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Measurements of electron density and electron temperature with plasma absorption probe and its application to deposited plasmas

Research Project

Project/Area Number 15340200
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Plasma science
Research InstitutionChubu University

Principal Investigator

NAKAMURA Keiji  Chubu University, Depart.Electrical Eng., Associate professor, 工学部, 助教授 (20227888)

Co-Investigator(Kenkyū-buntansha) IKEZAWA Shunjiro  Chubu University, Depart.Electronics, Professor, 工学部, 教授 (60065282)
YAMAGUCHI Sataro  Chubu University, Depart.Electrical Eng., Professor, 工学部, 教授 (10249964)
SUGAI Hideo  Nagoya university, Depart.Electrical Eng., Professor, 大学院・工学研究科, 教授 (40005517)
豊田 直樹  (株)ニッシン, 技術部・研究員
木下 啓蔵  超先端電子技術開発機構, 半導体MIRAIプロジェクト, サブグループリーダー(研究職)
Project Period (FY) 2003 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥13,200,000 (Direct Cost: ¥13,200,000)
Fiscal Year 2005: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 2004: ¥5,300,000 (Direct Cost: ¥5,300,000)
Fiscal Year 2003: ¥6,300,000 (Direct Cost: ¥6,300,000)
Keywordsplasma processing / electron density / deposition film / plasma absorption probe / dispersion relation / surface wave / sheath / 電子温度
Research Abstract

Recently, high performance LSI electronic devices has been studied to improve capability, calculation speed and power consumption. To achieve this issue, microfabrication with a feature size less than 〜100 nm and low-k materials for improvement of signal delay at distribution lines have been developed. Plasma processing has been widely used for the microfabrication and the low-k film formation, however there are still various problems to be solved. Understanding of plasma properties and precise control of the plasma suitable for desired process have been requred.
In this work, plasma absorption probes which enable us to measure electron density even under soiled conditions of insulated polymer deposition were improved to measure electron temperature of important parameters to characterize the plasma. We also applied the probe to diagnostics of CVD plasmas for the low-k film formation, and fundamental data to improve the materials process were obtained.
A sheath around the probe antenna a … More ffects on an absorption frequency measured with the probe, and sheath thickness is given by a several times of Debye length as a function of electron density and electron temperature. Therefore, when absorption frequencies are measured two surface wave absorption probes having different dependence on the sheath thickness, both of electron density and electron temperature can be simultaneously obtained. An antenna diameter of the probe significantly affected on the relation between the electron density and electron temperature, and the electron density satisfying the measured absorption frequency became independent of electron temperature as the antenna diameter increased. The different temperature dependence of the satisfying density between the two probes was preferable to accurately determine the density and the temperature. Therefore, the probes with much different antenna diameter were preferable to achieve accurate measurements. Finally, electron density and electron was available with the almost same accuracy of a conventional Langmuir probe.
The probe revealed the following characteristics of a narrow gap CVD plasma system for low-k film deposition. (1)An electron density as well as its radial profile significantly depended on conditions such as discharge powers and operating pressures, and a correlation between radial profiles of the electron density and a deposition rate over a 12-inch-diam. silicon wafer. (2)An electron temperature decreased with an increase in the total operating pressure as well as a fraction of parent material gases. Xe addition was also effective for reduction of the electron temperature. However significant radial profile was not clearly observed.
As derivative results, the probe system was also applied to other plasma systems for materials processing, and useful for their plasma diagnostics. Less

Report

(4 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (24 results)

All 2006 2005 2004 Other

All Journal Article (21 results) Publications (3 results)

  • [Journal Article] Investigetion on Surface Wave Probe for Measurements of Electron Density and Electron Temperature2006

    • Author(s)
      O.Hirono ほか 2名
    • Journal Title

      Proc. 6th Int. Conf. Reactive Plasmas(ICRP-6)/23rd Symp. Plasma Processing(January 2006,Japan)

      Pages: 727-728

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Decay Characterristics of Radical Denssities under Ion Bombardment in Fluorocarbon Plasmas2006

    • Author(s)
      K.Kumagai ほか 4名
    • Journal Title

      Proc. 6th Int. Conf. Reactive Plasmas(ICRP-6)/23rd Symp. Plasma Processing(January 2006,Japan)

      Pages: 477-478

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Investigation on Surface Wave Probe for Measurements of Electron Density and Electron Temperature2006

    • Author(s)
      O.Hirano, K.Nakamura, H.Sugai
    • Journal Title

      Proc.6th Int.Conf.Reactive Plasmas (ICRP-6)/ 23rd Symp.Plasma Processing, (January 2006, Japan), P-3B-14

      Pages: 727-728

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Stabilization of Radical Density in Fluorocarbon Plasmas2005

    • Author(s)
      K.Nakamura ほか 3名
    • Journal Title

      Proc. Int. Symp. Dry Process(DPS2005) (November 2005, Korea)

      Pages: 99-100

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Electron Density Measurements with Surface Wave Probes in Magnetized Plasmas2005

    • Author(s)
      K.Nakamura ほか 2名
    • Journal Title

      American Vacuum Society 52nd Int. Symp. & Exhibition

      Pages: 107-107

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Distributions of slectron density and deposition rate of anarrow-gap plasmas polymerization system2005

    • Author(s)
      K.Kinoshita ほか 6名
    • Journal Title

      Proc. 27th Int. Conf. Phenomena in Ionized Gases(ICPIG-2005) (July 2005, The Netherlands)

      Pages: 10-200

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Ionization Enhancement of Zirconium Atoms in Inductively Coupled Discharge2005

    • Author(s)
      K.Nakamura ほか 2名
    • Journal Title

      Surface and Coating Technology Vol. 196 No. 1-3

      Pages: 188-191

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Ionization Enhancement of Zirconium Atoms in Inductively Coupled Discharge2005

    • Author(s)
      K.Nakamura, H.Yoshinaga, K.Yukimura
    • Journal Title

      Surf.Coat.Technol. Vol.196, No.1-3

      Pages: 188-191

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Droplet-Free High-Density Metal Ion Source for Plasma Immersion Ion Implantation2005

    • Author(s)
      K.Nakamura, H.Yoshinaga, K.Yukimura
    • Journal Title

      Nuclear Instruments and Methods in Physics research B 242

      Pages: 315-317

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Ionization Enhancement of Zirconium Atoms in Inductively Coupled Discharge2005

    • Author(s)
      K.Nakamura, H.Yoshinaga, K.Yukimura
    • Journal Title

      Surf.Coat.Technol. 196

      Pages: 188-191

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Ionization Fraction in Sputter-Based Copper Ion Sources for Plasma Immersion Ion Implantation2005

    • Author(s)
      K.Nakamura, H.Suzuki
    • Journal Title

      Surf.Coat.Technol. 196

      Pages: 180-183

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Distributions of electron density and deposition rate of a narrow-gap plasma polymerization system2005

    • Author(s)
      K.Kinoshita, K.Nakamura, J.Kawahara, O.Kiso, N.Toyoda, H.Sugai, T.Kikkawa
    • Journal Title

      XXVII International Conference on Phenomena in Ionized Gases, (July 17-22, Netherlands), 10-200 CD-ROM

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Electron Density Measurements with Surface Wave Probes in Magnetized Plasmas2005

    • Author(s)
      K.Nakamura, S.Yajima, H.Sugai
    • Journal Title

      American Vacuum Society 52nd Int.Symp.& Exhibition(October 2005, U.S.A) PS-TuP22

      Pages: 107-107

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Electron Density Monitoring by Surface Wave Probe in Magnetic Field2004

    • Author(s)
      S.Yajima ほか2名
    • Journal Title

      Proc Int.Symp.Dry Process

      Pages: 81-84

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Polymer Deposition and Radical Composition in Fluorocarbon Plasma Source2004

    • Author(s)
      K.Nakamura ほか4名
    • Journal Title

      Proc Int.Symp.Dry Process

      Pages: 163-168

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Measurements of Electron Density in Low-Density/High-Pressure Plasmas with Surface Wave Probe2004

    • Author(s)
      K.Nakamura ほか5名
    • Journal Title

      Proc Int.Symp.Dry Process

      Pages: 169-174

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Investigation on Surface Wave Probe for Measurements of Electron Density and Electron Temperature

    • Author(s)
      O.Hirano, K.Nakamura, H.Sugai
    • Journal Title

      Proc.6th Int.Conf.Reactive Plasmas (ICRP-6)/23rd Symp.Plasma Processing (January 2006, Japan) P-3B-14

      Pages: 727-728

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Decay Characteristics of Radical Densities under Ion Bombardment in Fluorocarbon Plasmas

    • Author(s)
      K.Kumagai, T.Tatsumi, K.Oshima, k.Nagahata, K.Nakamura
    • Journal Title

      Proc.6th Int.Conf.Reactive Plasmas (ICRP-6)/23rd Symp.Plasma Processing (January 2006, Japan) P-2A-43

      Pages: 477-478

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Stabilization of Radical Density in Fluorocarbon Plasmas

    • Author(s)
      K.Nakamura, K.Kumagai, T.Tatsumi, K.Oshima
    • Journal Title

      Proc.Int.Symp.Dry Process (DPS2005);(November 2005, Korea) 5-36

      Pages: 99-100

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Electron Density Measurements with Surface Wave Probes in Magnetized Plasmas

    • Author(s)
      K.Nakamura, S.Yajima, H.Sugai
    • Journal Title

      American Vacuum Society 52nd Int.Symp. & Exhibition (October 2005, U.S.A) PS-TuP22

      Pages: 107-107

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Distributions of electron density and deposition rate of a narrow-gap plasma polymerization system

    • Author(s)
      K.Kinoshita, K.Nakamura, J.Kawahara, O.Kiso, N.Toyoda, H.Sugai, T.Kikkawa
    • Journal Title

      Proc.27th Int.Conf Phenomena in Ionized Gases(ICPIG-2005);(July 2005, The Netherlands) 10-200

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Publications] K.Nakamura 他2名: "Highly sensitive plasma absorption probe for measuring low-density high-pressure plasmas"Journal of Vacuum Science & Technology A. 21. 325-331 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.Nakamura 他2名: "Novel Plasma Sensor Detecting Abnormal Density Variations in Reactors for Mass-Production"Proc.Int.Symp.Dry Process (DPS2003). 157-162 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.Nakamura 他2名: "Measurement of Electron Density and Temperature with Plasma Absorption Probe"26th Int.Conf.Phenomena in Ionized Gases. 1. 185-186 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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