

    • Author(s)
      Hiroaki Abe, Takahiro Ishizaki, Feng Li, Sho Kano, Yanfen Li, et al.,
    • Journal Title

      Materials Transactions

      Volume: 55 Pages: 423-427

    • NAID

      130004455279

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Presentation] Investigation on creep behavior and fracture mechanisms of oxide dispersion strengthening ferritic steel2016

    • Author(s)
      Yanfen Li, H.L. Yang, J.J. Shen, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe
    • Organizer
      第132回金属材料研究所講演会
    • Place of Presentation
      仙台市
    • Year and Date
      2016-11-24
    • Related Report
      2016 Annual Research Report
  • [Presentation] Stability of as-fabricated and cold-rolled 12Cr-ODS steel during high temperature annealing2016

    • Author(s)
      J.J. Shen, H. Yang, Y. Li, F. Li, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe
    • Organizer
      The Ninth Pacific Rim International Conference on Advanced Materials and Processing (PRICM9)
    • Place of Presentation
      京都市
    • Year and Date
      2016-08-01
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 燃料被覆管の安全設計基準に資する環境劣化評価手法に関する研究開発 - 材料特性の環境劣化影響の評価2015

    • Author(s)
      叶野翔、楊会龍、李艶芬、松川義孝、佐藤祐樹、藪内聖皓, 阿部弘亨、等
    • Organizer
      2015年日本原子力学会春の大会
    • Place of Presentation
      茨城大学
    • Year and Date
      2015-03-20 – 2015-03-22
    • Related Report
      2014 Annual Research Report
  • [Presentation] Effects of excess oxygen level on mechanical properties and microstructure for two 9Cr-ODS steel2015

    • Author(s)
      Yanfen Li, J.J. Shen, F. Li, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe, T. Muroga
    • Organizer
      2015年日本金属学会春季大会
    • Place of Presentation
      東京大学
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] Recrystallization behavior and microstructure evolution during annealing of a cold-rolled 12Cr-ODS steel2015

    • Author(s)
      J.J. Shen, Yanfen Li, Feng Li, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe
    • Organizer
      2015年日本金属学会春季大会
    • Place of Presentation
      東京大学
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] Effects of fabrication routes on mechanical properties and microstructure for two 12Cr-ODS ferritic steels2014

    • Author(s)
      Yanfen Li, F. Li, J.J. Shen, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe, T. Muroga
    • Organizer
      材料試験炉に関する国際シンポジウム, 2014年度大洗研究会
    • Place of Presentation
      東北大学
    • Year and Date
      2014-12-11 – 2014-12-12
    • Related Report
      2014 Annual Research Report
  • [Presentation] Anisotropy in microstructures and mechanical properties of ODS ferritic steels2014

    • Author(s)
      Yanfen Li, F. Li, J.J. Shen, S. Kano, Y. Matsukawa, Y. Satoh, H. Abe, H.Y. Fu, T. Muroga
    • Organizer
      2014年日本原子力学会秋の大会
    • Place of Presentation
      京都大学
    • Year and Date
      2014-09-08 – 2014-09-10
    • Related Report
      2014 Annual Research Report
  • [Presentation] Effect of microstructural evolution on the stability of oxide nano-particles in ODS steels under electron irradiation2014

    • Author(s)
      Feng Li, H. Abe, T. Ishizaki, Yanfen Li, T. Nagasaka, T. Muroga, T. Nagase, H. Yasuda
    • Organizer
      2014年日本原子力学会秋の大会
    • Place of Presentation
      京都大学
    • Year and Date
      2014-09-08 – 2014-09-10
    • Related Report
      2014 Annual Research Report
  • [Presentation] Study on Anisotropy of Mechanical Property and Microstructure of 12Cr Ferritic - Oxide Dispersion Strengthened Steel2014

    • Author(s)
      Yanfen Li, H. Abe, Y. Satoh, Y. Matsukawa, F. Li, J.J. Shen, T. Muroga
    • Organizer
      2014年度春季第127回金属材料研究所講演会
    • Place of Presentation
      東北大学
    • Year and Date
      2014-05-28
    • Related Report
      2014 Annual Research Report
  • [Remarks] 原子力材料工学/Nuclear Materials Engineering

    • URL

      http://nuclmater.imr.tohoku.ac.jp/index.html

    • Related Report
      2016 Annual Research Report

URL: 

Published: 2015-01-22   Modified: 2024-03-26  

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